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Observation of the shock-induced β-Sn to b.c.t.-Sn transition using time-resolved X-ray diffraction

Journal Article · · Journal of Synchrotron Radiation (Online)
 [1];  [2];  [3];  [3];  [3];  [2];  [2]
  1. European Synchrotron Radiation Facility (ESRF), Grenoble (France); Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
  2. European Synchrotron Radiation Facility (ESRF), Grenoble (France)
  3. Alternative Energies and Atomic Energy Commission (CEA), Arpajon (France)
+ Show Author Affiliations
Time-resolved X-ray diffraction measurements have been carried out here on dynamically compressed Sn up to a maximum pressure of ~13 GPa at the European Synchrotron Radiation Facility. The phase transition from β-Sn to body-centered tetragonal (b.c.t.) Sn has been observed using synchrotron X-ray diffraction for the first time undergoing shock compression and release. Following maximum compression, the sample releases to lower pressures for several nanoseconds until the reverse transition occurs. The data are in good agreement with previous shock boundaries that indicate that the β-Sn phase is stable ~2 GPa higher than the static boundary upon compression and the b.c.t.-Sn phase is stable ~1 GPa lower upon release. The transition to the high-pressure phase reveals a loss of texture in the X-ray diffraction data from the `quasi' single-crystal β-Sn structure to a more powder-like Debye–Scherrer ring.
Research Organization:
European Synchrotron Radiation Facility (ESRF), Grenoble (France); Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
Sponsoring Organization:
European Union (EU); USDOE National Nuclear Security Administration (NNSA)
Grant/Contract Number:
AC52-07NA27344
OSTI ID:
1497280
Alternate ID(s):
OSTI ID: 23079288
Report Number(s):
LLNL-JRNL--747397; 931131
Journal Information:
Journal of Synchrotron Radiation (Online), Journal Name: Journal of Synchrotron Radiation (Online) Journal Issue: 1 Vol. 26; ISSN 1600-5775
Publisher:
International Union of CrystallographyCopyright Statement
Country of Publication:
United States
Language:
English

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Cited By (2)

Kinetics and structural changes in dynamically compressed bismuth journal August 2019
Picosecond pump–probe X-ray scattering at the Elettra SAXS beamline journal January 2020

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Related Subjects

36 MATERIALS SCIENCE
phase boundaries
shock compression
time-resolved X-ray diffraction