Correlation of precipitate evolution with Vickers hardness in Haynes® 282® superalloy: In-situ high-energy SAXS/WAXS investigation

Haas, Sylvio; Andersson, Joel; Fisk, Martin; Park, Jun -Sang; Lienert, Ulrich

doi:10.1016/j.msea.2017.11.035

Title: Correlation of precipitate evolution with Vickers hardness in Haynes® 282® superalloy: In-situ high-energy SAXS/WAXS investigation

Journal Article · Sat Nov 11 00:00:00 EST 2017 · Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing

DOI:https://doi.org/10.1016/j.msea.2017.11.035· OSTI ID:1461548

Haas, Sylvio ^[1]; Andersson, Joel ^[2]; Fisk, Martin ^[3]; Park, Jun -Sang ^[4]; Lienert, Ulrich ^[1]

Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)
Univ. West, Trollhattan (Sweden)
Malmo Univ., Malmo (Sweden); Lund Univ., Lund (Sweden)
Argonne National Lab. (ANL), Argonne, IL (United States)

Here, the aim of this work is to characterise precipitation kinetics in Haynes® 282® superalloy using high-energy Small Angle X-ray Scattering (SAXS) together with Wide Angle X-ray Scattering (WAXS). The phases identified by WAXS include: γ (matrix), γ' (hardening precipitates), MC (metallic carbides), and M₂₃C₆ /M₆C (secondary metallic carbides). The γ'-precipitates are spheroids with a diameter of several nanometres, depending on temperature and aging time. From the SAXS data quantitative parameters such as volume fraction, number density and inter-particle distance were determined and correlated with Vickers microhardness measurements performed ex situ. The strengthening components associated with precipitates and solid solutions were separated using the measured Vickers microhardness and SAXS model parameters. A power law dependence between strengthening attributable to the precipitates and the product of volume fraction and mean precipitate radius was found. The solid solution strengthening component was found to be correlated with the repulsion/diffusion zone width around the precipitates.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: Swedish Foundation for Strategic Research (SSF); USDOE

Grant/Contract Number:: AC02-06CH11357; DEAC02-06CH11357

OSTI ID:: 1461548

Alternate ID(s):: OSTI ID: 1549031

Journal Information:: Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing, Vol. 711, Issue C; ISSN 0921-5093

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 14 works

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Review of the Quench Sensitivity of Aluminium Alloys: Analysis of the Kinetics and Nature of Quench-Induced Precipitation Milkereit, Benjamin; Starink, Marco J.; Rometsch, Paul A. Materials, Vol. 12, Issue 24 https://doi.org/10.3390/ma12244083	journal	December 2019
Investigation of the Effect of Short Exposure in the Temperature Range of 750–950 °C on the Ductility of Haynes® 282® by Advanced Microstructural Characterization Hanning, Fabian; Khan, Abdul Khaliq; Steffenburg-Nordenström, Joachim Metals, Vol. 9, Issue 12 https://doi.org/10.3390/met9121357	journal	December 2019

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Title: Correlation of precipitate evolution with Vickers hardness in Haynes® 282® superalloy: In-situ high-energy SAXS/WAXS investigation

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