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Grain Boundary Characteristics of SiC in Irradiated, AGR-2 TRISO Particles

Conference ·
OSTI ID:1478774
Microstructural characterization of the SiC layer was carried out on neutron irradiated, tristructural isotropic (TRISO) particles from the Advanced Gas Reactor (AGR)-2 experiment. The SiC grain boundary distribution in each particle was characterized with precession electron diffraction in the transmission electron microscope. Generally, the distributions in the AGR-2 TRISO particles (fabricated at the pilot scale by an industrial vendor) were similar to the Variant 3, AGR-1 TRISO particles made on a laboratory-scale at Oak Ridge National Laboratory. Slightly more random, high-angle grain boundaries in conjunction with slightly less low-angle grain boundaries were found in the AGR-2 TRISO particles compared to AGR-1 TRISO particles. Plotting the Ag-110m retention exhibited by both Variant 3 AGR-1 and AGR-2 irradiated TRISO particles against various grain boundary types revealed Ag retention correlate with the random, high-angle and twin grain boundary fraction in the center area of the SiC layer. Observations associated with localized areas of precipitation also will be reported in this paper.
Research Organization:
Idaho National Laboratory (INL), Idaho Falls, ID (United States)
Sponsoring Organization:
USDOE Office of Nuclear Energy (NE)
DOE Contract Number:
AC07-05ID14517
OSTI ID:
1478774
Report Number(s):
INL/CON-18-44482-Rev001
Country of Publication:
United States
Language:
English