A CO2 laser heating system for in situ high pressure-temperature experiments at HPCAT

Smith, Dean; Smith, Jesse S.; Childs, Christian; Rod, Eric; Hrubiak, Rostislav; Shen, Guoyin; Salamat, Ashkan

doi:10.1063/1.5040508

Title: A CO₂ laser heating system for in situ high pressure-temperature experiments at HPCAT

Journal Article · Wed Aug 01 00:00:00 EDT 2018 · Review of Scientific Instruments

DOI:https://doi.org/10.1063/1.5040508· OSTI ID:1463723

^[1]; Smith, Jesse S. ^[2]; Childs, Christian ^[1]; Rod, Eric ^[2]; Hrubiak, Rostislav ^[2]; Shen, Guoyin ^[2];

^[1]

Univ. of Nevada, Las Vegas, NV (United States). HiPSEC & Physics Dept.
Carnegie Inst. of Science, Argonne, IL (United States). High Pressure Collaborative Access Team (HPCAT), Geophysical Lab.

We present a CO₂ laser heating setup for synchrotron x-ray diffraction inside a diamond anvil cell, situated at HPCAT (Sector 16, Advanced Photon Source, Argonne National Lab, Illinois, USA), which is modular and portable between the HPCAT experiment hutches. Specifically, the system allows direct laser heating of wide bandgap insulating materials to thousands of degrees at static high pressures up to the Mbar regime. Alignment of the focused CO₂ laser spot is performed using a mid-infrared microscope, which addressed past difficulties with aligning the invisible radiation. The implementation of the mid-infrared microscope alongside a mirror pinhole spatial filter system allows precise alignment of the heating laser spot and optical pyrometry measurement location to the x-ray probe. A comparatively large heating spot (~50 μm) relative to the x-ray beam (<10 μm) reduces the risk of temperature gradients across the probed area. Each component of the heating system and its diagnostics have been designed with portability in mind and compatibility with the various experimental hutches at the HPCAT beamlines. We present measurements on ZrO₂ at 5.5 GPa which demonstrate the improved room-temperature diffraction data quality afforded by annealing with the CO₂ laser. We also present in situ measurements at 5.5 GPa up to 2800 K in which we do not observe the postulated fluorite ZrO₂ structure, in agreement with recent findings.

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Research Organization:: Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA); National Science Foundation (NSF); USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: NA0001982; FG02-99ER45775; NA0001974; AC02-06CH11357

OSTI ID:: 1463723

Alternate ID(s):: OSTI ID: 1462453

Journal Information:: Review of Scientific Instruments, Vol. 89, Issue 8; ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: ENGLISH

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Cited by: 15 works

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Pressure-Tuneable Visible-Range Band Gap in the Ionic Spinel Tin Nitride Kearney, John S. C.; Graužinytė, Miglė; Smith, Dean Angewandte Chemie, Vol. 130, Issue 36 https://doi.org/10.1002/ange.201805038	journal	August 2018
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Probing disorder in high-pressure cubic tin (IV) oxide: a combined X-ray diffraction and absorption study Sneed, Daniel; Kearney, John S. C.; Smith, Dean Journal of Synchrotron Radiation, Vol. 26, Issue 4 https://doi.org/10.1107/s1600577519003904	journal	May 2019
From Molecules to Carbon Materials—High Pressure Induced Polymerization and Bonding Mechanisms of Unsaturated Compounds Yang, Xin; Wang, Xuan; Wang, Yida Crystals, Vol. 9, Issue 10 https://doi.org/10.3390/cryst9100490	journal	September 2019
Oxidation of High Yield Strength Metals Tungsten and Rhenium in High-Pressure High-Temperature Experiments of Carbon Dioxide and Carbonates Chuliá-Jordán, Raquel; Santamaría-Pérez, David; Marqueño, Tomás Crystals, Vol. 9, Issue 12 https://doi.org/10.3390/cryst9120676	journal	December 2019
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