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Title: Microwave-assisted synthesis of carbon and carbon-metal composites from lignin, tannin and asphalt derivatives

Patent ·
OSTI ID:1531731

A process for synthesizing carbon-metal nanocomposites. In one embodiment, the process includes the steps of preparing a metal derivative or a metal chelated derivative of a carbon-containing precursor in solid form, and subjecting the metal derivative or metal chelated derivative of a carbon-containing precursor in solid form to microwave radiation at a frequency in the range of 900 MHz to 5.8 GHz, for a period of time effective to generate a heat flow from inside of the metal derivative or metal chelated derivative of a carbon-containing precursor in solid form to the outside such that the temperature of the metal derivative or metal chelated derivative of a carbon-containing precursor in solid form reaches 1,000° C. in less than 6 minutes with a temperature (T) derivative over time (t), ΔT/Δt, no less than 2.5° C./second to form carbon-metal nanocomposites.

Research Organization:
Univ. of Arkansas, Little Rock, AR (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
FG36-06GO86072
Assignee:
Board of Trustees of the University of Arkansas (Little Rock, AR)
Patent Number(s):
8,167,973
Application Number:
12/487,174
OSTI ID:
1531731
Resource Relation:
Patent File Date: 2009-06-18
Country of Publication:
United States
Language:
English

References (11)

A synergistic assembly of nanoscale lamellar photoconductor hybrids journal December 2008
Method and apparatus for synthesizing diamond, electrode for diamond synthesis, and method for manufacturing the electrode patent-application August 2005
Carbon electrode material for electrochemical cells and method of making same patent October 1999
Sulfonated aromatic copolyesters containing hydroxyalkanoic acid groups and shaped articles produced therefrom patent April 2008
A Novel Carbothermal Method for the Preparation of Nano-sized WC on High Surface Area Carbon journal October 2006
Polymeric nanocomposites comprising epoxy-functionalized graft polymer patent May 2007
Carbon electrode material for electrochemical cells and method of making same patent August 2000
Ferromagnetic conducting lignosulfonic acid-doped polyaniline nanocomposites patent July 2004
Manufacturing method of a thin film on a substrate patent November 2002
High volume production of nanostructured materials patent-application November 2007
Negative Active Material Including Metal Nanocrystal Composite, Method Of Preparing The Same, And Anode And Lithium Battery Including The Negative Active Material patent-application November 2007

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