Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements

Podlesnyak, Andrey A.; Loguillo, Mark; Rucker, Gerald M.; Haberl, Bianca; Boehler, Reinhard; Ehlers, Georg; Daemen, Luke L.; Armitage, Douglas P.; Frontzek, Matthias D.; Lumsden, Mark D.

doi:10.1080/08957959.2018.1519560

Title: Clamp cell with in situ pressure monitoring for low-temperature neutron scattering measurements

Journal Article · Thu Sep 20 00:00:00 EDT 2018 · High Pressure Research

DOI:https://doi.org/10.1080/08957959.2018.1519560· OSTI ID:1474603

^[1]; Loguillo, Mark ^[1]; Rucker, Gerald M. ^[1];

^[1]; Boehler, Reinhard ^[1];

^[2]; Daemen, Luke L. ^[1]; Armitage, Douglas P. ^[1];

^[1];

^[1]

Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Neutron Scattering Division
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Neutron Technologies Division

In this study, a clamp pressure cell for neutron scattering experiments at low temperatures and in external magnetic fields under pressure up to 2 GPa has been fabricated and tested. The cell provides optical access to the sample space that allows instantaneous pressure determination during sample loading, cooling and measuring using ruby and/or samarium doped strontium tetraborate fluorescence monitoring. Additionally, a new calibration curve of the pressure-induced shift of the ⁷D₀-⁵F₀ (0-0) line in the fluorescent spectrum of SrB₄O₇:Sm²⁺ for moderate pressures, P≤2 GPa, is given.

View Accepted Manuscript (DOE)

Cite

Export

Save

Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC05-00OR22725

OSTI ID:: 1474603

Journal Information:: High Pressure Research, Vol. 38, Issue 4; ISSN 0895-7959

Publisher:: Taylor & FrancisCopyright Statement

Country of Publication:: United States

Language:: English

Citation Metrics:

Cited by: 8 works

Citation information provided by
Web of Science

References (40)

Pressure-induced topological quantum phase transition in Sb $_{2}$ Se $_{3}$ Li, Wei; Wei, Xin-Yuan; Zhu, Jian-Xin Physical Review B, Vol. 89, Issue 3 https://doi.org/10.1103/PhysRevB.89.035101	journal	January 2014
Novel diamond cells for neutron diffraction using multi-carat CVD anvils Boehler, R.; Molaison, J. J.; Haberl, B. Review of Scientific Instruments, Vol. 88, Issue 8 https://doi.org/10.1063/1.4997265	journal	August 2017
Pressure-Induced Spin-State Transition in BiCoO ₃ Oka, Kengo; Azuma, Masaki; Chen, Wei-tin Journal of the American Chemical Society, Vol. 132, Issue 27 https://doi.org/10.1021/ja102987d	journal	July 2010
On the temperature correction to the ruby pressure scale Vos, Willem L.; Schouten, Jan A. Journal of Applied Physics, Vol. 69, Issue 9 https://doi.org/10.1063/1.348903	journal	May 1991
Optical pressure sensors for high-pressure–high-temperature studies in a diamond anvil cell Datchi, F.; Dewaele, A.; Loubeyre, P. High Pressure Research, Vol. 27, Issue 4 https://doi.org/10.1080/08957950701659593	journal	December 2007
Pressure-tuned quantum criticality in the antiferromagnetic Kondo semimetal CeNi _{2− δ} As ₂ Luo, Yongkang; Ronning, F.; Wakeham, N. Proceedings of the National Academy of Sciences, Vol. 112, Issue 44 https://doi.org/10.1073/pnas.1509581112	journal	October 2015
Sudden reversal in the pressure dependence of Tc in the iron-based superconductor KFe2As2 Tafti, F. F.; Juneau-Fecteau, A.; Delage, M-È. Nature Physics, Vol. 9, Issue 6 https://doi.org/10.1038/nphys2617	journal	May 2013
An Optical Fluorescence System for Quantitative Pressure Measurement in the Diamond‐Anvil Cell Barnett, J. D.; Block, S.; Piermarini, G. J. Review of Scientific Instruments, Vol. 44, Issue 1 https://doi.org/10.1063/1.1685943	journal	January 1973
Pressure Measurement Made by the Utilization of Ruby Sharp-Line Luminescence Forman, R. A.; Piermarini, G. J.; Barnett, J. D. Science, Vol. 176, Issue 4032 https://doi.org/10.1126/science.176.4032.284	journal	April 1972
SEQUOIA: A Newly Operating Chopper Spectrometer at the SNS Granroth, G. E.; Kolesnikov, A. I.; Sherline, T. E. Journal of Physics: Conference Series, Vol. 251 https://doi.org/10.1088/1742-6596/251/1/012058	journal	November 2010
A comparison of four direct geometry time-of-flight spectrometers at the Spallation Neutron Source Stone, M. B.; Niedziela, J. L.; Abernathy, D. L. Review of Scientific Instruments, Vol. 85, Issue 4 https://doi.org/10.1063/1.4870050	journal	April 2014
New diamond cell for single-crystal x-ray diffraction Boehler, Reinhard Review of Scientific Instruments, Vol. 77, Issue 11 https://doi.org/10.1063/1.2372734	journal	November 2006
Ruby under pressure Syassen, K. High Pressure Research, Vol. 28, Issue 2 https://doi.org/10.1080/08957950802235640	journal	June 2008
Fabrication and efficiency evaluation of a hybrid NiCrAl pressure cell up to 4GPa Fujiwara, Naoki; Matsumoto, Takehiko; Nakazawab, Kazuko- Review of Scientific Instruments, Vol. 78, Issue 7 https://doi.org/10.1063/1.2757129	journal	July 2007
Neutron diffraction observations of interstitial protons in dense ice Guthrie, M.; Boehler, R.; Tulk, C. A. Proceedings of the National Academy of Sciences, Vol. 110, Issue 26 https://doi.org/10.1073/pnas.1309277110	journal	June 2013
Quantum phase transition under pressure in the heavily hydrogen-doped iron-based superconductor LaFeAsO Fujiwara, Naoki; Kawaguchi, Naoto; IImura, Soushi Physical Review B, Vol. 96, Issue 14 https://doi.org/10.1103/PhysRevB.96.140507	journal	October 2017
Freezing of glycerol–water mixtures under pressure Klotz, S.; Takemura, K.; Strässle, Th Journal of Physics: Condensed Matter, Vol. 24, Issue 32 https://doi.org/10.1088/0953-8984/24/32/325103	journal	June 2012
Resolution of VISION, a crystal-analyzer spectrometer Seeger, Philip A.; Daemen, Luke L.; Larese, John Z. Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 604, Issue 3 https://doi.org/10.1016/j.nima.2009.03.204	journal	June 2009
SrB ₄ O ₇ :Sm ²⁺ pressure optical sensor: Investigations in the megabar range Leger, J. M.; Chateau, C.; Lacam, A. Journal of Applied Physics, Vol. 68, Issue 5 https://doi.org/10.1063/1.346543	journal	September 1990
Improved calibration of the SrB4O7:Sm2+ optical pressure gauge: Advantages at very high pressures and high temperatures Datchi, F.; LeToullec, R.; Loubeyre, P. Journal of Applied Physics, Vol. 81, Issue 8 https://doi.org/10.1063/1.365025	journal	April 1997
Reemergent Superconductivity and Avoided Quantum Criticality in Cd-Doped ${CeIrIn}_{5}$ under Pressure Chen, Y.; Jiang, W. B.; Guo, C. Y. Physical Review Letters, Vol. 114, Issue 14 https://doi.org/10.1103/PhysRevLett.114.146403	journal	April 2015
Hydrostatic limits in liquids and solids to 100 kbar Piermarini, G. J.; Block, S.; Barnett, J. D. Journal of Applied Physics, Vol. 44, Issue 12 https://doi.org/10.1063/1.1662159	journal	December 1973
Design and operation of the wide angular-range chopper spectrometer ARCS at the Spallation Neutron Source Abernathy, D. L.; Stone, M. B.; Loguillo, M. J. Review of Scientific Instruments, Vol. 83, Issue 1 https://doi.org/10.1063/1.3680104	journal	January 2012
Drastic Pressure Effect on the Extremely Large Magnetoresistance in ${WTe}_{2}$ : Quantum Oscillation Study Cai, P. L.; Hu, J.; He, L. P. Physical Review Letters, Vol. 115, Issue 5 https://doi.org/10.1103/PhysRevLett.115.057202	journal	July 2015
Charge disproportionation and the pressure-induced insulator–metal transition in cubic perovskite PbCrO ₃ Cheng, Jinguang; Kweon, K. E.; Larregola, S. A. Proceedings of the National Academy of Sciences, Vol. 112, Issue 6 https://doi.org/10.1073/pnas.1424431112	journal	January 2015
Linewidth and Temperature Shift of the R Lines in Ruby McCumber, D. E.; Sturge, M. D. Journal of Applied Physics, Vol. 34, Issue 6 https://doi.org/10.1063/1.1702657	journal	June 1963
High‐Pressure Equation of State for NaCl, KCl, and CsCl Decker, D. L. Journal of Applied Physics, Vol. 42, Issue 8 https://doi.org/10.1063/1.1660714	journal	July 1971
Neutron scattering lengths and cross sections Sears, Varley F. Neutron News, Vol. 3, Issue 3 https://doi.org/10.1080/10448639208218770	journal	January 1992
Material properties of Ni Cr Al alloy and design of a 4 GPa class non-magnetic high-pressure cell Uwatoko, Yoshiya; Todo, Sakae; Ueda, Kazuhiro Journal of Physics: Condensed Matter, Vol. 14, Issue 44 https://doi.org/10.1088/0953-8984/14/44/469	journal	October 2002
Recent progress on HYSPEC, and its polarization analysis capabilities Winn, Barry; Filges, Uwe; Garlea, V. Ovidiu EPJ Web of Conferences, Vol. 83 https://doi.org/10.1051/epjconf/20158303017	journal	January 2015
Large-volume diamond cells for neutron diffraction above 90 GPa Boehler, R.; Guthrie, M.; Molaison, J. J. High Pressure Research, Vol. 33, Issue 3 https://doi.org/10.1080/08957959.2013.823197	journal	August 2013
Calibration of the ruby pressure gauge to 800 kbar under quasi-hydrostatic conditions Mao, H. K.; Xu, J.; Bell, P. M. Journal of Geophysical Research, Vol. 91, Issue B5, p. 4673-4676 https://doi.org/10.1029/JB091iB05p04673	journal	January 1986
High‐pressure measurements at moderate temperatures in a diamond anvil cell with a new optical sensor: SrB ₄ O ₇ :Sm ² ⁺ Lacam, A.; Chateau, C. Journal of Applied Physics, Vol. 66, Issue 1 https://doi.org/10.1063/1.343884	journal	July 1989
Optical calibration of pressure sensors for high pressures and temperatures Goncharov, Alexander F.; Zaug, Joseph M.; Crowhurst, Jonathan C. Journal of Applied Physics, Vol. 97, Issue 9 https://doi.org/10.1063/1.1895467	journal	May 2005
The new cold neutron chopper spectrometer at the Spallation Neutron Source: Design and performance Ehlers, G.; Podlesnyak, A. A.; Niedziela, J. L. Review of Scientific Instruments, Vol. 82, Issue 8 https://doi.org/10.1063/1.3626935	journal	August 2011
The cold neutron chopper spectrometer at the Spallation Neutron Source—A review of the first 8 years of operation Ehlers, G.; Podlesnyak, A. A.; Kolesnikov, A. I. Review of Scientific Instruments, Vol. 87, Issue 9 https://doi.org/10.1063/1.4962024	journal	September 2016
The Wide Angle Neutron Diffractometer squared (WAND2) - Possibilities and future Frontzek, M. D.; Andrews, K. M.; Jones, A. B. Physica B: Condensed Matter, Vol. 551 https://doi.org/10.1016/j.physb.2017.12.027	journal	December 2018
Quantum Phase transition under pressure in a heavily hydrogen-doped iron-based superconductor LaFeAsO Fujiwara, Naoki; Kawaguchi, Naoto; IImura, Soushi arXiv https://doi.org/10.48550/arxiv.1710.06640	text	January 2017
Hydrostatic limits of 11 pressure transmitting media Klotz, S.; Chervin, J-C.; Munsch, P. Journal of Physics D: Applied Physics, Vol. 42, Issue 7, Article No. 075413 https://doi.org/10.1088/0022-3727/42/7/075413	journal	March 2009
The Cold Neutron Chopper Spectrometer at the Spallation Neutron Source - A Review of the first 8 Years of Operation Ehlers, Georg; Podlesnyak, Andrey A.; Kolesnikov, Alexander I. arXiv https://doi.org/10.48550/arxiv.1609.00348	text	January 2016

Cited By (2)

Effect of fine-tuning pore structures on the dynamics of confined water Kolesnikov, A. I.; Anovitz, L. M.; Hawthorne, F. C. The Journal of Chemical Physics, Vol. 150, Issue 20 https://doi.org/10.1063/1.5096771	journal	May 2019
Metal–organic frameworks under pressure Collings, Ines E.; Goodwin, Andrew L. Journal of Applied Physics, Vol. 126, Issue 18 https://doi.org/10.1063/1.5126911	journal	November 2019

Figures / Tables (6)

Similar Records

Improved calibration of the {bold SrB}{sub 4}{bold O}{sub 7}{bold :Sm}{sup 2+} optical pressure gauge: Advantages at very high pressures and high temperatures

Journal Article · Tue Apr 01 00:00:00 EST 1997 · Journal of Applied Physics · OSTI ID:1474603

Datchi, F; LeToullec, R; Loubeyre, P

Optical calibration of pressure sensors for high pressures and temperatures

Journal Article · Mon Oct 04 00:00:00 EDT 2004 · Journal of Applied Physics · OSTI ID:1474603

Goncharov, A F; Gregoryanz, E; Zaug, J M; +1 more

Optical calibration of pressure sensors for high pressures and temperatures

Journal Article · Sun May 01 00:00:00 EDT 2005 · Journal of Applied Physics · OSTI ID:1474603

Goncharov, Alexander F; Zaug, Joseph M; Crowhurst, Jonathan C; +1 more

Related Subjects

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY
neutron scattering
pressure measurements
clamp cell
fluorescence