In situ capabilities of Small Angle X-ray Scattering

Feng, Jinghua; Kriechbaum, Manfred; Liu, Li (Emily)

doi:10.1515/ntrev-2019-0032

In situ capabilities of Small Angle X-ray Scattering

Journal Article · Wed Dec 04 04:00:00 EST 2019 · Nanotechnology Reviews

DOI:https://doi.org/10.1515/ntrev-2019-0032· OSTI ID:1613517

Feng, Jinghua ^[1]; Kriechbaum, Manfred; Liu, Li (Emily)

DOE/OSTI

Abstract

Small Angle X-ray Scattering (SAXS) is an ideal characterization tool to explore nanoscale systems. In order to investigate nanostructural changes of materials under realistic sample environments, it is essential to equip SAXS with diversein situcapabilities based on the corresponding requirements. In this paper, we highlight the representative experimental setups and corresponding applications of five widely usedin situcapabilities: temperature, pressure, stretching, flow-through, and electric field. Additionally, we also briefly introduce other fourin situtechniques including humidity, high-throughput, rheology, and magnetic field.

Research Organization:: Rensselaer Polytechnic Inst., Troy, NY (United States)

Sponsoring Organization:: USDOE Office of Energy Efficiency and Renewable Energy (EERE)

DOE Contract Number:: EE0008380

OSTI ID:: 1613517

Journal Information:: Nanotechnology Reviews, Journal Name: Nanotechnology Reviews Journal Issue: 1 Vol. 8; ISSN 2191-9097

Publisher:: de Gruyter

Country of Publication:: United States

Language:: English

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Nanostructured composite membrane with cross-linked sulfonated poly(arylene ether ketone)/silica for high-performance polymer electrolyte membrane fuel cells under low relative humidity Bae, Insung; Oh, Keun-Hwan; Yun, Minhyuk Journal of Membrane Science, Vol. 549 https://doi.org/10.1016/j.memsci.2017.12.060	journal	March 2018
Time-Resolved SAXS Study of Nucleation and Growth of Silica Colloids Pontoni, D.; Narayanan, T.; Rennie, A. R. Langmuir, Vol. 18, Issue 1 https://doi.org/10.1021/la015503c	journal	January 2002
LSPR and SAXS studies of starch stabilized Ag–Cu alloy nanoparticles Singh, Manjeet; Sinha, I.; Singh, A. K. Colloids and Surfaces A: Physicochemical and Engineering Aspects, Vol. 384, Issue 1-3 https://doi.org/10.1016/j.colsurfa.2011.05.037	journal	July 2011
Microstructural characterization of polycrystalline materials by synchrotron X-rays Wang, Leyun; Li, Meimei; Almer, Jonathan Frontiers of Materials Science, Vol. 7, Issue 2 https://doi.org/10.1007/s11706-013-0201-0	journal	May 2013
The thermodynamic properties of flow-induced precursor of polyethylene Liu, Dong; Cui, Kunpeng; Huang, Ningdong Science China Chemistry, Vol. 58, Issue 10 https://doi.org/10.1007/s11426-015-5361-6	journal	March 2015
Structural investigation on bulk poly(3-hexylthiophene): Combined SAXS, WAXD, and AFM studies Canetti, Maurizio; Bertini, Fabio; Scavia, Guido European Polymer Journal, Vol. 45, Issue 9 https://doi.org/10.1016/j.eurpolymj.2009.06.012	journal	September 2009

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Synchrotron Scattering Methods for Nanomaterials and Soft Matter Research Narayanan, Theyencheri; Konovalov, Oleg Materials, Vol. 13, Issue 3 https://doi.org/10.3390/ma13030752	journal	February 2020

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