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Elucidation of the photoaquation reaction mechanism in ferrous hexacyanide using synchrotron x-rays with sub-pulse-duration sensitivity

Journal Article · · Journal of Chemical Physics
DOI:https://doi.org/10.1063/1.5117318· OSTI ID:1607390
 [1];  [1];  [2];  [1];  [1];  [1];  [1];  [1];  [3];  [2];  [4];  [5];  [6];  [4];  [2];  [1]
  1. Argonne National Lab. (ANL), Lemont, IL (United States)
  2. Pacific Northwest National Lab. (PNNL), Richland, WA (United States). Environmental Molecular Sciences Lab. (EMSL)
  3. Lund Univ. (Sweden)
  4. European X-ray Free-Electron Laser (XFEL), Hamburg (Germany)
  5. Wigner Research Centre for Physics, Hungarian Academy Sciences, H-1525 Budapest, Hungary
  6. Hungarian Academy Sciences, Budapest (Hungary). Wigner Research Centre for Physics
Ligand substitution reactions are common in solvated transition metal complexes, and harnessing them through initiation with light promises interesting practical applications, driving an interest in new means of probing their mechanisms. In this work, using a combination of timeresolved x-ray absorption spectroscopy (XAS) and hybrid quantum mechanical, molecular mechanics (QM/MM) molecular dynamics (MD) simulations and x-ray absorption nearedge spectroscopy (XANES) calculations, we elucidate the mechanism of photoaquation in the model system iron(II) hexacyanide, where UV excitation results in the exchange of a CN ligand with a water molecule from the solvent. We take advantage of the high flux and stability of synchrotron x-rays to capture high precision x-ray absorption spectra that allow us to overcome the usual limitation of the relatively long x-ray pulses and extract the spectrum of the short-lived intermediate pentacoordinated species. Additionally, we determine its lifetime to be 19 (±5) ps and kinetic fits suggest a formation time of 1.5 (0.6) ps. The QM/MM simulations support our experimental findings and explain the ~20 ps timescale for aquation as involving interconversion between the square pyramidal (SP) and trigonal bipyramidal (TBP) pentacoordinated geometries, with aquation being only active in the SP configuration.
Research Organization:
Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Sponsoring Organization:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22). Chemical Sciences, Geosciences & Biosciences Division; USDOE Office of Science (SC), Biological and Environmental Research (BER) (SC-23)
Grant/Contract Number:
AC02-06CH11357
OSTI ID:
1607390
Alternate ID(s):
OSTI ID: 1608558
OSTI ID: 1570031
Journal Information:
Journal of Chemical Physics, Journal Name: Journal of Chemical Physics Journal Issue: 14 Vol. 151; ISSN 0021-9606
Publisher:
American Institute of Physics (AIP)Copyright Statement
Country of Publication:
United States
Language:
English

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