Shock and Microstructural Characterization of the α-ω Phase Transition in Titanium Crystals

Morrow, Benjamin M.; Rigg, Paulo A.; Jones, David R.; Addessio, Francis L.; Trujillo, Carl P.; Saavedra, Ramon A.; Martinez, Daniel T.; Cerreta, Ellen K.

doi:10.1007/s40870-017-0129-z

Shock and Microstructural Characterization of the α-ω Phase Transition in Titanium Crystals

Journal Article · Thu Sep 14 00:00:00 EDT 2017 · Journal of Dynamic Behavior of Materials

DOI:https://doi.org/10.1007/s40870-017-0129-z· OSTI ID:1458953

Morrow, Benjamin M. ^[1]; Rigg, Paulo A. ^[2]; Jones, David R. ^[1]; Addessio, Francis L. ^[1]; Trujillo, Carl P. ^[1]; Saavedra, Ramon A. ^[1]; Martinez, Daniel T. ^[1]; Cerreta, Ellen K. ^[1]

Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
Argonne National Lab. (ANL), Argonne, IL (United States)

In this paper, a multicrystal comprised of a small number of large crystals of high-purity titanium and a

[0001]

oriented high-purity single crystal titanium sample were shock loaded using gas gun plate impact experiments. Tests were performed at stresses above the

α - ω

phase transition stress (for high-purity polycrystalline specimens) to observe the behavior of oriented crystals under similar conditions. Post-mortem characterization of the shocked microstructure was conducted on the single crystal sample to measure textures, and quantify phases and twinning. The apparent activation of plastic and transformation mechanisms was dependent upon crystal orientation. Specifically, the

[0001]

crystal showed a higher Hugoniot elastic limit than the

[10 \bar{1} 0]

[3 \bar{1} \bar{4} 4]

orientations. The slope of velocity as a function of time was lower in the

[0001]

orientation than the other orientations during plastic deformation, indicating sluggish transformation kinetics for the α to ω phase transition for the

[0001]

oriented crystal. Finally, microtexture measurements of a recovered

[0001]

oriented single crystal revealed the presence of retained ω phase after unloading, with orientations of the constituent phase fractions indicative of the forward α→ω transition, rather than the reverse ω→α transition, suggesting that the material never achieved a state of 100% ω phase.

View Accepted Manuscript (DOE)

Research Organization:: Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

Sponsoring Organization:: USDOE

Grant/Contract Number:: AC52-06NA25396

OSTI ID:: 1458953

Report Number(s):: LA-UR--16-29363

Journal Information:: Journal of Dynamic Behavior of Materials, Journal Name: Journal of Dynamic Behavior of Materials Journal Issue: 4 Vol. 3; ISSN 2199-7446

Publisher:: SpringerCopyright Statement

Country of Publication:: United States

Language:: English

References (59)

Characterization and Modeling of Titanium Single Crystals Following Dynamic Compression by Split-Hopkinson Pressure Bar Morrow, Benjamin M.; Lebensohn, Ricardo A.; Trujillo, Carl P. Proceedings of the 13th World Conference on Titanium https://doi.org/10.1002/9781119296126.ch194	book	May 2016
The orientation relationship between the α- and ω-phases of titanium and zirconium Usikov, M. P.; Zilbershtein, V. A. Physica Status Solidi (a), Vol. 19, Issue 1 https://doi.org/10.1002/pssa.2210190103	journal	September 1973
The influence of crystallographic texture and interstitial impurities on the mechanical behavior of zirconium Kaschner, G. C.; Gray, G. T. Metallurgical and Materials Transactions A, Vol. 31, Issue 8 https://doi.org/10.1007/s11661-000-0227-7	journal	August 2000
Effects of high rates of loading on the deformation behavior and failure mechanisms of hexagonal close-packed metals and alloys Ramesh, K. T. Metallurgical and Materials Transactions A, Vol. 33, Issue 3 https://doi.org/10.1007/s11661-002-0162-x	journal	March 2002
Orientation Effect on Mechanical Properties of Commercially Pure Titanium at Room Temperature Battaini, M.; Pereloma, E. V.; Davies, C. H. J. Metallurgical and Materials Transactions A, Vol. 38, Issue 2 https://doi.org/10.1007/s11661-006-9040-2	journal	February 2007
In-Situ TEM Observation of Twinning and Detwinning During Cyclic Loading in Mg Morrow, Benjamin M.; McCabe, Rodney J.; Cerreta, Ellen K. Metallurgical and Materials Transactions A, Vol. 45, Issue 1 https://doi.org/10.1007/s11661-013-1765-0	journal	April 2013
Observations of the Atomic Structure of Tensile and Compressive Twin Boundaries and Twin–Twin Interactions in Zirconium Morrow, Benjamin M.; McCabe, Rodney J.; Cerreta, Ellen K. Metallurgical and Materials Transactions A, Vol. 45, Issue 13 https://doi.org/10.1007/s11661-014-2481-0	journal	August 2014
Foreword: Multiscale Perspectives on Plasticity in HCP Metals Morrow, Benjamin M.; Mathaudhu, Suveen N.; Cerreta, Ellen K. Metallurgical and Materials Transactions A, Vol. 45, Issue 13 https://doi.org/10.1007/s11661-014-2578-5	journal	September 2014
Transmission Electron Microscope In Situ Straining Technique to Directly Observe Defects and Interfaces During Deformation in Magnesium Morrow, B. M.; Cerreta, E. K.; McCabe, R. J. JOM, Vol. 67, Issue 8 https://doi.org/10.1007/s11837-015-1432-6	journal	May 2015
Crystallography and a model of the α → ω phase transformation in zirconium Rabinkin, A.; Talianker, M.; Botstein, O. Acta Metallurgica, Vol. 29, Issue 4 https://doi.org/10.1016/0001-6160(81)90152-8	journal	April 1981
Omega phase in materials Sikka, S. K.; Vohra, Y. K.; Chidambaram, R. Progress in Materials Science, Vol. 27, Issue 3-4 https://doi.org/10.1016/0079-6425(82)90002-0	journal	January 1982
Deformation twinning Christian, J. W.; Mahajan, S. Progress in Materials Science, Vol. 39, Issue 1-2 https://doi.org/10.1016/0079-6425(94)00007-7	journal	January 1995
Evolution of microstructure and shear-band formation in α-hcp titanium Meyers, M. A.; Subhash, G.; Kad, B. K. Mechanics of Materials, Vol. 17, Issue 2-3 https://doi.org/10.1016/0167-6636(94)90058-2	journal	March 1994
Constitutive description of dynamic deformation: physically-based mechanisms Meyers, M. A.; Benson, D. J.; Vöhringer, O. Materials Science and Engineering: A, Vol. 322, Issue 1-2 https://doi.org/10.1016/S0921-5093(01)01131-5	journal	January 2002
A model for experimentally-observed high-strain-rate dynamic strain aging in titanium Cheng, Jingyi; Nemat-Nasser, Sia Acta Materialia, Vol. 48, Issue 12 https://doi.org/10.1016/S1359-6454(00)00124-5	journal	July 2000
Strain hardening of titanium: role of deformation twinning Salem, Ayman A.; Kalidindi, Surya R.; Doherty, Roger D. Acta Materialia, Vol. 51, Issue 14 https://doi.org/10.1016/S1359-6454(03)00239-8	journal	August 2003
The high-strain-rate response of alpha-titanium: experiments, deformation mechanisms and modeling Chichili, D. R.; Ramesh, K. T.; Hemker, K. J. Acta Materialia, Vol. 46, Issue 3 https://doi.org/10.1016/S1359-6454(97)00287-5	journal	January 1998
Mechanical properties and deformation mechanisms of a commercially pure titanium Nemat-Nasser, S.; Guo, W. G.; Cheng, J. Y. Acta Materialia, Vol. 47, Issue 13 https://doi.org/10.1016/S1359-6454(99)00203-7	journal	October 1999
The effects of deformation conditions on microstructure and texture of commercially pure Ti Zeng, Zhipeng; Jonsson, Stefan; Roven, Hans Jørgen Acta Materialia, Vol. 57, Issue 19 https://doi.org/10.1016/j.actamat.2009.08.016	journal	November 2009
Influence of texture and test velocity on the dynamic, high-strain, tensile behavior of zirconium Escobedo, J. P.; Cerreta, E. K.; Trujillo, C. P. Acta Materialia, Vol. 60, Issue 11 https://doi.org/10.1016/j.actamat.2012.05.001	journal	June 2012
An examination of the use of the Modified Jogged-Screw model for predicting creep behavior in Zircaloy-4 Morrow, B. M.; Kozar, R. W.; Anderson, K. R. Acta Materialia, Vol. 61, Issue 12 https://doi.org/10.1016/j.actamat.2013.04.014	journal	July 2013
The influence of phase and substructural evolution during dynamic loading on subsequent mechanical properties of zirconium Cerreta, E. K.; Escobedo, J. P.; Rigg, P. A. Acta Materialia, Vol. 61, Issue 20 https://doi.org/10.1016/j.actamat.2013.09.009	journal	December 2013
Anisotropic shock response of titanium: Reorientation and transformation mechanisms Zong, Hongxiang; Lookman, Turab; Ding, Xiangdong Acta Materialia, Vol. 65 https://doi.org/10.1016/j.actamat.2013.11.047	journal	February 2014
Shear banding in commercial pure titanium deformed by dynamic compression Sun, J. L.; Trimby, P. W.; Yan, F. K. Acta Materialia, Vol. 79 https://doi.org/10.1016/j.actamat.2014.07.011	journal	October 2014
Hardening evolution of AZ31B Mg sheet Lou, X.; Li, M.; Boger, R. International Journal of Plasticity, Vol. 23, Issue 1 https://doi.org/10.1016/j.ijplas.2006.03.005	journal	January 2007
A dislocation-based constitutive law for pure Zr including temperature effects Beyerlein, I. J.; Tomé, C. N. International Journal of Plasticity, Vol. 24, Issue 5 https://doi.org/10.1016/j.ijplas.2007.07.017	journal	May 2008
Quantitative analysis of deformation twinning in zirconium McCabe, Rodney J.; Proust, Gwénaëlle; Cerreta, Ellen K. International Journal of Plasticity, Vol. 25, Issue 3 https://doi.org/10.1016/j.ijplas.2008.03.010	journal	March 2009
Anisotropic response of high-purity α-titanium: Experimental characterization and constitutive modeling Nixon, Michael E.; Cazacu, Oana; Lebensohn, Ricardo A. International Journal of Plasticity, Vol. 26, Issue 4 https://doi.org/10.1016/j.ijplas.2009.08.007	journal	April 2010
Flow asymmetry and nucleation stresses of twinning and non-basal slip in magnesium El Kadiri, Haitham; Baird, J. C.; Kapil, J. International Journal of Plasticity, Vol. 44 https://doi.org/10.1016/j.ijplas.2012.11.004	journal	May 2013
Stochastic modeling of twin nucleation in polycrystals: An application in hexagonal close-packed metals Niezgoda, Stephen R.; Kanjarla, Anand K.; Beyerlein, Irene J. International Journal of Plasticity, Vol. 56 https://doi.org/10.1016/j.ijplas.2013.11.005	journal	May 2014
Characterization and modeling of mechanical behavior of single crystal titanium deformed by split-Hopkinson pressure bar Morrow, B. M.; Lebensohn, R. A.; Trujillo, C. P. International Journal of Plasticity, Vol. 82 https://doi.org/10.1016/j.ijplas.2016.03.006	journal	July 2016
Dynamic mechanical behavior of pure titanium Li, Qiang; Xu, Y. B.; Bassim, M. N. Journal of Materials Processing Technology, Vol. 155-156 https://doi.org/10.1016/j.jmatprotec.2004.04.327	journal	November 2004
Experimental study on the dynamic tensile behavior of a poly-crystal pure titanium at elevated temperatures Huang, Wen; Zan, Xiang; Nie, Xu Materials Science and Engineering: A, Vol. 443, Issue 1-2 https://doi.org/10.1016/j.msea.2006.06.041	journal	January 2007
The use of X-ray diffraction to determine slip and twinning activity in commercial-purity (CP) titanium Ungár, T.; Glavicic, M. G.; Balogh, L. Materials Science and Engineering: A, Vol. 493, Issue 1-2 https://doi.org/10.1016/j.msea.2007.06.096	journal	October 2008
Effect of twinning on microstructure and texture evolutions of pure Ti during dynamic plastic deformation Xu, Feng; Zhang, Xiyan; Ni, Haitao Materials Science and Engineering: A, Vol. 564 https://doi.org/10.1016/j.msea.2012.11.097	journal	March 2013
Variability in EBSD statistics for textured zirconium Morrow, B. M.; McCabe, R. J.; Cerreta, E. K. Materials Science and Engineering: A, Vol. 574 https://doi.org/10.1016/j.msea.2013.02.043	journal	July 2013
Toward understanding twin–twin interactions in hcp metals: Utilizing multiscale techniques to characterize deformation mechanisms in magnesium Morrow, B. M.; Cerreta, E. K.; McCabe, R. J. Materials Science and Engineering: A, Vol. 613 https://doi.org/10.1016/j.msea.2014.06.062	journal	September 2014
Substructure evolution of Zircaloy-4 during creep and implications for the Modified Jogged-Screw model Morrow, B. M.; Kozar, R. W.; Anderson, K. R. Materials Science and Engineering: A, Vol. 665 https://doi.org/10.1016/j.msea.2016.04.016	journal	May 2016
Pressure-induced transition in titanium metal a systematic study of the effects of uniaxial stress Errandonea, Daniel; Meng, Y.; Somayazulu, M. Physica B: Condensed Matter, Vol. 355, Issue 1-4, p. 116-125 https://doi.org/10.1016/j.physb.2004.10.030	journal	January 2005
Impurities block the α to ω martensitic transformation in titanium Hennig, Richard G.; Trinkle, Dallas R.; Bouchet, Johann Nature Materials, Vol. 4, Issue 2 https://doi.org/10.1038/nmat1292	journal	January 2005
Shock-induced α–ω transition in titanium Greeff, C. W.; Trinkle, D. R.; Albers, R. C. Journal of Applied Physics, Vol. 90, Issue 5 https://doi.org/10.1063/1.1389334	journal	September 2001
Modeling Dynamic Phase Transitions in Ti and Zr Greeff, C. W. SHOCK COMPRESSION OF CONDENSED MATTER - 2003: Proceedings of the Conference of the American Physical Society Topical Group on Shock Compression of Condensed Matter, AIP Conference Proceedings https://doi.org/10.1063/1.1780218	conference	January 2004
Influence of Temperature upon the α→ω Transition in Titanium Bezruchko, G. S. SHOCK COMPRESSION OF CONDENSED MATTER - 2005: Proceedings of the Conference of the American Physical Society Topical Group on Shock Compression of Condensed Matter, AIP Conference Proceedings https://doi.org/10.1063/1.2263296	conference	January 2006
The Influence of Interstitial Oxygen on the Alpha to Omega Phase Transition in Titanium and Zirconium Cerreta, E. SHOCK COMPRESSION OF CONDENSED MATTER - 2005: Proceedings of the Conference of the American Physical Society Topical Group on Shock Compression of Condensed Matter, AIP Conference Proceedings https://doi.org/10.1063/1.2263526	conference	January 2006
Compact system for high-speed velocimetry using heterodyne techniques Strand, O. T.; Goosman, D. R.; Martinez, C. Review of Scientific Instruments, Vol. 77, Issue 8 https://doi.org/10.1063/1.2336749	journal	August 2006
Inelastic deformation and phase transformation of shock compressed silicon single crystals Turneaure, Stefan J.; Gupta, Y. M. Applied Physics Letters, Vol. 91, Issue 20 https://doi.org/10.1063/1.2814067	journal	November 2007
Influence of impurities on the α to ω phase transition in zirconium under dynamic loading conditions Rigg, P. A.; Greeff, C. W.; Knudson, M. D. Journal of Applied Physics, Vol. 106, Issue 12 https://doi.org/10.1063/1.3267325	journal	December 2009
Omega phase formation in shock-loaded zirconium Song, Shihong; Gray, George T. High-pressure science and technology—1993, AIP Conference Proceedings https://doi.org/10.1063/1.46321	conference	January 1994
Examination of the α-ω two-phase shock-induced microstructure in zirconium and titanium Morrow, Benjamin M.; Escobedo, J. Pablo; Field, Robert D. SHOCK COMPRESSION OF CONDENSED MATTER - 2015: Proceedings of the Conference of the American Physical Society Topical Group on Shock Compression of Condensed Matter, AIP Conference Proceedings https://doi.org/10.1063/1.4971658	conference	January 2017
The α–ω phase transition in shock-loaded titanium Jones, David R.; Morrow, Benjamin M.; Trujillo, Carl P. Journal of Applied Physics, Vol. 122, Issue 4 https://doi.org/10.1063/1.4987146	journal	July 2017
Microscopic and crystallographic aspects of retained omega phase in shock-loaded zirconium and its formation mechanism Song, S. G.; Gray, G. T. Philosophical Magazine A, Vol. 71, Issue 2 https://doi.org/10.1080/01418619508244356	journal	February 1995
Micro-cantilever testing of ⟨a⟩ prismatic slip in commercially pure Ti Gong, Jicheng; Wilkinson, Angus J. Philosophical Magazine, Vol. 91, Issue 7-9 https://doi.org/10.1080/14786435.2010.495359	journal	March 2011
Structural phase stability in nanocrystalline titanium to 161 GPa Velisavljevic, Nenad; Jacobsen, Matthew K.; Vohra, Yogesh K. Materials Research Express, Vol. 1, Issue 3 https://doi.org/10.1088/2053-1591/1/3/035044	journal	September 2014
Computational design of recovery experiments for ductile metals Bourne, N. K.; Gray, G. T. Proceedings of the Royal Society A: Mathematical, Physical and Engineering Sciences, Vol. 461, Issue 2062 https://doi.org/10.1098/rspa.2005.1501	journal	August 2005
Adiabatic release measurements in α -quartz between 300 and 1200 GPa: Characterization of α -quartz as a shock standard in the multimegabar regime Knudson, M. D.; Desjarlais, M. P. Physical Review B, Vol. 88, Issue 18 https://doi.org/10.1103/PhysRevB.88.184107	journal	November 2013
Collective nature of plasticity in mediating phase transformation under shock compression Zong, Hongxiang; Ding, Xiangdong; Lookman, Turab Physical Review B, Vol. 89, Issue 22 https://doi.org/10.1103/PhysRevB.89.220101	journal	June 2014
Orientation Relations During the α - ω Phase Transition of Zirconium: In Situ Texture Observations at High Pressure and Temperature Wenk, H. -R.; Kaercher, P.; Kanitpanyacharoen, W. Physical Review Letters, Vol. 111, Issue 19 https://doi.org/10.1103/PhysRevLett.111.195701	journal	November 2013
New Mechanism for the α to ω Martensitic Transformation in Pure Titanium Trinkle, D. R.; Hennig, R. G.; Srinivasan, S. G. Physical Review Letters, Vol. 91, Issue 2 https://doi.org/10.1103/PhysRevLett.91.025701	journal	July 2003
Alpha to Omega Transition in Shock Compressed Zirconium: Crystallographic Aspects Jyoti, G.; Tewari, R.; Joshi, K. D. Defect and Diffusion Forum, Vol. 279 https://doi.org/10.4028/www.scientific.net/DDF.279.133	journal	August 2008

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Shock and Microstructural Characterization of the α-ω Phase Transition in Titanium Crystals

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