Characterization and modeling of microstructural stresses in alumina

Teague, Melissa C.; Rodgers, Theron; Grutzik, Scott Joseph; Meserole, Stephen

doi:10.1111/jace.15369

Characterization and modeling of microstructural stresses in alumina

Journal Article · Wed Dec 06 23:00:00 EST 2017 · Journal of the American Ceramic Society

DOI:https://doi.org/10.1111/jace.15369· OSTI ID:1476936

^[1]; Rodgers, Theron ^[1]; Grutzik, Scott Joseph ^[1]; Meserole, Stephen ^[1]

Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)

Brittle failure is often influenced by difficult to measure and variable microstructure–scale stresses. Recent advances in photoluminescence spectroscopy (PLS), including improved confocal laser measurement and rapid spectroscopic data collection have established the potential to map stresses with microscale spatial resolution (< 2 μm). Advanced PLS was successfully used to investigate both residual and externally applied stresses in polycrystalline alumina at the microstructure scale. The measured average stresses matched those estimated from beam theory to within one standard deviation, validating the technique. Modeling the residual stresses within the microstructure produced qualitative agreement in comparison with the experimentally measured results. In conclusion, microstructure scale modeling is primed to take advantage of advanced PLS to enable its refinement and validation, eventually enabling microstructure modeling to become a predictive tool for brittle materials.

View Accepted Manuscript (DOE)

Research Organization:: Sandia National Laboratories (SNL-NM), Albuquerque, NM (United States)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA)

Grant/Contract Number:: AC04-94AL85000

OSTI ID:: 1476936

Report Number(s):: SAND--2018-10407J; 668234

Journal Information:: Journal of the American Ceramic Society, Journal Name: Journal of the American Ceramic Society Journal Issue: 5 Vol. 101; ISSN 0002-7820

Publisher:: American Ceramic SocietyCopyright Statement

Country of Publication:: United States

Language:: English

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Cited By (3)

Full stress tensor measurement using fluorescence spectroscopy Grutzik, S. J.; Teague, M. C. Journal of Applied Physics, Vol. 125, Issue 15 https://doi.org/10.1063/1.5088584	journal	April 2019
Stress Measurements in Alumina by Optical Fluorescence: Revisited Cook, Robert F.; Michaels, Chris A. SSRN Electronic Journal https://doi.org/10.2139/ssrn.3275460	journal	January 2018
Stress Measurements in Alumina by Optical Fluorescence: Revisited Cook, Robert F.; Michaels, Chris A. Journal of Research of the National Institute of Standards and Technology, Vol. 124 https://doi.org/10.6028/jres.124.020	journal	January 2019

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36 MATERIALS SCIENCE
alumina
modeling/model
photoluminescence
stress

Characterization and modeling of microstructural stresses in alumina

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