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Title: Binder jet additive manufacturing method to fabricate near net shape crack-free highly dense Fe-6.5 wt.% Si soft magnets

Journal Article · · Heliyon

High silicon (Si) electrical steel has the potential for efficient use in applications such as electrical motors and generators with cost-effective in processing, but it is difficult to manufacture. Increasing the Si content beyond 3 wt.% improves magnetic and electrical properties, with 6.5 wt.% being achievable. The main goal of this research is to design, develop, and implement a scalable additive manufacturing process to fabricate Fe with 6.5 wt.% Si (Fe–6Si) steel with high magnetic permeability, high electrical resistivity, low coercivity, and low residual induction that other methods cannot achieve because of manufacturing limitations. Binder jet additive manufacturing was used to deposit near net shape components that were subsequently sintered via solid-state sintering to achieve near full densification. Here, it is shown that the use of solid-state sintering mitigates cracking since no rapid solidification occurs unlike fusion-based additive technologies. The Fe–6Si samples demonstrated an ultimate tensile strength of 434 MPa, electrical resistivity of 98 μΩ cm, and saturation magnetization of 1.83 T with low coercivity and high permeability. The results strongly supports to replace the only available 0.1 mm thick chemical vapor deposition (CVD) produced Si steel using the cost effective AM method with good mechanical and magnetic properties for motor applications.

Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Organization:
USDOE Office of Energy Efficiency and Renewable Energy (EERE)
Grant/Contract Number:
AC05-00OR22725
OSTI ID:
1574542
Alternate ID(s):
OSTI ID: 1607076
Journal Information:
Heliyon, Journal Name: Heliyon Vol. 5 Journal Issue: 11; ISSN 2405-8440
Publisher:
ElsevierCopyright Statement
Country of Publication:
United Kingdom
Language:
English

References (29)

Relative effect(s) of texture and grain size on magnetic properties in a low silicon non-grain oriented electrical steel journal August 2003
Magnetic properties evaluation of spray formed and rolled Fe–6.5wt.% Si–1.0wt.% Al alloy journal March 2007
Review of Fe-6.5 wt%Si high silicon steel—A promising soft magnetic material for sub-kHz application journal July 2019
Evolution of Optimum Grain Size for Low Loss Ferritic FeSi Steels journal September 2017
Big Area Additive Manufacturing of High Performance Bonded NdFeB Magnets journal October 2016
Binder Jetting: A Novel NdFeB Bonded Magnet Fabrication Process journal April 2016
Production of high silicon steel for electrical applications by thermomechanical processing journal December 2003
Texture of Cold Rolled Strip of Fe-3Si Steel Produced by Thin Slab Casting and Rolling journal March 2011
Basic Investigation of CVD Method for Manufacturing 6.5% Si Steel Sheet. journal January 1996
High-silicon steel produced by hot dipping and diffusion annealing journal January 2002
Texture and magnetic properties of rapidly quenched Fe-6.5wt%Si ribbon journal July 1984
Coincidence Site Lattice (CSL) grain boundaries and Goss texture development in Fe-3% Si alloy journal December 1996
Recent developments of non-oriented electrical steel sheets journal September 1984
Influence of plastic strain on magnetic behaviour of non-oriented Fe–3Si and application to manufacturing test by punching journal May 1995
Texture of hot rolled strip for Fe-3Si steel produced by thin slab casting and rolling journal December 2010
The effect of heat treatments and Si contents on B2 ordering reaction in high-silicon steels journal June 2001
Thermomechanical processing of high Si-steel (up to 6.3% Si) journal July 2001
Effects of precipitated phase and order degree on bending properties of an Fe-6.5 wt%Si alloy with columnar grains journal July 2011
Effect of annealing on the microstructure and magnetic properties of soft magnetic Fe-Si produced via laser additive manufacturing journal January 2018
On abnormal growth of Goss grains in grain-oriented silicon steel journal March 2011
On the development of the goss texture in iron-3% silicon journal December 1984
The Eftects of Superheating on Texture and Microstructure of Fe-4.5wt%Si Steel Strip by Twin-roll Strip Casting. journal January 2001
Metallurgy of high-silicon steel parts produced using Selective Laser Melting journal May 2016
Additive manufacturing of anisotropic hybrid NdFeB-SmFeN nylon composite bonded magnets journal December 2018
Study of order-disorder effect on magnetic properties of rapidly quenched Fe-6.5 wt% Si alloys journal February 1989
Additive manufacturing of near-net-shape bonded magnets: Prospects and challenges journal July 2017
Influence of thermal debinding on the final properties of Fe–Si soft magnetic alloys for metal injection molding (MIM) journal October 2016
Ordering–disordering phenomena and micro-hardness characteristics of B2 phase in Fe–(5–6.5%)Si alloys journal October 2005
Frequency dependence of core loss in rapidly quenched Fe‐6.5 wt. %Si journal November 1988