Synthesis of Hierarchical Titanium Carbide from Titania-Coated Cellulose Paper
An aqueous-based, inexpensive, TiO2 precursor, Tyzor-LA, and cellulose paper have been used to prepare TiC via carbothermal reduction in an Ar flow. The hierarchical cellulose structures were also completely maintained through the agglomeration of 10-50nm TiC nanoparticles, and the lattice parameter of TiC increased with the increase of reaction temperature, while the oxygen content in the sample decreased (0.24wt% at 1500 C).
- Research Organization:
- Pacific Northwest National Lab., Richland, WA (US), Environmental Molecular Sciences Laboratory (US)
- Sponsoring Organization:
- US Department of Energy (US)
- DOE Contract Number:
- AC05-76RL01830
- OSTI ID:
- 15009999
- Report Number(s):
- PNNL-SA-41057; 5107a; KC0201050; TRN: US200433%%416
- Journal Information:
- Advanced Materials, Vol. 16, Issue 14; Other Information: PBD: 19 Jul 2004
- Country of Publication:
- United States
- Language:
- English
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