Skip to main content
U.S. Department of Energy
Office of Scientific and Technical Information

Time-of-Flight Neutron Diffraction (TOF-ND) Analyses of the Composition and Minting of Ancient Judaean “Biblical” Coins

Journal Article · · Journal of Analytical Methods in Chemistry
DOI:https://doi.org/10.1155/2019/6164058· OSTI ID:1509546
TOF-ND elastic scattering of thermal neutrons offers some important advantages over X-ray diffraction (XRD), X-ray fluorescence (XRF), and metallography for the study of archaeological and numismatic problems. Traditional analytical methods are usually destructive and often probe only the surface. Neutrons deeply penetrate samples, simultaneously giving nondestructive bulk information about the crystal structure, composition, and texture (alignment of crystallites) from which thermomechanical manufacturing processes (e.g., cast, struck, or rolled) may be inferred. An analysis of the metal composition and minting processes used for making ancient Judaean bronze and leaded bronze coins from first century BCE and CE is used as a case study. One of the first ND analyses of the temperature used for striking bronze coins is also presented.
Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Organization:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)
Grant/Contract Number:
AC05-00OR22725
OSTI ID:
1509546
Journal Information:
Journal of Analytical Methods in Chemistry, Journal Name: Journal of Analytical Methods in Chemistry Journal Issue: N/A Vol. 2019; ISSN 2090-8865
Publisher:
HindawiCopyright Statement
Country of Publication:
United States
Language:
English

References (51)

Non-destructive Phase Analysis of Archaeological Ceramics using TOF Neutron Diffraction journal February 2001
Applications of TOF neutron diffraction in archaeometry journal March 2006
Crystallographic texture analysis of archaeological metals: interpretation of manufacturing techniques journal August 2007
Characterization of bronze Roman coins of the fifth century called nummi through different analytical techniques journal May 2013
Quantitative multiphase analysis of archaeological bronzes by neutron diffraction journal December 2002
Evaluation of segregation in Roman sestertius coins journal October 2017
Effect of Strain Rate on Evolution of the Deformation Microstructure and Texture in Polycrystalline Copper and Nickel journal July 2010
Strain hardening regimes and microstructural evolution during large strain compression of low stacking fault energy fcc alloys that form deformation twins journal September 1997
“Biblical” bronze coins: new insights into their timing and attribution using copper and lead isotopes journal December 2012
The Cu–Sn phase diagram, Part I: New experimental results journal March 2013
Preliminary neutron diffraction study of two fenestrated axes from the ‘Enot Shuni' Bronze Age cemetery (Israel) journal December 2009
Neutron diffraction analyses of Bronze Age swords from the Alpine region: Benchmarking neutron diffraction against laboratory methods journal August 2018
A multi-technique investigation of the incuse coinage of Magna Graecia journal August 2018
Non-invasive in-situ analysis of a wreath of gold leaves from the National Archaeological Museum of Taranto, Italy journal October 2018
New insights into the manufacturing technique and corrosion of high leaded antique bronze coins journal May 2016
Portable EDXRF investigation of the patinas on the Riace Bronzes
  • Buccolieri, Giovanni; Buccolieri, Alessandro; Donati, Paola
  • Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 343 https://doi.org/10.1016/j.nimb.2014.11.064
journal January 2015
VULCAN—The engineering diffractometer at the SNS journal November 2006
Modeling the Mechanical Behavior of Dynamically Deformed Cu using the Theories of Crystal Plasticity journal January 2017
Texture analysis of ancient coins with TOF neutron diffraction journal May 2004
Integrated X-ray and neutron-based analysis of bronze artefacts from the Ligurian settlement of Guardamonte-Monte Vallassa journal January 2011
PIND: High spatial resolution by pinhole neutron diffraction journal June 2018
Texture formation in metal alloys with cubic crystal structures journal January 2016
FCC Rolling Textures Reviewed in the Light of Quantitative Comparisons between Simulated and Experimental Textures journal June 2014
Neutron scattering material analysis of Bronze Age metal artefacts journal February 2008
Texture of Metals journal January 1974
Pontius Pilate — An Aqueduct Builder? — Recent Findings and New Suggestions journal January 2000
First In Situ Lattice Strains Measurements Under Load at VULCAN journal October 2010
Texture Evolution and Phase Transformation in Titanium Investigated by In-Situ Neutron Diffraction journal March 2011
In-situ residual stress analysis during annealing treatments using neutron diffraction in combination with a novel furnace design journal November 2016
Compositional and microstructural characterization of Celtic silver coins from northern Italy using neutron diffraction analysis journal May 2016
The lattice parameter of α-bronzes as a function of solute content: application to archaeological materials journal February 2005
Texture analysis of ancient coins with TOF neutron diffraction journal May 2004
Casting technology of Renaissance bronze statuettes: the use of TOF-neutron diffraction for studying afterwork of Renaissance casting techniques journal January 2011
From Koto age to modern times: Quantitative characterization of Japanese swords with Time of Flight Neutron Diffraction journal January 2011
New insights into alloy compositions: studying Renaissance bronze statuettes by combined neutron imaging and neutron diffraction techniques journal January 2011
Integrated X-ray and neutron-based analysis of bronze artefacts from the Ligurian settlement of Guardamonte-Monte Vallassa journal January 2011
A suite-level review of the neutron powder diffraction instruments at Oak Ridge National Laboratory journal September 2018
Neutron scattering lengths and cross sections journal January 1992
Micro-mechanical aspects of texture evolution in nickel and nickel–cobalt alloys: role of stacking fault energy journal September 2016
Texture and anisotropy journal July 2004
EXPGUI , a graphical user interface for GSAS journal April 2001
A profile refinement method for nuclear and magnetic structures journal June 1969
Extracting grain-orientation-dependent data from in situ time-of-flight neutron diffraction. I. Inverse pole figures journal November 2014
A Second Investigation into the Chemical Composition of the Roman Provincial (Procuratorial) Coinage of Judaea, AD 6-66* journal February 2003
MC-ICP-MS analyses of tin isotopes in Roman-era bronze coins reveal temporal and spatial variation: MC-ICP-MS analyses of tin isotopes in Roman-era bronze coins journal January 2019
Non-Destructive Investigation of Bronze Artefacts from the Marches National Museum of Archaeology Using Neutron Diffraction* journal January 2006
NON-DESTRUCTIVE CHEMICAL ANALYSIS OF OLD SOUTH ARABIAN COINS, FOURTH CENTURY BCE TO THIRD CENTURY CE: Non-destructive chemical analysis of Old South Arabian coins journal April 2011
Preferred orientations in cast metals journal May 2005
Chemical Attribution of Corroded Coins Using X-ray Fluorescence and Lead Isotope Ratios: A Case Study from First Century Judaea journal April 2010
The Tax Law of Palmyra: Evidence for Economic History in a City of the Roman East journal November 1984
Metallurgical and Technological Investigation on Augustean Auxiliary Coins from Thraco-Moesia journal April 2011

Similar Records

Microscopical Examination of Ancient Silver Coins
Journal Article · Mon Apr 23 00:00:00 EDT 2007 · AIP Conference Proceedings · OSTI ID:21057285

Neutron tomographic analysis: Material characterization of silver and electrum coins from the 6th and 5th centuries BCE
Journal Article · Mon Aug 15 00:00:00 EDT 2016 · Materials Characterization · OSTI ID:22689578

Gold Provenance Studies for Romanian Archaeological Objects Using Micro-SR-XRF
Journal Article · Tue Apr 06 00:00:00 EDT 2010 · AIP Conference Proceedings · OSTI ID:21371752

Related Subjects