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Title: Design, characterization, and performance of a hard x-ray transmission microscope at the National Synchrotron Light Source II 18-ID beamline

Journal Article · · Review of Scientific Instruments
DOI:https://doi.org/10.1063/1.5088124· OSTI ID:1524554

A transmission X-ray microscope (TXM) has been designed and commissioned at the 18-ID Fullfield X-ray Imaging (FXI) beamline at the National Synchrotron Light Source-II (NSLS-II). This instrument operates in the 5-11 keV range, and, with the current set of optics, is capable of 30 nm spatial resolution imaging, with a field of view (FOV) of about 40 microns. For absorption contrast, the minimum exposure time for a single projection image is about 20 ms and an entire 3D tomography data set can be acquired in under one minute. The system enables tomographic reconstructions with sub-50 nm spatial resolution without the use of markers on the sample or corrections for rotation run-outs.

Research Organization:
Brookhaven National Laboratory (BNL), Upton, NY (United States)
Sponsoring Organization:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
Grant/Contract Number:
SC0012704
OSTI ID:
1524554
Alternate ID(s):
OSTI ID: 1511070
Report Number(s):
BNL-211719-2019-JAAM
Journal Information:
Review of Scientific Instruments, Vol. 90, Issue 5; ISSN 0034-6748
Publisher:
American Institute of Physics (AIP)Copyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 15 works
Citation information provided by
Web of Science

References (13)

Design and performance of an X-ray scanning microscope at the Hard X-ray Nanoprobe beamline of NSLS-II journal October 2017
Oxygen Release Induced Chemomechanical Breakdown of Layered Cathode Materials journal April 2018
Full-field transmission x-ray microscopy at SSRL journal September 2009
Design and performance of a scanning ptychography microscope journal March 2014
Hard X-ray Microscopy with sub 30 nm Spatial Resolution
  • Tang, Mau-Tsu; Song, Yen-Fang; Yin, Gung-Chian
  • SYNCHROTRON RADIATION INSTRUMENTATION: Ninth International Conference on Synchrotron Radiation Instrumentation, AIP Conference Proceedings https://doi.org/10.1063/1.2436296
conference January 2007
Hard X-ray nanotomography beamline 7C XNI at PLS-II journal May 2014
Lifetime of the solar nebula constrained by meteorite paleomagnetism journal February 2017
One-minute nano-tomography using hard X-ray full-field transmission microscope journal August 2018
Automated markerless full field hard x-ray microscopic tomography at sub-50 nm 3-dimension spatial resolution journal April 2012
A high-precision instrument for mapping of rotational errors in rotary stages journal October 2014
FXI: a full-field imaging beamline at NSLS-II conference September 2015
Performance and characterization of the prototype nm-scale spatial resolution scanning multilayer Laue lenses microscope journal March 2013
Heterogeneous silicon mesostructures for lipid-supported bioelectric interfaces journal June 2016

Cited By (5)

Cooling Induced Surface Reconstruction during Synthesis of High‐Ni Layered Oxides journal October 2019
Anisotropically Electrochemical–Mechanical Evolution in Solid‐State Batteries and Interfacial Tailored Strategy journal November 2019
Anisotropically Electrochemical–Mechanical Evolution in Solid‐State Batteries and Interfacial Tailored Strategy journal November 2019
Stability investigation of a cryo soft x-ray microscope by fiber interferometry journal February 2020
Distributed optimization for nonrigid nano-tomography text January 2020

Figures / Tables (13)


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