Visualization of dynamic fiber-matrix interfacial shear debonding

Chu, Jou -Mei; Claus, Benjamin; Parab, Niranjan; O’Brien, Daniel; Sun, Tao; Fezzaa, Kamel; Chen, Wayne

doi:10.1007/s10853-017-1759-1

Visualization of dynamic fiber-matrix interfacial shear debonding

Journal Article · Tue Oct 31 00:00:00 EDT 2017 · Journal of Materials Science

DOI:https://doi.org/10.1007/s10853-017-1759-1· OSTI ID:1460090

^[1]; Claus, Benjamin ^[1]; Parab, Niranjan ^[2]; O’Brien, Daniel ^[3]; Sun, Tao ^[2]; Fezzaa, Kamel ^[2]; Chen, Wayne ^[1]

Purdue Univ., West Lafayette, IN (United States)
Argonne National Lab. (ANL), Lemont, IL (United States)
U.S. Army Research Lab., Adelphi, MD (United States)

To visualize the debonding event in real time for the study of dynamic crack initiation and propagation at the fiber–matrix interface, a modified tension Kolsky bar was integrated with a high-speed synchrotron X-ray phase-contrast imaging setup. In the gage section, the pull-out configuration was utilized to understand the behavior of interfacial debonding between SC-15 epoxy matrix and S-2 glass fiber, tungsten wire, steel wire, and carbon fiber composite Z-pin at pull-out velocities of 2.5 and 5.0 m s^–1. The load history and images of the debonding progression were simultaneously recorded. Both S-2 glass fiber and Z-pin experienced catastrophic interfacial debonding whereas tungsten and steel wire experienced both catastrophic debonding and stick–slip behavior. Even though S-2 glass fiber and Z-pin samples exhibited a slight increase and tungsten and steel wire samples exhibited a slight decrease in average peak force and average interfacial shear stress as the pull-out velocities were increased, no statistical difference was found for most properties when the velocity was increased. Furthermore, the debonding behavior for each fiber material is similar with increasing pull-out velocity. Thus, the debonding mechanism, peak force, and interfacial shear stress were rate insensitive as the pull-out velocity doubled from 2.5 to 5.0 m s^–1. In conclusion, scanning electron microscope imaging of recovered epoxy beads revealed a snap-back behavior around the meniscus region of the bead for S-2 glass, tungsten, and steel fiber materials at 5.0 m s^–1 whereas those at 2.5 m s^–1 exhibited no snap-back behavior.

View Accepted Manuscript (DOE)

Research Organization:: Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Organization:: U.S. Army Research Laboratory, U.S. Army Research Office (ARO); USDOE

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1460090

Alternate ID(s):: OSTI ID: 22754691

Journal Information:: Journal of Materials Science, Journal Name: Journal of Materials Science Journal Issue: 8 Vol. 53; ISSN 0022-2461

Publisher:: SpringerCopyright Statement

Country of Publication:: United States

Language:: English

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Understanding mechanical behavior of interfaces in materials Dongare, Avinash M.; Rajendran, Arunachalam M.; Namburu, Raju Journal of Materials Science, Vol. 53, Issue 8 https://doi.org/10.1007/s10853-018-2030-0	journal	January 2018
In-Situ Visualization of Tensile Failure in Additively Manufactured 316 L Stainless Steel Kirk, C. D.; Parab, N. D.; Kedir, N. Experimental Mechanics, Vol. 59, Issue 6 https://doi.org/10.1007/s11340-019-00524-0	journal	July 2019
Rate effects on fiber–matrix interfacial transverse debonding behavior Chu, Jou-Mei; Claus, Benjamin; Lim, Boon Him Journal of Composite Materials, Vol. 54, Issue 4 https://doi.org/10.1177/0021998319866904	journal	October 2019

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Related Subjects

36 MATERIALS SCIENCE
Kolsky bar
high-speed synchrotron x-ray
interfacial shear stress
phase contrast imaging
pull-out technique

Visualization of dynamic fiber-matrix interfacial shear debonding

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