Boehmite and Gibbsite Nanoplates for the Synthesis of Advanced Alumina Products

Zhang, Xin; Huestis, Patricia L.; Pearce, Carolyn I.; Hu, Jian Zhi; Page, Katharine; Anovitz, Lawrence M.; Aleksandrov, Alexandr B.; Prange, Micah P.; Kerisit, Sebastien; Bowden, Mark E.; Cui, Wenwen; Wang, Zheming; Jaegers, Nicholas R.; Graham, Trent R.; Dembowski, Mateusz; Wang, Hsiu-Wen; Liu, Jue; N’Diaye, Alpha T.; Bleuel, Markus; Mildner, David F.  R.; Orlando, Thomas M.; Kimmel, Greg A.; La Verne, Jay A.; Clark, Sue B.; Rosso, Kevin M.

doi:10.1021/acsanm.8b01969

Boehmite and Gibbsite Nanoplates for the Synthesis of Advanced Alumina Products

Journal Article · Tue Nov 13 23:00:00 EST 2018 · ACS Applied Nano Materials

DOI:https://doi.org/10.1021/acsanm.8b01969· OSTI ID:1508137

^[1]; Huestis, Patricia L. ^[2]; ^[1]; ^[1]; ^[3]; ^[3]; Aleksandrov, Alexandr B. ^[4]; Prange, Micah P. ^[1]; ^[1]; Bowden, Mark E. ^[1]; Cui, Wenwen ^[1]; Wang, Zheming ^[1]; ^[1]; ; Dembowski, Mateusz ^[1]; ^[3]; ^[3]; N’Diaye, Alpha T. ^[5]; Bleuel, Markus ^[6]; Mildner, David F. R. ^[6] more »

Pacific Northwest National Laboratory, Richland, Washington 99354, United States
Radiation Laboratory and Department of Physics, University of Notre Dame, Notre Dame, Indiana 46556, United States
Oak Ridge National Laboratory, Oak Ridge, Tennessee 37830, United States
School of Chemistry and Biochemistry, Georgia Institute of Technology, Atlanta, Georgia 30332, United States
Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720, United States
National Institute of Standards and Technology, Gaithersburg, Maryland 20899, United States

Boehmite (?-AlOOH) and gibbsite (a-Al(OH)3) are important archetype (oxy)hydroxides of aluminum in nature that also play diverse roles across a plethora of industrial applications. Developing the ability to understand and predict the properties and characteristics of these materials, on the basis of their natural growth or synthesis pathways, is an important fundamental science enterprise with wide ranging impacts. The present study describes bulk and surface characteristics of these novel materials in comprehensive detail, using a collectively-sophisticated set of experimental capabilities, including a range of conventional laboratory solids analyses and national user facility analyses such as synchrotron X-ray absorption and scattering spectroscopies, as well as small angle neutron scattering. Their thermal stability is investigated using in situ temperature-dependent Raman spectroscopy. These pure and effectively defect-free materials are ideal for synthesis of advanced alumina products.

Research Organization:: Energy Frontier Research Centers (EFRC) (United States). Interfacial Dynamics in Radioactive Environments and Materials (IDREAM); Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)

DOE Contract Number:: AC05-76RL01830

OSTI ID:: 1508137

Report Number(s):: PNNL-SA-139693

Journal Information:: ACS Applied Nano Materials, Journal Name: ACS Applied Nano Materials Journal Issue: 12 Vol. 1; ISSN 2574-0970

Publisher:: American Chemical Society (ACS)

Country of Publication:: United States

Language:: English

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