“Wiring” Fe-Nx-Embedded Porous Carbon Framework onto 1D Nanotubes for Efficient Oxygen Reduction Reaction in Alkaline and Acidic Media

Ahn, Sung Hoon; Yu, Xingwen; Manthiram, Arumugam

doi:10.1002/adma.201606534

“Wiring” Fe-N_x-Embedded Porous Carbon Framework onto 1D Nanotubes for Efficient Oxygen Reduction Reaction in Alkaline and Acidic Media

Journal Article · Mon Apr 24 00:00:00 EDT 2017 · Advanced Materials

DOI:https://doi.org/10.1002/adma.201606534· OSTI ID:1533036

Ahn, Sung Hoon ^[1]; Yu, Xingwen ^[2]; Manthiram, Arumugam ^[2]

Univ. of Texas, Austin, TX (United States). Materials Science and Engineering Program. Texas Materials Inst.; DOE/OSTI
Univ. of Texas, Austin, TX (United States). Materials Science and Engineering Program. Texas Materials Inst.

This study presents a novel metal-organic-framework-engaged synthesis route based on porous tellurium nanotubes as a sacrificial template for hierarchically porous 1D carbon nanotubes. Furthermore, an ultrathin Fe-ion-containing polydopamine layer has been introduced to generate highly effective FeN_xC active sites into the carbon framework and to induce a high degree of graphitization. The synergistic effects between the hierarchically porous 1D carbon structure and the embedded FeN_xC active sites in the carbon framework manifest in superior catalytic activity toward oxygen reduction reaction (ORR) compared to Pt/C catalyst in both alkaline and acidic media. A rechargeable zinc-air battery assembled in a decoupled configuration with the nonprecious pCNT@Fe@GL/CNF ORR electrode and Ni-Fe LDH/NiF oxygen evolution reaction (OER) electrode exhibits charge–discharge overpotentials similar to the counterparts of Pt/C ORR electrode and IrO₂ OER electrode.

View Accepted Manuscript (DOE)

Research Organization:: Univ. of Texas, Austin, TX (United States)

Sponsoring Organization:: USDOE; USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: SC0005397

OSTI ID:: 1533036

Alternate ID(s):: OSTI ID: 1400841

Journal Information:: Advanced Materials, Journal Name: Advanced Materials Journal Issue: 26 Vol. 29; ISSN 0935-9648

Publisher:: WileyCopyright Statement

Country of Publication:: United States

Language:: English

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The Proportion of Fe‐N _X , N Doping Species and Fe ₃ C to Oxygen Catalytic Activity in Core‐Shell Fe‐N/C Electrocatalyst Liu, Yanyan; Zhu, Yihua; Jiang, Hongliang Chemistry – An Asian Journal, Vol. 15, Issue 2 https://doi.org/10.1002/asia.201901571	journal	December 2019
Bottom‐Up Fabrication of a Sandwich‐Like Carbon/Graphene Heterostructure with Built‐In FeNC Dopants as Non‐Noble Electrocatalyst for Oxygen Reduction Reaction Lv, Xiaoxia; Xue, Xue; Gan, Xingyu Chemistry – An Asian Journal, Vol. 15, Issue 3 https://doi.org/10.1002/asia.201901616	journal	December 2019
Recent Advances in Metal‐Organic Framework Derivatives as Oxygen Catalysts for Zinc‐Air Batteries Zhong, Yijun; Xu, Xiaomin; Wang, Wei Batteries & Supercaps, Vol. 2, Issue 4 https://doi.org/10.1002/batt.201800093	journal	November 2018
Structural Advantage Induced by Sulfur to Boost the Catalytic Performance of FeNC Catalyst towards the Oxygen Reduction Reaction Luo, Ergui; Xiao, Meiling; Wang, Yuemin ChemCatChem, Vol. 10, Issue 17 https://doi.org/10.1002/cctc.201800771	journal	July 2018
Facile Synthesis of Fe/N/S‐Doped Carbon Tubes as High‐Performance Cathode and Anode for Microbial Fuel Cells Yang, Wei; Li, Jun; Lan, Linghan ChemCatChem, Vol. 11, Issue 24 https://doi.org/10.1002/cctc.201901084	journal	September 2019
Recent Progress of Carbon-Based Materials in Oxygen Reduction Reaction Catalysis Wang, Yao; Li, Jing; Wei, Zidong ChemElectroChem, Vol. 5, Issue 14 https://doi.org/10.1002/celc.201701335	journal	January 2018
Electrochemical Evidence for Two Sub-families of FeN _x C _y Moieties with Concentration-Dependent Cyanide Poisoning Chung, Min Wook; Chon, Gajeon; Kim, Hyungjun ChemElectroChem, Vol. 5, Issue 14 https://doi.org/10.1002/celc.201800067	journal	March 2018
Synthesis and Active Site Identification of Fe−N−C Single-Atom Catalysts for the Oxygen Reduction Reaction Wan, Xin; Chen, Weiqi; Yang, Jiarui ChemElectroChem, Vol. 6, Issue 2 https://doi.org/10.1002/celc.201801302	journal	November 2018
Bimetal/Metal Oxide Encapsulated in Graphitic Nitrogen Doped Mesoporous Carbon Networks for Enhanced Oxygen Electrocatalysis Jose, Vishal; Jayakumar, Anjali; Lee, Jong‐Min ChemElectroChem, Vol. 6, Issue 5 https://doi.org/10.1002/celc.201801508	journal	January 2019
In Situ Synthesis and Electrocatalytic Performance of Fe/Fe _2.5 C/Fe ₃ N/Nitrogen‐Doped Carbon Nanotubes for the Oxygen Reduction Reaction Yan, Ping; Kong, Dewang; Yuan, Wenjing ChemElectroChem, Vol. 6, Issue 12 https://doi.org/10.1002/celc.201900716	journal	May 2019
Thermal Conversion of MOF@MOF: Synthesis of an N-Doped Carbon Material with Excellent ORR Performance Zhang, Mengxin; Wu, Dan; Ye, Yingxiang ChemPlusChem, Vol. 83, Issue 11 https://doi.org/10.1002/cplu.201800392	journal	October 2018
Freestanding 1D Hierarchical Porous Fe‐N‐Doped Carbon Nanofibers as Efficient Oxygen Reduction Catalysts for Zn–Air Batteries Wu, Mengchen; Li, Congling; Liu, Rui Energy Technology, Vol. 7, Issue 3 https://doi.org/10.1002/ente.201800790	journal	March 2019
Pearl Necklace Fibrous Carbon Sharing Fe–N/Fe–P Dual Active Sites as Efficient Oxygen Reduction Catalyst in Broad Media and for Liquid/Solid‐State Rechargeable Zn–Air Battery Wu, Mengchen; Liu, Rui Energy Technology, Vol. 8, Issue 3 https://doi.org/10.1002/ente.201901263	journal	December 2019
Pearl Necklace Fibrous Carbon Sharing Fe–N/Fe–P Dual Active Sites as Efficient Oxygen Reduction Catalyst in Broad Media and for Liquid/Solid‐State Rechargeable Zn–Air Battery Wu, Mengchen; Liu, Rui Energy Technology, Vol. 8, Issue 3 https://doi.org/10.1002/ente.202070034	journal	December 2019
ZIF-8/ZIF-67-Derived Co-N _x -Embedded 1D Porous Carbon Nanofibers with Graphitic Carbon-Encased Co Nanoparticles as an Efficient Bifunctional Electrocatalyst Zhang, Wenming; Yao, Xiuyun; Zhou, Shengnan Small, Vol. 14, Issue 24 https://doi.org/10.1002/smll.201800423	journal	May 2018
Atomic‐Level Fe‐N‐C Coupled with Fe ₃ C‐Fe Nanocomposites in Carbon Matrixes as High‐Efficiency Bifunctional Oxygen Catalysts Sun, Xueping; Wei, Peng; Gu, Songqi Small, Vol. 16, Issue 6 https://doi.org/10.1002/smll.201906057	journal	December 2019
Recent Progress in Oxygen Electrocatalysts for Zinc-Air Batteries Yang, Dongjiang; Zhang, Lijie; Yan, Xuecheng Small Methods, Vol. 1, Issue 12 https://doi.org/10.1002/smtd.201700209	journal	November 2017
Cobalt@Nitrogen‐Doped Porous Carbon Fiber Derived from the Electrospun Fiber of Bimetal–Organic Framework for Highly Active Oxygen Reduction Bai, Qing; Shen, Feng‐Cui; Li, Shun‐Li Small Methods, Vol. 2, Issue 12 https://doi.org/10.1002/smtd.201800049	journal	May 2018
Nitrogen‐Doped Porous Carbon Supported Nonprecious Metal Single‐Atom Electrocatalysts: from Synthesis to Application Guo, Jiaojiao; Huo, Juanjuan; Liu, Yan Small Methods, Vol. 3, Issue 9 https://doi.org/10.1002/smtd.201900159	journal	May 2019
Rational Microstructure Design on Metal–Organic Framework Composites for Better Electrochemical Performances: Design Principle, Synthetic Strategy, and Promotion Mechanism Li, Zhaoqiang; Ge, Xiaoli; Li, Caixia Small Methods, Vol. 4, Issue 3 https://doi.org/10.1002/smtd.201900756	journal	January 2020
β-Mo2C/N, P-co-doped carbon as highly efficient catalyst for hydrogen evolution reaction Tan, Jiabin; He, Xiaobo; Yin, Fengxiang Journal of Materials Science, Vol. 54, Issue 6 https://doi.org/10.1007/s10853-018-03190-0	journal	December 2018
Strategies for Enhancing the Electrocatalytic Activity of M–N/C Catalysts for the Oxygen Reduction Reaction Sa, Young Jin; Woo, Jinwoo; Joo, Sang Hoon Topics in Catalysis, Vol. 61, Issue 9-11 https://doi.org/10.1007/s11244-018-0935-0	journal	May 2018
Recent advances in active sites identification and regulation of M-N/C electro-catalysts towards ORR Liu, Jie; Jin, Zhao; Wang, Xian Science China Chemistry, Vol. 62, Issue 6 https://doi.org/10.1007/s11426-018-9425-5	journal	March 2019
Metal organic frameworks derived single atom catalysts for electrocatalytic energy conversion Sun, Tingting; Xu, Lianbin; Wang, Dingsheng Nano Research, Vol. 12, Issue 9 https://doi.org/10.1007/s12274-019-2345-4	journal	March 2019
Oxygen Reduction Reactions of Fe-N-C Catalysts: Current Status and the Way Forward Shen, Hangjia; Thomas, Tiju; Rasaki, Sefiu Abolaji Electrochemical Energy Reviews, Vol. 2, Issue 2 https://doi.org/10.1007/s41918-019-00030-w	journal	March 2019
Identifying the structure of Zn-N2 active sites and structural activation Li, Feng; Bu, Yunfei; Han, Gao-Feng Nature Communications, Vol. 10, Issue 1 https://doi.org/10.1038/s41467-019-10622-1	journal	June 2019
In situ synthesis of ultrathin metal–organic framework nanosheets: a new method for 2D metal-based nanoporous carbon electrocatalysts Huang, Liang; Zhang, Xueping; Han, Yujie Journal of Materials Chemistry A, Vol. 5, Issue 35 https://doi.org/10.1039/c7ta05821g	journal	January 2017
Co,N-codoped nanotube/graphene 1D/2D heterostructure for efficient oxygen reduction and hydrogen evolution reactions Yang, Liu; Lv, Yanlong; Cao, Dapeng Journal of Materials Chemistry A, Vol. 6, Issue 9 https://doi.org/10.1039/c7ta11140a	journal	January 2018
In situ synthesis of nitrogen doped carbon with embedded Co@Co ₃ O ₄ nanoparticles as a bifunctional electrocatalyst for oxygen reduction and oxygen evolution reactions Wang, Ying; Hu, Tianjun; Qiao, Yanting Chemical Communications, Vol. 54, Issue 90 https://doi.org/10.1039/c8cc07956k	journal	January 2018
Creation of oxygen reduction reaction active sites on titanium oxynitride without increasing the nitrogen doping level Chisaka, Mitsuharu Physical Chemistry Chemical Physics, Vol. 20, Issue 23 https://doi.org/10.1039/c8cp01420e	journal	January 2018
Fe(CN) ₅ @PIL-derived N-doped porous carbon with FeC _x N _y active sites as a robust electrocatalyst for the oxygen reduction reaction Zhang, Shao-hua; Gao, Yi-jing; Cheng, Shan Catalysis Science & Technology, Vol. 9, Issue 1 https://doi.org/10.1039/c8cy01694a	journal	January 2019
Phosphor and nitrogen co-doped rutile TiO ₂ covered on TiN for oxygen reduction reaction in acidic media Chisaka, Mitsuharu; Morioka, Hiroyuki Catalysis Science & Technology, Vol. 9, Issue 3 https://doi.org/10.1039/c8cy01973h	journal	January 2019
A coordination polymer-derived Co ₃ O ₄ /Co–N@NMC composite material as a Zn–air battery cathode electrocatalyst and microwave absorber Wang, Yaqin; Xu, Xinxin; Liu, Luyao Dalton Transactions, Vol. 48, Issue 21 https://doi.org/10.1039/c8dt03792b	journal	January 2019
Electronic structure engineering to boost oxygen reduction activity by controlling the coordination of the central metal Han, Yunhu; Wang, Yanggang; Xu, Ruirui Energy & Environmental Science, Vol. 11, Issue 9 https://doi.org/10.1039/c8ee01481g	journal	January 2018
Unveiling dual-linkage 3D hexaiminobenzene metal–organic frameworks towards long-lasting advanced reversible Zn–air batteries Shinde, Sambhaji S.; Lee, Chi Ho; Jung, Jin-Young Energy & Environmental Science, Vol. 12, Issue 2 https://doi.org/10.1039/c8ee02679c	journal	January 2019
Iron-decorated nitrogen-rich carbons as efficient oxygen reduction electrocatalysts for Zn–air batteries Liu, Zhuang; Liu, Jing; Wu, Hao Bin Nanoscale, Vol. 10, Issue 36 https://doi.org/10.1039/c8nr04627a	journal	January 2018
Efficient ORR electrocatalytic activity of peanut shell-based graphitic carbon microstructures Wu, Yanling; Chen, Yanli; Wang, Huiqiu Journal of Materials Chemistry A, Vol. 6, Issue 25 https://doi.org/10.1039/c8ta02839g	journal	January 2018
Polydopamine-inspired nanomaterials for energy conversion and storage Qu, Konggang; Wang, Yinghua; Vasileff, Anthony Journal of Materials Chemistry A, Vol. 6, Issue 44 https://doi.org/10.1039/c8ta05245j	journal	January 2018
A eutectic salt-assisted semi-closed pyrolysis route to fabricate high-density active-site hierarchically porous Fe/N/C catalysts for the oxygen reduction reaction Li, Jia; Chen, Siguo; Li, Wei Journal of Materials Chemistry A, Vol. 6, Issue 32 https://doi.org/10.1039/c8ta05419c	journal	January 2018
Hierarchical 3D macrosheets composed of interconnected in situ cobalt catalyzed nitrogen doped carbon nanotubes as superior bifunctional oxygen electrocatalysts for rechargeable Zn–air batteries Li, Yapeng; Gao, Jingyu; Zhang, Fu Journal of Materials Chemistry A, Vol. 6, Issue 32 https://doi.org/10.1039/c8ta06057f	journal	January 2018
Mesoporous CoO/Co–N–C nanofibers as efficient cathode catalysts for Li–O ₂ batteries He, Biao; Wang, Jun; Fan, Yuqi Journal of Materials Chemistry A, Vol. 6, Issue 39 https://doi.org/10.1039/c8ta07185c	journal	January 2018
In situ derived Fe/N/S-codoped carbon nanotubes from ZIF-8 crystals as efficient electrocatalysts for the oxygen reduction reaction and zinc–air batteries Jin, Huihui; Zhou, Huang; Li, Wenqiang Journal of Materials Chemistry A, Vol. 6, Issue 41 https://doi.org/10.1039/c8ta07849a	journal	January 2018
One-pot synthesis of Fe/N/S-doped porous carbon nanotubes for efficient oxygen reduction reaction Tan, Zhong; Li, Huanxin; Feng, Qiaoxia Journal of Materials Chemistry A, Vol. 7, Issue 4 https://doi.org/10.1039/c8ta09589b	journal	January 2019
Atomically dispersed metal catalysts for the oxygen reduction reaction: synthesis, characterization, reaction mechanisms and electrochemical energy applications Liu, Minmin; Wang, Linlin; Zhao, Kangning Energy & Environmental Science, Vol. 12, Issue 10 https://doi.org/10.1039/c9ee01722d	journal	January 2019
β-Cyclodextrin-based hollow nanoparticles with excellent adsorption performance towards organic and inorganic pollutants Liu, Yinli; Liu, Miao; Jia, Jie Nanoscale, Vol. 11, Issue 40 https://doi.org/10.1039/c9nr07342f	journal	January 2019
Size-dependence of the electrochemical performance of Fe–N–C catalysts for the oxygen reduction reaction and cathodes of direct methanol fuel cells Xu, Xinlong; Xia, Zhangxun; Zhang, Xiaoming Nanoscale, Vol. 12, Issue 5 https://doi.org/10.1039/c9nr08458d	journal	January 2020
Bimetallic ZIF derived Co nanoparticle anchored N-doped porous carbons for an efficient oxygen reduction reaction Li, Kaili; Li, Daohao; Zhu, Liangkui Inorganic Chemistry Frontiers, Vol. 7, Issue 4 https://doi.org/10.1039/c9qi01487j	journal	January 2020
g-C ₃ N ₄ templated synthesis of the Fe ₃ C@NSC electrocatalyst enriched with Fe–N _x active sites for efficient oxygen reduction reaction Eissa, Ahmed A.; Peera, Shaik Gouse; Kim, Nam Hoon Journal of Materials Chemistry A, Vol. 7, Issue 28 https://doi.org/10.1039/c9ta01837a	journal	January 2019
Mechanochemical synthesis of multi-site electrocatalysts as bifunctional zinc–air battery electrodes Guo, Beibei; Ju, Qiangjian; Ma, Ruguang Journal of Materials Chemistry A, Vol. 7, Issue 33 https://doi.org/10.1039/c9ta06411g	journal	January 2019
A flexible non-precious metal Fe-N/C catalyst for highly efficient oxygen reduction reaction He, Xinping; Xia, Yang; Liang, Chu Nanotechnology, Vol. 30, Issue 14 https://doi.org/10.1088/1361-6528/aafc7c	journal	February 2019
Core-Shell Polydopamine@Zr-Hemin MOFs Derived Fe-N-Doped Porous Carbon Nanospheres Electrocatalysts for the Oxygen Reduction Wang, Yinling; Wang, Juan; Zhang, Youliang Journal of The Electrochemical Society, Vol. 165, Issue 10 https://doi.org/10.1149/2.1101810jes	journal	January 2018

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1D nanotubes
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