Skip to main content
U.S. Department of Energy
Office of Scientific and Technical Information

Instrumentation for in situ flow electrochemical Scanning Transmission X-ray Microscopy (STXM)

Journal Article · · Review of Scientific Instruments
DOI:https://doi.org/10.1063/1.5023288· OSTI ID:1441043
 [1];  [2];  [3];  [3];  [4];  [4];  [1]
  1. Department of Chemistry and Chemical Biology, McMaster University, Hamilton, Ontario L8S4M1, Canada
  2. BayCEER, University of Bayreuth, D-95448 Bayreuth, Germany
  3. Norcada, Inc., Edmonton, Alberta T6E5B6, Canada
  4. Canadian Light Source, 44 Innovation Boulevard, Saskatoon, Saskatchewan S7N 2V3, Canada
Not Available
Sponsoring Organization:
USDOE
Grant/Contract Number:
AC02-05CH11231
OSTI ID:
1441043
Journal Information:
Review of Scientific Instruments, Journal Name: Review of Scientific Instruments Journal Issue: 6 Vol. 89; ISSN 0034-6748
Publisher:
American Institute of PhysicsCopyright Statement
Country of Publication:
United States
Language:
English

References (66)

Electrochemistry at Microscopic Liquid–Liquid Interfaces journal December 2000
Beyond Intercalation-Based Li-Ion Batteries: The State of the Art and Challenges of Electrode Materials Reacting Through Conversion Reactions (Adv. Mater. 35/2010) journal September 2010
Electrochemical photovoltaic cells-review of recent developments journal November 2010
Mass Transport to micro- and nanoelectrodes and their arrays: a review journal December 2011
X-Ray Interactions: Photoabsorption, Scattering, Transmission, and Reflection at E = 50-30,000 eV, Z = 1-92 journal July 1993
NEXAFS Spectroscopy book January 1992
An improved cell for in-situ electrochemical ESR journal November 1985
Evidence of two kinds of spin in polyaniline from in situ EPR and electrochemistry journal February 1990
Stripping voltammetry at micro-interface arrays: A review journal March 2013
Overview of current development in electrical energy storage technologies and the application potential in power system operation journal January 2015
Ambient-pressure photoelectron spectroscopy for heterogeneous catalysis and electrochemistry journal April 2013
In situ soft X-ray dynamic microscopy of electrochemical processes journal November 2008
Kinetics of copper deposition on Pt(111) and Au(111) electrodes in solutions of different acidities journal September 2005
Development of a liquid flow cell to measure soft X-ray absorption in transmission mode: A test for liquid water journal March 2010
Soft X-ray ptychography as a tool for in operando morphochemical studies of electrodeposition processes with nanometric lateral resolution journal October 2017
Electroanalysis in micro- and nano-scales journal January 2013
Soft X-ray spectromicroscopy beamline at the CLS: Commissioning results
  • Kaznatcheev, K. V.; Karunakaran, Ch.; Lanke, U. D.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 582, Issue 1 https://doi.org/10.1016/j.nima.2007.08.083
journal November 2007
Inkjet 3D Printing – Studies on Applicability for Lab-on-a-chip Technique journal January 2016
A review on fuel cell technologies and power electronic interface journal December 2009
Electrodeposition of composite coatings containing nanoparticles in a metal deposit journal September 2006
Biomolecule-nanoparticle hybrids for electrochemical biosensors journal January 2009
Spectroelectrochemical study of polypyrrole films journal July 1983
Development of Wet Environmental TEM (Wet-ETEM) for In Situ Studies of Liquid-Catalyst Reactions on the Nanoscale journal February 2002
In Situ Electrochemical Measurements in the Nanoaquarium journal August 2013
Quantitative Electrochemical Measurements Using In Situ ec-S/TEM Devices journal March 2014
In-Situ Electrochemical Transmission Electron Microscopy for Battery Research journal April 2014
Tuning Electrodeposition Parameters for Tailored Nanoparticle Size, Shape, and Morphology: An In Situ ec-STEM Investigation journal August 2014
Visualization of Active and Passive Control of Morphology during Electrodeposition journal August 2014
In Situ Spatial and Time-Resolved Studies of Electrochemical Reactions by Scanning Transmission X-ray Microscopy journal June 2005
Spectroelectrochemical Microscopy:  Spatially Resolved Spectroelectrochemistry of Carrier-Based Ion-Selective Membranes journal April 2005
Fabrication of a Sealed Electrochemical Microcell for in Situ Soft X-ray Microspectroscopy and Testing with in Situ Co-Polypyrrole Composite Electrodeposition for Pt-Free Oxygen Electrocatalysis journal December 2013
Interfacial Insight from Operando XAS/TEM for Magnesium Metal Deposition with Borohydride Electrolytes journal August 2017
The Coordinated Use of Synchrotron Spectroelectrochemistry for Corrosion Studies on Heritage Metals journal June 2010
Aqueous Cu(II)–Organic Complexation Studied in Situ Using Soft X-ray and Vibrational Spectroscopies journal November 2013
Fourier transform infrared spectroscopy study of conducting polymer polypyrrole: higher order structure of electrochemically-synthesized film journal July 1991
Quantitative Mapping of Structured Polymeric Systems Using Singular Value Decomposition Analysis of Soft X-ray Images journal May 2002
Electron–Water Interactions and Implications for Liquid Cell Electron Microscopy journal September 2014
Early Stages of Copper Electrocrystallization:  Electrochemical and in Situ X-ray Absorption Fine Structure Studies of Coadsorption of Copper and Chloride at the Au(111) Electrode Surface journal December 1997
All-Nanoparticle Thin-Film Coatings journal October 2006
Atomic-Resolution Spectroscopic Imaging of Ensembles of Nanocatalyst Particles Across the Life of a Fuel Cell journal December 2011
Nanoscale Imaging of Lithium Ion Distribution During In Situ Operation of Battery Electrode and Electrolyte journal February 2014
In Situ Transmission Electron Microscopy of Lead Dendrites and Lead Ions in Aqueous Solution journal June 2012
Near-edge X-ray absorption spectra for metallic Cu and Mn journal November 1981
Ionic-liquid materials for the electrochemical challenges of the future journal July 2009
Dynamic microscopy of nanoscale cluster growth at the solid–liquid interface journal July 2003
In-situ Photoelectron Microspectroscopy and Imaging of Electrochemical Processes at the Electrodes of a Self-driven Cell journal October 2013
Electrochemical deposition of layered copper thin films based on the diffusion limited aggregation journal October 2016
Physical and chemical properties of Cu( i ) compounds with O and/or H journal January 2017
In situ chemical mapping of a lithium-ion battery using full-field hard X-ray spectroscopic imaging journal January 2013
Capsule-free fluid delivery and beam-induced electrodeposition in a scanning electron microscope journal January 2013
Real-time imaging and local elemental analysis of nanostructures in liquids journal January 2014
Soft X-ray spectroscopy from image sequences with sub-100 nm spatial resolution journal February 2000
Recent Advances in Inner-Shell Excitation of Free Molecules by Electron Energy Loss Spectroscopy
  • Brion, C. E.; Daviel, S.; Sodhi, R.
  • X-RAY AND ATOMIC INNER-SHELL PHYSICS, X-82: 1982 International Conference, AIP Conference Proceedings https://doi.org/10.1063/1.2948749
conference January 1982
Electro-deposition of Cu studied with in situ electrochemical scanning transmission x-ray microscopy
  • Hitchcock, A. P.; Qin, Z.; Rosendahl, S. M.
  • XRM 2014: Proceedings of the 12th International Conference on X-Ray Microscopy, AIP Conference Proceedings https://doi.org/10.1063/1.4937497
conference January 2016
Development of in-situ sample cells for scanning transmission x-ray microscopy
  • Ohigashi, Takuji; Nagasaka, Masanari; Horigome, Toshio
  • PROCEEDINGS OF THE 12TH INTERNATIONAL CONFERENCE ON SYNCHROTRON RADIATION INSTRUMENTATION – SRI2015, AIP Conference Proceedings https://doi.org/10.1063/1.4952922
conference January 2016
Dynamic electron microscopy of ATP-induced myosin head movement in living muscle thick filaments journal April 1997
Unoccupied electronic structure and core-hole effects in the x-ray-absorption spectra of Cu 2 O journal February 1992
Comparative soft-x-ray resonant-photoemission study on Bi2Sr2CaCu2O8, CuO, and Cu2O journal April 1992
Energy dependence of Cu L 2 , 3 satellites using synchrotron excited x-ray-emission spectroscopy journal November 1997
Interferometer-controlled scanning transmission X-ray microscopes at the Advanced Light Source journal February 2003
Ordering in a Fluid Inert Gas Confined by Flat Surfaces journal March 2002
Origin and hysteresis of lithium compositional spatiodynamics within battery primary particles journal August 2016
Copper Metallization for High Performance Silicon Technology journal August 2000
Advanced in situ Spectroscopic Techniques and Their Applications in Environmental Biogeochemistry: Introduction to the Special Section journal January 2011
Electrochemical Biosensors - Sensor Principles and Architectures journal March 2008
Characterization of Electrode Materials for Lithium Ion and Sodium Ion Batteries Using Synchrotron Radiation Techniques journal January 2013

Similar Records

Soft x-ray scanning transmission x-ray microscopy (STXM) ofactinide particles
Journal Article · Tue Apr 05 00:00:00 EDT 2005 · Analytical and Bioanalytical Chemistry · OSTI ID:885239

Scanning Transmission X-ray Microscopy (STXM) in Biogeochemical Environments
Journal Article · Mon Dec 31 23:00:00 EST 2007 · Geochimica et Cosmochimica Acta · OSTI ID:980443

Scanning transmission X-ray microscopy study of microbialcalcification
Journal Article · Wed Feb 01 23:00:00 EST 2006 · Geobiology · OSTI ID:876721

Related Subjects