Single crystal toroidal diamond anvils for high pressure experiments beyond 5 megabar

Jenei, Zs.; O’Bannon, E. F.; Weir, S. T.; Cynn, H.; Lipp, M. J.; Evans, W. J.

doi:10.1038/s41467-018-06071-x

Title: Single crystal toroidal diamond anvils for high pressure experiments beyond 5 megabar

Journal Article · Mon Sep 03 00:00:00 EDT 2018 · Nature Communications

DOI:https://doi.org/10.1038/s41467-018-06071-x· OSTI ID:1474369

^[1]; O’Bannon, E. F. ^[1]; Weir, S. T. ^[1]; Cynn, H. ^[1]; Lipp, M. J. ^[1]; Evans, W. J. ^[1]

Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

Static compression experiments over 4 Mbar are rare, yet critical for developing accurate fundamental physics and chemistry models, relevant to a range of topics including modeling planetary interiors. Here we show that focused ion beam crafted toroidal single-crystal diamond anvils with ~9.0 μm culets are capable of producing pressures over 5 Mbar. The toroidal surface prevents gasket outflow and provides a means to stabilize the central culet. We have reached a maximum pressure of ~6.15 Mbar using Re as in situ pressure marker, a pressure regime typically accessed only by double-stage diamond anvils and dynamic compression platforms. In conclusion, optimizing single-crystal diamond anvil design is key for extending the pressure range over which studies can be performed in the diamond anvil cell.

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Research Organization:: Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA)

Grant/Contract Number:: AC52-07NA27344

OSTI ID:: 1474369

Report Number(s):: LLNL-JRNL-746958; 931484

Journal Information:: Nature Communications, Vol. 9, Issue 1; ISSN 2041-1723

Publisher:: Nature Publishing GroupCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 48 works

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Contributed Review: Culet diameter and the achievable pressure of a diamond anvil cell: Implications for the upper pressure limit of a diamond anvil cell O’Bannon, Earl F.; Jenei, Zsolt; Cynn, Hyunchae Review of Scientific Instruments, Vol. 89, Issue 11 https://doi.org/10.1063/1.5049720	journal	November 2018
Fly scan apparatus for high pressure research using diamond anvil cells Smith, Jesse S.; Rod, Eric A.; Shen, Guoyin Review of Scientific Instruments, Vol. 90, Issue 1 https://doi.org/10.1063/1.5057445	journal	January 2019
High-pressure isothermal equation of state of composite materials: A case study of LX-17 polymer bonded explosive Leversee, River A.; Zaug, Joseph M.; Sain, John D. Applied Physics Letters, Vol. 115, Issue 5 https://doi.org/10.1063/1.5108677	journal	July 2019
Intermolecular coupling and fluxional behavior of hydrogen in phase IV Goncharov, Alexander F.; Chuvashova, Irina; Ji, Cheng Proceedings of the National Academy of Sciences, Vol. 116, Issue 51 https://doi.org/10.1073/pnas.1916385116	journal	December 2019
Intermolecular coupling and fluxional behavior of hydrogen in phase IV Goncharov, Alexander F.; Chuvashova, Irina; Ji, Cheng arXiv https://doi.org/10.48550/arxiv.1908.05703	text	January 2019

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