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Influence of Alloying on α-α' Phase Separation in Duplex Stainless Steels

Conference ·
Thermal embrittlement caused by phase transformations in the temperature range of 204–538 °C limits the service temperature of duplex stainless steels. The present study investigates a set of wrought (2003, 2101, and 2205) and weld (2209-w and 2101-w) alloys in order to better understand how alloying elements affect thermal embrittlement. Samples were aged at 427 °C for up to 10,000 h. The embrittlement and thermal instability were assessed via nanoindentation, impact toughness testing, and atom probe tomography (APT). Results demonstrate that the spinodal amplitude is not an accurate predictor of mechanical degradation, and that nanoindentation within the ferrite grains served as a reasonable approximate for the embrittlement behavior. Compositionally, alloys with a lower concentration of Cr, Mo, and Ni were found to exhibit superior mechanical properties following aging.
Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC05-00OR22725
OSTI ID:
1495985
Country of Publication:
United States
Language:
English

References (7)

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Quantitative Evaluation of Spinodal Decomposition in Fe-Cr by Atom Probe Tomography and Radial Distribution Function Analysis journal May 2013
An atom probe perspective on phase separation and precipitation in duplex stainless steels journal May 2016
Phase Separation in Lean-Grade Duplex Stainless Steel 2101 journal August 2015
Duplex stainless steels, a review after DSS'07 in Grado journal March 2008
Atom Probe Studies of the Fe–Cr System and Stainless Steels Aged at Intermediate Temperature journal January 2000
Annealing induced recovery of long-term thermal aging embrittlement in a duplex stainless steel journal March 2013

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