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Ambient and High-Temperature Bulk Characterization of Additively Manufactured Ti-6Al-4V Using Neutron Diffraction

Journal Article · · JOM. Journal of the Minerals, Metals & Materials Society
 [1];  [2];  [1];  [3];  [3];  [4];  [4]
  1. Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
  2. Los Alamos National Lab. (LANL), Los Alamos, NM (United States); JFE Steel Corporation, Kurashiki (Japan)
  3. Nuclear Research Center Negev, Beer-Sheva (Israel). Physics Dept.
  4. Nuclear Research Center Negev, Beer-Sheva (Israel). Materials Engineering Dept.; Rotem Industries Ltd, Mishor Yamin (Israel)
Characterization of the bulk microstructure using neutron diffraction has been applied to investigate the phase fractions and textures of α- and β-phases in Ti-6Al-4V fabricated by additive manufacturing. The microstructure of a specimen cut from a fan structure, built by either electron beam melting (EBM) or selective laser melting, indicated that predominantly the build direction and not the fan angle determines the microstructure. In situ heating experiments of specimens from a rod built using EBM provided insight into the lattice strain, phase fraction, and texture evolution, providing a rich picture of the microstructure changes during heat treatment of additively manufactured Ti-6Al-4V. Finally, a remarkably low weight fraction of β-phase at lower temperatures, deviations from thermal expansion behavior attributed to vanadium repartitioning, as well as texture strengthening were observed.
Research Organization:
Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)
Sponsoring Organization:
Israel Ministry of Science, Technology and Space; USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)
Grant/Contract Number:
89233218CNA000001; AC52-06NA25396
OSTI ID:
1483519
Report Number(s):
LA-UR--18-23062
Journal Information:
JOM. Journal of the Minerals, Metals & Materials Society, Journal Name: JOM. Journal of the Minerals, Metals & Materials Society Journal Issue: 9 Vol. 70; ISSN 1047-4838
Publisher:
SpringerCopyright Statement
Country of Publication:
United States
Language:
English

References (35)

In-Situ Observation of Texture Changes during Phase Transformations in Ultra-Low-Carbon Steel journal February 2007
Overview of Materials Qualification Needs for Metal Additive Manufacturing journal January 2016
Evaluation of the high temperature texture of the β phase of a TA6V sample from the individual orientations of grains of the low temperature α phase journal February 1994
On the process of transition of the cubic-body-centered modification into the hexagonal-close-packed modification of zirconium journal May 1934
Texture analysis in hexagonal materials journal July 2003
A method to determine the orientation of the high-temperature beta phase from measured EBSD data for the low-temperature alpha phase in Ti-6Al-4V journal April 2003
Metal Fabrication by Additive Manufacturing Using Laser and Electron Beam Melting Technologies journal January 2012
Texture changes in the hcp→bcc→hcp transformation of zirconium studied in situ by neutron diffraction journal April 2004
In situ observation of texture evolution during α→β and β→α phase transformations in titanium alloys investigated by neutron diffraction journal October 2007
Texture inheritance and variant selection through an hcp–bcc–hcp phase transformation journal June 2010
Texture and training of magnetic shape memory foam journal April 2013
Memory effects of transformation textures in steel and its prediction by the double Kurdjumov–Sachs relation journal May 2013
Magnetocaloric response of non-stoichiometric Ni2MnGa alloys and the influence of crystallographic texture journal September 2015
Variant selection mechanism by elastic anisotropy and double K-S relation for transformation texture in steel; difference between martensite and ferrite journal March 2018
An overview of Direct Laser Deposition for additive manufacturing; Part II: Mechanical behavior, process parameter optimization and control journal October 2015
The status, challenges, and future of additive manufacturing in engineering journal December 2015
Modeling of additive manufacturing processes for metals: Challenges and opportunities journal August 2017
Role of element partitioning on the α–β phase transformation kinetics of a bi-modal Ti–6Al–6V–2Sn alloy during continuous heating journal March 2015
Texture evolution during annealing of hot extruded U-10wt%Zr alloy by in situ neutron diffraction journal December 2017
In situ observations of lattice expansion and transformation rates of α and β phases in Ti–6Al–4V journal January 2005
Texture analysis with the new HIPPO TOF diffractometer
  • Wenk, H. -R.; Lutterotti, L.; Vogel, S.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 515, Issue 3 https://doi.org/10.1016/j.nima.2003.05.001
journal December 2003
The Los Alamos Neutron Science Center
  • Lisowski, Paul W.; Schoenberg, Kurt F.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 562, Issue 2 https://doi.org/10.1016/j.nima.2006.02.178
journal June 2006
A review on selective laser sintering/melting (SLS/SLM) of aluminium alloy powders: Processing, microstructure, and properties journal October 2015
Additive manufacturing of metallic components – Process, structure and properties journal March 2018
Additive Manufacturing of Titanium Alloy for Aircraft Components journal January 2015
A study of the mechanism of α to β phase transformation by tracking texture evolution with temperature in Ti–6Al–4V using neutron diffraction journal January 2006
In situ investigation of phase transformations in Ti-6Al-4V under additive manufacturing conditions combining laser melting and high-speed micro-X-ray diffraction journal November 2017
Combined texture and structure analysis of deformed limestone from time-of-flight neutron diffraction spectra journal January 1997
A furnace with rotating load frame for in situ high temperature deformation and creep experiments in a neutron diffraction beam line journal May 2012
Laser powder bed fusion additive manufacturing of metals; physics, computational, and materials challenges journal December 2015
Additive manufacturing of metallic components by selective electron beam melting — a review journal March 2016
A six-axis robotic sample changer for high-throughput neutron powder diffraction and texture measurements journal November 2014
Texture measurements using the new neutron diffractometer HIPPO and their analysis using the Rietveld method journal March 2004
Rietveld texture analysis from TOF neutron diffraction data journal September 2010
Spatial variation of melt pool geometry, peak temperature and solidification parameters during laser assisted additive manufacturing process journal November 2014

Cited By (1)

Mapping the Tray of Electron Beam Melting of Ti-6Al-4V: Properties and Microstructure journal May 2019

Figures / Tables (9)


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