skip to main content
OSTI.GOV title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Radiation instability of equal channel angular extruded T91 at ultra-high damage levels

Journal Article · · Acta Materialia
 [1];  [1];  [1];  [2]; ORCiD logo [1]
  1. Texas A & M Univ., College Station, TX (United States)
  2. Texas A & M Univ., College Station, TX (United States); Radiation Effects Consulting, Richland, WA (United States)

Although several studies have shown that nano-grained alloys have higher radiation resistance than coarse-grained variants, with dense grain boundary structures acting as defect sinks to remove damage, the present study shows the failure of severe deformation to suppress void swelling in T91 alloy at ultra-high damage levels. Fe self-ion irradiation up to 1000 peak dpa produced significantly more swelling in extruded T91 than conventional T91 at 475 °C. Dramatic radiation-enhanced grain growth was observed in the extruded T91, manifested in two rapid grain growth stages. One stage occurs at a relatively low damage level, and the other at a higher damage level beyond 750 peak dpa. The second rapid growth stage is correlated with void swelling and starts at the end of the swelling incubation period. The study suggests that the defect sink properties of the growing grain boundaries under a coarsening process are different from that of stable boundary configurations. When void swelling becomes significant and voids act as a biased sink for vacancies, the growing grain boundaries act as a biased sink for interstitials, leading to rapid growth at higher damage levels.

Research Organization:
Texas A & M Univ., College Station, TX (United States). Texas A & M Engineering Experiment Station
Sponsoring Organization:
USDOE Office of Nuclear Energy (NE)
Grant/Contract Number:
NE0008297
OSTI ID:
1533475
Alternate ID(s):
OSTI ID: 1550497
Journal Information:
Acta Materialia, Vol. 132, Issue C; ISSN 1359-6454
Publisher:
ElsevierCopyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 26 works
Citation information provided by
Web of Science

References (40)

Microstructural development in reduced activation ferritic alloys irradiated to 200 dpa at 420°C journal September 1994
Length-scale Effects in Cascade Damage Production in Iron journal January 2008
Effect of grain boundary character on sink efficiency journal October 2012
Prediction of swelling of 18Cr10NiTi austenitic steel over a wide range of displacement rates journal April 2010
Compositional and temperature dependence of void swelling in model Fe–Cr base alloys irradiated in the EBR-II fast reactor journal December 2000
Theory and experimental background on dimensional changes in irradiated alloys journal October 1994
Probing grain boundary sink strength at the nanoscale: Energetics and length scales of vacancy and interstitial absorption by grain boundaries in α -Fe journal February 2012
Irradiation creep and swelling of the US fusion heats of HT9 and 9Cr-1Mo to 208 dpa at ~ 400°C journal September 1994
Efficient Annealing of Radiation Damage Near Grain Boundaries via Interstitial Emission journal March 2010
Response of equal channel angular extrusion processed ultrafine-grained T91 steel subjected to high temperature heavy ion irradiation journal August 2014
Recent insights on the swelling and creep of irradiated austenitic alloys journal May 1984
Void-swelling in irons and ferritic steels journal November 1979
Dislocation Models of Crystal Grain Boundaries journal May 1950
Very high swelling and embrittlement observed in a Fe–18Cr–10Ni–Ti hexagonal fuel wrapper irradiated in the BOR-60 fast reactor journal September 2008
Void-swelling in irons and ferritic steels journal November 1979
Bulk nanostructured materials from severe plastic deformation journal March 2000
SANS and TEM of ferritic–martensitic steel T91 irradiated in FFTF up to 184dpa at 413°C journal September 2013
Nanostructuring of metals by severe plastic deformation for advanced properties journal August 2004
Modification of SRIM-calculated dose and injected ion profiles due to sputtering, injected ion buildup and void swelling
  • Wang, Jing; Toloczko, Mychailo B.; Bailey, Nathan
  • Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 387 https://doi.org/10.1016/j.nimb.2016.09.015
journal November 2016
The relationship between grain boundary structure, defect mobility and grain boundary sink efficiency journal March 2015
The microstructure and tensile properties of Fe–Cr alloys after neutron irradiation at 400°C to 5.5–7.1 dpa journal August 1998
The Influence of Grain Boundaries on Radiation-Induced Point Defect Production in Materials: A Review of Atomistic Studies journal January 2013
Irradiation damage of single crystal, coarse-grained, and nanograined copper under helium bombardment at 450 °C journal October 2013
Effect of defect imbalance on void swelling distributions produced in pure iron irradiated with 3.5 MeV self-ions journal October 2014
SRIM – The stopping and range of ions in matter (2010)
  • Ziegler, James F.; Ziegler, M. D.; Biersack, J. P.
  • Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 268, Issue 11-12 https://doi.org/10.1016/j.nimb.2010.02.091
journal June 2010
On the use of SRIM for computing radiation damage exposure journal September 2013
The influence of ion beam rastering on the swelling of self-ion irradiated pure iron at 450 °C journal October 2015
Radiation response of alloy T91 at damage levels up to 1000 peak dpa journal December 2016
Swelling and microstructure of pure Fe and Fe–Cr alloys after neutron irradiation to ∼26dpa at 400°C journal September 2006
Factors which control the swelling of FeCrNi ternary austenitic alloys journal June 1997
Comparison of swelling and irradiation creep behavior of fcc-austenitic and bcc-ferritic/martensitic alloys at high neutron exposure journal January 2000
The process of grain refinement in equal-channel angular pressing journal May 1998
Point defect annihilation at grain boundaries in gold journal April 1985
Microstructural analysis of neutron-irradiated martensitic steels journal June 1996
Irradiation-induced grain growth in nanocrystalline reduced activation ferrite/martensite steel journal September 2014
Microstructural evolution and radiation stability of steels and alloys journal May 1999
Microstructure of 9 Cr-1 MoVNb steel irradiated to 36 dpa at elevated temperatures in HFIR journal May 1984
Grain refinement of T91 alloy by equal channel angular pressing journal May 2009
Effect of self-ion irradiation on the microstructural changes of alloy EK-181 in annealed and severely deformed conditions journal April 2017
Grain boundaries in ultrafine grained materials processed by severe plastic deformation and related phenomena journal April 2012

Similar Records

Radiation response of alloy T91 at damage levels up to 1000 peak dpa
Journal Article · Tue Oct 04 00:00:00 EDT 2016 · Journal of Nuclear Materials · OSTI ID:1533475

Radiation response of alloy T91 at damage levels up to 1000 peak dpa
Journal Article · Thu Dec 01 00:00:00 EST 2016 · Journal of Nuclear Materials · OSTI ID:1533475

From suppressed void growth to significant void swelling in NiCoFeCr complex concentrated solid-solution alloy
Journal Article · Sun Mar 01 00:00:00 EST 2020 · Materialia · OSTI ID:1533475