Fullerene-Based In Situ Doping of N and Fe into a 3D Cross-Like Hierarchical Carbon Composite for High-Performance Supercapacitors

Peng, Zhiyao; Hu, Yajing; Wang, Jingjing; Liu, Sijie; Li, Chenxi; Jiang, Qinglong; Lu, Jun; Zeng, Xiaoqiao; Peng, Ping; Li, Fang‐Fang

doi:10.1002/aenm.201802928

Title: Fullerene-Based In Situ Doping of N and Fe into a 3D Cross-Like Hierarchical Carbon Composite for High-Performance Supercapacitors

Journal Article · Mon Feb 04 00:00:00 EST 2019 · Advanced Energy Materials

DOI:https://doi.org/10.1002/aenm.201802928· OSTI ID:1558111

Peng, Zhiyao ^[1]; Hu, Yajing ^[1]; Wang, Jingjing ^[1]; Liu, Sijie ^[1]; Li, Chenxi ^[1]; Jiang, Qinglong ^[2]; Lu, Jun ^[3]; Zeng, Xiaoqiao ^[3]; Peng, Ping ^[1];

^[1]

Huazhong Univ. of Science and Technology, Wuhan (China)
Univ. of Arkansas, Pine Bluff, AR (United States)
Argonne National Lab. (ANL), Lemont, IL (United States)

Fullerene-based carbons are interesting electrode materials for supercapacitors due to their unique carbon structures and tunable architectures at the molecular level. By presenting various functional groups with many elements on the fullerene cages, diverse in situ metal/nonmetal-doped carbon materials with enhanced pseudocapacitances and/or double layer capacitances can be prepared. Here, a fullerene derivative, ferrocenylpyrrolidine C₆₀, containing nitrogen and iron, is chosen as the only precursor. A unique microstructure is fabricated by a liquid-liquid interfacial precipitation process. Subsequently, a facile, one-step annealing of the microstructure at different temperatures is performed. A series of in situ N and Fe-codoped laminated 3D hierarchical carbon composites in the shape of a cross are successfully synthesized. The as-prepared N and Fe-codoped carbon material treated at 700 °C exhibits a high specific capacitance of 505.4 F g^-1 at 0.1 A g^-1. To the best knowledge, this is the highest supercapacitor capacitance based on fullerene electrode materials. The use of a fullerene derivative as an in-situ doped carbon for applications in energy storage opens a new avenue for developing future synthetic strategies to extend the repertoire of electrode materials with high performance.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC); National Natural Science Foundation of China (NSFC)

Grant/Contract Number:: AC02-06CH11357; AC02‐06CH11357

OSTI ID:: 1558111

Alternate ID(s):: OSTI ID: 1493367

Journal Information:: Advanced Energy Materials, Vol. 9, Issue 11; ISSN 1614-6832

Publisher:: WileyCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 87 works

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37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
N and Fe-codoped carbon
fullerenes
hierarchical structures
liquid–liquid interfacial precipitation
supercapacitor

Title: Fullerene-Based In Situ Doping of N and Fe into a 3D Cross-Like Hierarchical Carbon Composite for High-Performance Supercapacitors

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