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Direct formation of metal nanoparticles using ultrasound

Patent ·
OSTI ID:1600440

A method for creating nanoparticles directly from bulk metal by applying ultrasound to the surface in the presence of a two-part surfactant system. Implosive collapse of cavitation bubbles near the bulk metal surface generates powerful microjets, leading to material ejection. This liberated material is captured and stabilized by a surfactant bilayer in the form of nanoparticles. Nanoparticles can be produced regardless of the bulk metal form factor. The method is generally applicable of metals and alloys. The method can be applied to an environmentally important problem, the reclamation of gold from an electronic waste stream.

Research Organization:
National Technology & Engineering Solutions of Sandia, LLC, Albuquerque, NM (United States)
Sponsoring Organization:
USDOE National Nuclear Security Administration (NNSA)
DOE Contract Number:
NA0003525
Assignee:
National Technology & Engineering Solutions of Sandia, LLC (Albuquerque, NM)
Patent Number(s):
10,518,330
Application Number:
16/219,482
OSTI ID:
1600440
Country of Publication:
United States
Language:
English

References (22)

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Digestive Ripening of Thiolated Gold Nanoparticles:  The Effect of Alkyl Chain Length journal October 2002
Gold nanoparticles obtained by aqueous digestive ripening: Their application as X-ray contrast agents journal February 2015
Micro- and nano-spheres of low melting point metals and alloys, formed by ultrasonic cavitation journal January 2013
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Rapid formation of high-quality self-assembled monolayers of dodecanethiol on polycrystalline gold under ultrasonic irradiation journal March 2008
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Interparticle collisions driven by ultrasound journal March 1990
Measuring cavitation and its cleaning effect journal March 2016
Using sonochemistry for the fabrication of nanomaterials journal April 2004
Continuous microfluidic synthesis and functionalization of gold nanorods journal February 2016
Surface acoustic cavitation understood via nanosecond electrochemistry. Part III: shear stress in ultrasonic cleaning journal November 2002
A facile way for preparing tin nanoparticles from bulk tin via ultrasound dispersion journal January 2007
A Technical Method of Extraction of gold from E-Waste: a Multi-Sensor Based Method Using Microcontroller journal May 2014
Sonophysical cost effective rapid indigenous preparation of aluminium particles via exfoliation of aluminium foil journal January 2016
Measurement and Modeling of Propeller Cavitation in Uniform Inflow journal July 2004
Size-Controlled Synthesis of Gold Nanoparticles from Bulk Gold Substrates by Sonoelectrochemical Methods journal November 2004
Observations of cavitation erosion pit formation journal July 2013
Synthesis of low-melting-point metallic nanoparticles with an ultrasonic nanoemulsion method journal May 2011

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