Negating interfacial impedance in garnet-based solid-state Li metal batteries

Han, Xiaogang; Gong, Yunhui; Fu, Kun (Kelvin); He, Xingfeng; Hitz, Gregory T.; Dai, Jiaqi; Pearse, Alex; Liu, Boyang; Wang, Howard; Rubloff, Gary; Mo, Yifei; Thangadurai, Venkataraman; Wachsman, Eric D.; Hu, Liangbing

doi:10.1038/nmat4821

Negating interfacial impedance in garnet-based solid-state Li metal batteries

Journal Article · Mon Dec 19 00:00:00 EST 2016 · Nature Materials

DOI:https://doi.org/10.1038/nmat4821· OSTI ID:1433807

Han, Xiaogang ^[1]; Gong, Yunhui ^[2]; Fu, Kun (Kelvin) ^[2]; He, Xingfeng ^[2]; Hitz, Gregory T. ^[2]; Dai, Jiaqi ^[2]; Pearse, Alex ^[3]; Liu, Boyang ^[2]; Wang, Howard ^[2]; Rubloff, Gary ^[3]; ^[2]; Thangadurai, Venkataraman ^[4]; Wachsman, Eric D. ^[2]; Hu, Liangbing ^[2]

Univ. of Maryland, College Park, MD (United States). Energy Research Center. Dept. of Materials Science and Engineering; University of Maryland
Univ. of Maryland, College Park, MD (United States). Energy Research Center. Dept. of Materials Science and Engineering
Univ. of Maryland, College Park, MD (United States). Energy Research Center. Dept. of Materials Science and Engineering. Inst. for Systems Research
Univ. of Calgary, AB (Canada). Dept. of Chemistry

Garnet-type solid-state electrolytes have attracted extensive attention due to their high ionic conductivity, approaching 1 mS cm^-1, excellent environmental stability, and wide electrochemical stability window, from lithium metal to ~6 V. However, to date, there has been little success in the development of high-performance solid-state batteries using these exceptional materials, the major challenge being the high solid–solid interfacial impedance between the garnet electrolyte and electrode materials. In this paper, we effectively address the large interfacial impedance between a lithium metal anode and the garnet electrolyte using ultrathin aluminium oxide (Al₂O₃) by atomic layer deposition. Li₇La_2.75Ca_0.25Zr_1.75Nb_0.25O₁₂ (LLCZN) is the garnet composition of choice in this work due to its reduced sintering temperature and increased lithium ion conductivity. A significant decrease of interfacial impedance, from 1,710 Ω cm² to 1 Ω cm², was observed at room temperature, effectively negating the lithium metal/garnet interfacial impedance. Experimental and computational results reveal that the oxide coating enables wetting of metallic lithium in contact with the garnet electrolyte surface and the lithiated-alumina interface allows effective lithium ion transport between the lithium metal anode and garnet electrolyte. Finally, we also demonstrate a working cell with a lithium metal anode, garnet electrolyte and a high-voltage cathode by applying the newly developed interface chemistry.

View Accepted Manuscript (DOE)

Research Organization:: Univ. of Maryland, College Park, MD (United States)

Sponsoring Organization:: National Science Foundation (NSF) (United States); USDOE Advanced Research Projects Agency - Energy (ARPA-E); USDOE Office of Energy Efficiency and Renewable Energy (EERE), Vehicle Technologies Office (EE-3V); USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)

Grant/Contract Number:: AR0000384; EE0006860; SC0001160

OSTI ID:: 1433807

Alternate ID(s):: OSTI ID: 1388692

Journal Information:: Nature Materials, Journal Name: Nature Materials Journal Issue: 5 Vol. 16; ISSN 1476-1122

Publisher:: Nature Publishing GroupCopyright Statement

Country of Publication:: United States

Language:: English

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Incorporating Flexibility into Stiffness: Self‐Grown Carbon Nanotubes in Melamine Sponges Enable A Lithium‐Metal‐Anode Capacity of 15 mA h cm ⁻² Cyclable at 15 mA cm ⁻² Xie, Jian; Ye, Jianglin; Pan, Fei Advanced Materials https://doi.org/10.1002/adma.201805654	journal	December 2018
Self‐Suppression of Lithium Dendrite in All‐Solid‐State Lithium Metal Batteries with Poly(vinylidene difluoride)‐Based Solid Electrolytes Zhang, Xue; Wang, Shuo; Xue, Chuanjiao Advanced Materials, Vol. 31, Issue 11 https://doi.org/10.1002/adma.201806082	journal	January 2019
Lithium-Graphite Paste: An Interface Compatible Anode for Solid-State Batteries Duan, Jian; Wu, Wangyan; Nolan, Adelaide M. Advanced Materials, Vol. 31, Issue 10 https://doi.org/10.1002/adma.201807243	journal	January 2019
Extended Electrochemical Window of Solid Electrolytes via Heterogeneous Multilayered Structure for High‐Voltage Lithium Metal Batteries Duan, Hui; Fan, Min; Chen, Wan‐Ping Advanced Materials, Vol. 31, Issue 12 https://doi.org/10.1002/adma.201807789	journal	January 2019
An Autotransferable g‐C ₃ N ₄ Li ⁺ ‐Modulating Layer toward Stable Lithium Anodes Guo, Yanpeng; Niu, Ping; Liu, Yayuan Advanced Materials, Vol. 31, Issue 27 https://doi.org/10.1002/adma.201900342	journal	May 2019
Interlayered Dendrite‐Free Lithium Plating for High‐Performance Lithium‐Metal Batteries Xu, Ying; Li, Tao; Wang, Liping Advanced Materials, Vol. 31, Issue 29 https://doi.org/10.1002/adma.201901662	journal	May 2019
Electrochemical and Structural Analysis in All‐Solid‐State Lithium Batteries by Analytical Electron Microscopy: Progress and Perspectives Zhang, Chunchen; Feng, Yuzhang; Han, Zhen Advanced Materials https://doi.org/10.1002/adma.201903747	journal	October 2019
Reduced‐Graphene‐Oxide‐Guided Directional Growth of Planar Lithium Layers Li, Nan; Zhang, Kun; Xie, Keyu Advanced Materials, Vol. 32, Issue 7 https://doi.org/10.1002/adma.201907079	journal	November 2019
Advances in Interfaces between Li Metal Anode and Electrolyte Zhang, Xue-Qiang; Cheng, Xin-Bing; Zhang, Qiang Advanced Materials Interfaces, Vol. 5, Issue 2 https://doi.org/10.1002/admi.201701097	journal	December 2017
The Ab Initio Calculations on the Areal Specific Resistance of Li‐Metal/Li ₇ La ₃ Zr ₂ O ₁₂ Interphase Gao, Jian; Guo, Xuyun; Li, Yutao Advanced Theory and Simulations https://doi.org/10.1002/adts.201900028	journal	April 2019
Correlating Electrode-Electrolyte Interface and Battery Performance in Hybrid Solid Polymer Electrolyte-Based Lithium Metal Batteries Pan, Qiwei; Barbash, Dmitri; Smith, Derrick M. Advanced Energy Materials, Vol. 7, Issue 22 https://doi.org/10.1002/aenm.201701231	journal	August 2017
Universal Soldering of Lithium and Sodium Alloys on Various Substrates for Batteries Wang, Chengwei; Xie, Hua; Zhang, Lei Advanced Energy Materials, Vol. 8, Issue 6 https://doi.org/10.1002/aenm.201701963	journal	October 2017
A Material Perspective of Rechargeable Metallic Lithium Anodes Li, Bin; Wang, Ying; Yang, Shubin Advanced Energy Materials, Vol. 8, Issue 13 https://doi.org/10.1002/aenm.201702296	journal	February 2018
Germanium Thin Film Protected Lithium Aluminum Germanium Phosphate for Solid-State Li Batteries Liu, Yijie; Li, Chao; Li, Bojie Advanced Energy Materials, Vol. 8, Issue 16 https://doi.org/10.1002/aenm.201702374	journal	February 2018
New Na-Ion Solid Electrolytes Na ₄₋ _x Sn ₁₋ _x Sb _x S ₄ (0.02 ≤ x ≤ 0.33) for All-Solid-State Na-Ion Batteries Heo, Jongwook W.; Banerjee, Abhik; Park, Kern Ho Advanced Energy Materials, Vol. 8, Issue 11 https://doi.org/10.1002/aenm.201702716	journal	January 2018
Stable Lithium Electrodeposition at Ultra-High Current Densities Enabled by 3D PMF/Li Composite Anode Fan, Lei; Zhuang, Houlong L.; Zhang, Weidong Advanced Energy Materials, Vol. 8, Issue 15 https://doi.org/10.1002/aenm.201703360	journal	February 2018
Vertically Aligned Lithiophilic CuO Nanosheets on a Cu Collector to Stabilize Lithium Deposition for Lithium Metal Batteries Zhang, Chen; Lv, Wei; Zhou, Guangmin Advanced Energy Materials, Vol. 8, Issue 21 https://doi.org/10.1002/aenm.201703404	journal	April 2018
Flexible, Scalable, and Highly Conductive Garnet-Polymer Solid Electrolyte Templated by Bacterial Cellulose Xie, Hua; Yang, Chunpeng; Fu, Kun Kelvin Advanced Energy Materials, Vol. 8, Issue 18 https://doi.org/10.1002/aenm.201703474	journal	March 2018
Design Strategies, Practical Considerations, and New Solution Processes of Sulfide Solid Electrolytes for All-Solid-State Batteries Park, Kern Ho; Bai, Qiang; Kim, Dong Hyeon Advanced Energy Materials, Vol. 8, Issue 18 https://doi.org/10.1002/aenm.201800035	journal	April 2018
Sulfide Solid Electrolytes for Lithium Battery Applications Lau, Jonathan; DeBlock, Ryan H.; Butts, Danielle M. Advanced Energy Materials, Vol. 8, Issue 27 https://doi.org/10.1002/aenm.201800933	journal	August 2018
Perovskite Membranes with Vertically Aligned Microchannels for All-Solid-State Lithium Batteries Jiang, Zhouyang; Xie, Huiqi; Wang, Suqing Advanced Energy Materials, Vol. 8, Issue 27 https://doi.org/10.1002/aenm.201801433	journal	August 2018
Ion-Sieving Carbon Nanoshells for Deeply Rechargeable Zn-Based Aqueous Batteries Wu, Yutong; Zhang, Yamin; Ma, Yao Advanced Energy Materials, Vol. 8, Issue 36 https://doi.org/10.1002/aenm.201802470	journal	October 2018
Correlation between Li Plating Behavior and Surface Characteristics of Carbon Matrix toward Stable Li Metal Anodes Cui, Jiang; Yao, Shanshan; Ihsan-Ul-Haq, Muhammad Advanced Energy Materials, Vol. 9, Issue 1 https://doi.org/10.1002/aenm.201802777	journal	November 2018
Slurry‐Fabricable Li ⁺ ‐Conductive Polymeric Binders for Practical All‐Solid‐State Lithium‐Ion Batteries Enabled by Solvate Ionic Liquids Oh, Dae Yang; Nam, Young Jin; Park, Kern Ho Advanced Energy Materials, Vol. 9, Issue 16 https://doi.org/10.1002/aenm.201802927	journal	February 2019
Graphitic Carbon Nitride Induced Micro-Electric Field for Dendrite-Free Lithium Metal Anodes Lu, Ziyang; Liang, Qinghua; Wang, Bo Advanced Energy Materials, Vol. 9, Issue 7 https://doi.org/10.1002/aenm.201803186	journal	January 2019
Dopant‐Dependent Stability of Garnet Solid Electrolyte Interfaces with Lithium Metal Zhu, Yisi; Connell, Justin G.; Tepavcevic, Sanja Advanced Energy Materials, Vol. 9, Issue 12 https://doi.org/10.1002/aenm.201803440	journal	January 2019
Viscoelastic and Nonflammable Interface Design–Enabled Dendrite‐Free and Safe Solid Lithium Metal Batteries Ma, Qiang; Zeng, Xian‐Xiang; Yue, Junpei Advanced Energy Materials, Vol. 9, Issue 13 https://doi.org/10.1002/aenm.201803854	journal	February 2019
S‐Doped Graphene‐Regional Nucleation Mechanism for Dendrite‐Free Lithium Metal Anodes Wang, Tianshuai; Zhai, Pengbo; Legut, Dominik Advanced Energy Materials, Vol. 9, Issue 24 https://doi.org/10.1002/aenm.201804000	journal	May 2019
Rational Design of Hierarchical “Ceramic‐in‐Polymer” and “Polymer‐in‐Ceramic” Electrolytes for Dendrite‐Free Solid‐State Batteries Huo, Hanyu; Chen, Yue; Luo, Jing Advanced Energy Materials, Vol. 9, Issue 17 https://doi.org/10.1002/aenm.201804004	journal	March 2019
Commercialization of Lithium Battery Technologies for Electric Vehicles Zeng, Xiaoqiao; Li, Matthew; Abd El‐Hady, Deia Advanced Energy Materials, Vol. 9, Issue 27 https://doi.org/10.1002/aenm.201900161	journal	June 2019
Suppressing Lithium Dendrite Growth via Sinusoidal Ripple Current Produced by Triboelectric Nanogenerators Zhang, Zailei; Wang, Zhong Lin; Lu, Xianmao Advanced Energy Materials, Vol. 9, Issue 20 https://doi.org/10.1002/aenm.201900487	journal	April 2019
Revealing the Short‐Circuiting Mechanism of Garnet‐Based Solid‐State Electrolyte Song, Yongli; Yang, Luyi; Zhao, Wenguang Advanced Energy Materials, Vol. 9, Issue 21 https://doi.org/10.1002/aenm.201900671	journal	April 2019
Thick Electrode Batteries: Principles, Opportunities, and Challenges Kuang, Yudi; Chen, Chaoji; Kirsch, Dylan Advanced Energy Materials, Vol. 9, Issue 33 https://doi.org/10.1002/aenm.201901457	journal	July 2019
Ultrathin Bilayer of Graphite/SiO ₂ as Solid Interface for Reviving Li Metal Anode Pathak, Rajesh; Chen, Ke; Gurung, Ashim Advanced Energy Materials, Vol. 9, Issue 36 https://doi.org/10.1002/aenm.201901486	journal	August 2019
Constructing Multifunctional Interphase between Li _1.4 Al _0.4 Ti _1.6 (PO ₄ ) ₃ and Li Metal by Magnetron Sputtering for Highly Stable Solid‐State Lithium Metal Batteries Hao, Xiaoge; Zhao, Qiang; Su, Shiming Advanced Energy Materials, Vol. 9, Issue 34 https://doi.org/10.1002/aenm.201901604	journal	July 2019
Interfacial Incompatibility and Internal Stresses in All‐Solid‐State Lithium Ion Batteries He, Yanming; Lu, Chuanyang; Liu, Shan Advanced Energy Materials, Vol. 9, Issue 36 https://doi.org/10.1002/aenm.201901810	journal	August 2019
Polymer‐in‐“Quasi‐Ionic Liquid” Electrolytes for High‐Voltage Lithium Metal Batteries Wu, Haiping; Xu, Yaobin; Ren, Xiaodi Advanced Energy Materials, Vol. 9, Issue 41 https://doi.org/10.1002/aenm.201902108	journal	September 2019
A 3D Lithium/Carbon Fiber Anode with Sustained Electrolyte Contact for Solid‐State Batteries Zhang, Ying; Shi, Yang; Hu, Xin‐Cheng Advanced Energy Materials, Vol. 10, Issue 3 https://doi.org/10.1002/aenm.201903325	journal	December 2019
Understanding Li‐Ion Dynamics in Lithium Hydroxychloride (Li ₂ OHCl) Solid State Electrolyte via Addressing the Role of Protons Song, Ah‐Young; Turcheniuk, Kostiantyn; Leisen, Johannes Advanced Energy Materials, Vol. 10, Issue 8 https://doi.org/10.1002/aenm.201903480	journal	January 2020
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A Smart Flexible Zinc Battery with Cooling Recovery Ability Zhao, Jingwen; Sonigara, Keval K.; Li, Jiajia Angewandte Chemie, Vol. 129, Issue 27 https://doi.org/10.1002/ange.201704373	journal	June 2017
Transient Behavior of the Metal Interface in Lithium Metal-Garnet Batteries Fu, Kun Kelvin; Gong, Yunhui; Fu, Zhezhen Angewandte Chemie, Vol. 129, Issue 47 https://doi.org/10.1002/ange.201708637	journal	October 2017
A Perovskite Electrolyte That Is Stable in Moist Air for Lithium‐Ion Batteries Li, Yutao; Xu, Henghui; Chien, Po‐Hsiu Angewandte Chemie, Vol. 130, Issue 28 https://doi.org/10.1002/ange.201804114	journal	June 2018
Salt-Based Organic-Inorganic Nanocomposites: Towards A Stable Lithium Metal/Li ₁₀ GeP ₂ S ₁₂ Solid Electrolyte Interface Gao, Yue; Wang, Daiwei; Li, Yuguang C. Angewandte Chemie, Vol. 130, Issue 41 https://doi.org/10.1002/ange.201807304	journal	September 2018
Active‐Oxygen‐Enhanced Homogeneous Nucleation of Lithium Metal on Ultrathin Layered Double Hydroxide Li, Zhenhua; Liu, Ke; Fan, Kui Angewandte Chemie, Vol. 131, Issue 12 https://doi.org/10.1002/ange.201814705	journal	February 2019
Ice as Solid Electrolyte To Conduct Various Kinds of Ions Guo, Zeliang; Wang, Tianshuai; Wei, Hehe Angewandte Chemie, Vol. 131, Issue 36 https://doi.org/10.1002/ange.201907832	journal	July 2019
Water‐Mediated Synthesis of a Superionic Halide Solid Electrolyte Li, Xiaona; Liang, Jianwen; Chen, Ning Angewandte Chemie, Vol. 131, Issue 46 https://doi.org/10.1002/ange.201909805	journal	September 2019
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Columnar Lithium Metal Anodes Zhang, Xue-Qiang; Chen, Xiang; Xu, Rui Angewandte Chemie International Edition, Vol. 56, Issue 45 https://doi.org/10.1002/anie.201707093	journal	September 2017
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In situ formation of a bifunctional interlayer enabled by a conversion reaction to initiatively prevent lithium dendrites in a garnet solid electrolyte Fu, Jiamin; Yu, Pengfei; Zhang, Nian Energy & Environmental Science, Vol. 12, Issue 4 https://doi.org/10.1039/c8ee03390k	journal	January 2019
Sur-/interfacial regulation in all-solid-state rechargeable Li-ion batteries based on inorganic solid-state electrolytes: advances and perspectives Liang, Longwei; Sun, Xuan; Zhang, Jinyang Materials Horizons, Vol. 6, Issue 5 https://doi.org/10.1039/c8mh01593g	journal	January 2019
2D MXene-containing polymer electrolytes for all-solid-state lithium metal batteries Pan, Qiwei; Zheng, Yongwei; Kota, Sankalp Nanoscale Advances, Vol. 1, Issue 1 https://doi.org/10.1039/c8na00206a	journal	January 2019
Formation of self-limited, stable and conductive interfaces between garnet electrolytes and lithium anodes for reversible lithium cycling in solid-state batteries He, Minghui; Cui, Zhonghui; Chen, Cheng Journal of Materials Chemistry A, Vol. 6, Issue 24 https://doi.org/10.1039/c8ta02276c	journal	January 2018
Progress and future prospects of high-voltage and high-safety electrolytes in advanced lithium batteries: from liquid to solid electrolytes Chen, Shimou; Wen, Kaihua; Fan, Juntian Journal of Materials Chemistry A, Vol. 6, Issue 25 https://doi.org/10.1039/c8ta03358g	journal	January 2018
Diagnosis of failure modes for all-solid-state Li-ion batteries enabled by three-electrode cells Nam, Young Jin; Park, Kern Ho; Oh, Dae Yang Journal of Materials Chemistry A, Vol. 6, Issue 30 https://doi.org/10.1039/c8ta03450h	journal	January 2018
A substrate-influenced three-dimensional unoriented dispersion pathway for dendrite-free lithium metal anodes Hu, Mengfei; Yuan, Yuan; Guo, Man Journal of Materials Chemistry A, Vol. 6, Issue 30 https://doi.org/10.1039/c8ta04343d	journal	January 2018
An in situ element permeation constructed high endurance Li–LLZO interface at high current densities Lu, Yang; Huang, Xiao; Ruan, Yadong Journal of Materials Chemistry A, Vol. 6, Issue 39 https://doi.org/10.1039/c8ta07241h	journal	January 2018
Interface engineering in solid state Li metal batteries by quasi-2D hybrid perovskites Wu, Jiafeng; Li, Xinyue; Zhao, Yizhou Journal of Materials Chemistry A, Vol. 6, Issue 42 https://doi.org/10.1039/c8ta07643j	journal	January 2018
Electrochemical performance of a garnet solid electrolyte based lithium metal battery with interface modification Alexander, George V.; Rosero-Navarro, Nataly Carolina; Miura, Akira Journal of Materials Chemistry A, Vol. 6, Issue 42 https://doi.org/10.1039/c8ta07652a	journal	January 2018
A deeply rechargeable zinc anode with pomegranate-inspired nanostructure for high-energy aqueous batteries Chen, Peng; Wu, Yutong; Zhang, Yamin Journal of Materials Chemistry A, Vol. 6, Issue 44 https://doi.org/10.1039/c8ta07809b	journal	January 2018
Ultra-fine surface solid-state electrolytes for long cycle life all-solid-state lithium–air batteries Wang, Sheng; Wang, Jue; Liu, Jingjing Journal of Materials Chemistry A, Vol. 6, Issue 43 https://doi.org/10.1039/c8ta08095j	journal	January 2018
Elucidating the role of dopants in the critical current density for dendrite formation in garnet electrolytes Pesci, Federico M.; Brugge, Rowena H.; Hekselman, A. K. Ola Journal of Materials Chemistry A, Vol. 6, Issue 40 https://doi.org/10.1039/c8ta08366e	journal	January 2018
Atomic layer deposition and first principles modeling of glassy Li ₃ BO ₃ –Li ₂ CO ₃ electrolytes for solid-state Li metal batteries Kazyak, Eric; Chen, Kuan-Hung; Davis, Andrew L. Journal of Materials Chemistry A, Vol. 6, Issue 40 https://doi.org/10.1039/c8ta08761j	journal	January 2018
Revisiting polymeric single lithium-ion conductors as an organic route for all-solid-state lithium ion and metal batteries Jeong, Kihun; Park, Sodam; Lee, Sang-Young Journal of Materials Chemistry A, Vol. 7, Issue 5 https://doi.org/10.1039/c8ta09056d	journal	January 2019
Utilization of biomass pectin polymer to build high efficiency electrode architectures with sturdy construction and fast charge transfer structure to boost sodium storage performance for NASICON-type cathode Zhao, Jing; Yang, Xu; Zhang, Yu Journal of Materials Chemistry A, Vol. 7, Issue 4 https://doi.org/10.1039/c8ta10624j	journal	January 2019
A Li ⁺ conductive metal organic framework electrolyte boosts the high-temperature performance of dendrite-free lithium batteries Chen, Nan; Li, Yuejiao; Dai, Yujuan Journal of Materials Chemistry A, Vol. 7, Issue 16 https://doi.org/10.1039/c8ta12539b	journal	January 2019
A painted layer for high-rate and high-capacity solid-state lithium–metal batteries Sun, Bin; Jin, Yang; Lang, Jialiang Chemical Communications, Vol. 55, Issue 47 https://doi.org/10.1039/c9cc02394a	journal	January 2019
Conversion inorganic interlayer of a LiF/graphene composite in all-solid-state lithium batteries Li, Yingxiang; Li, Yiqiu; Yang, Yanan Chemical Communications, Vol. 56, Issue 11 https://doi.org/10.1039/c9cc09318d	journal	January 2020
LiAl ₅ O ₈ as a potential coating material in lithium-ion batteries: a first principles study Mo, Sijia; Zhang, Bingkai; Zhang, Kecheng Physical Chemistry Chemical Physics, Vol. 21, Issue 25 https://doi.org/10.1039/c9cp02650a	journal	January 2019
Lithium migration pathways at the composite interface of LiBH ₄ and two-dimensional MoS ₂ enabling superior ionic conductivity at room temperature Liu, Zhixiang; Xiang, Mengyuan; Zhang, Yao Physical Chemistry Chemical Physics, Vol. 22, Issue 7 https://doi.org/10.1039/c9cp06090a	journal	January 2020
A graphite intercalation compound associated with liquid Na–K towards ultra-stable and high-capacity alkali metal anodes Zhang, Leyuan; Peng, Sangshan; Ding, Yu Energy & Environmental Science, Vol. 12, Issue 6 https://doi.org/10.1039/c9ee00437h	journal	January 2019
Recent advances in the interface engineering of solid-state Li-ion batteries with artificial buffer layers: challenges, materials, construction, and characterization Du, Mingjie; Liao, Kaiming; Lu, Qian Energy & Environmental Science, Vol. 12, Issue 6 https://doi.org/10.1039/c9ee00515c	journal	January 2019
A bird's-eye view of Li-stuffed garnet-type Li ₇ La ₃ Zr ₂ O ₁₂ ceramic electrolytes for advanced all-solid-state Li batteries Samson, Alfred Junio; Hofstetter, Kyle; Bag, Sourav Energy & Environmental Science, Vol. 12, Issue 10 https://doi.org/10.1039/c9ee01548e	journal	January 2019
Design of a mixed conductive garnet/Li interface for dendrite-free solid lithium metal batteries Huo, Hanyu; Chen, Yue; Li, Ruying Energy & Environmental Science, Vol. 13, Issue 1 https://doi.org/10.1039/c9ee01903k	journal	January 2020
Polar polymer–solvent interaction derived favorable interphase for stable lithium metal batteries Bae, Jiwoong; Qian, Yumin; Li, Yutao Energy & Environmental Science, Vol. 12, Issue 11 https://doi.org/10.1039/c9ee02558h	journal	January 2019
Nano-SiO ₂ coating enabled uniform Na stripping/plating for dendrite-free and long-life sodium metal batteries Jiang, Fuyi; Li, Tianjiao; Ju, Peng Nanoscale Advances, Vol. 1, Issue 12 https://doi.org/10.1039/c9na00658c	journal	January 2019
Nanopore separator of cross-linked poly(propylene glycol)- co -pentaerythritol triacrylate for effectively suppressing polysulfide shuttling in Li–S batteries Li, Haixia; Tang, Wentao; Huang, Yifu Polymer Chemistry, Vol. 10, Issue 21 https://doi.org/10.1039/c9py00206e	journal	January 2019
Solid-state electrolyte considerations for electric vehicle batteries Shen, Hao; Yi, Eongyu; Cheng, Lei Sustainable Energy & Fuels, Vol. 3, Issue 7 https://doi.org/10.1039/c9se00119k	journal	January 2019
A review on strategies addressing interface incompatibilities in inorganic all-solid-state lithium batteries Gurung, Ashim; Pokharel, Jyotshna; Baniya, Abiral Sustainable Energy & Fuels, Vol. 3, Issue 12 https://doi.org/10.1039/c9se00549h	journal	January 2019
Acid induced conversion towards a robust and lithiophilic interface for Li–Li ₇ La ₃ Zr ₂ O ₁₂ solid-state batteries Ruan, Yadong; Lu, Yang; Huang, Xiao Journal of Materials Chemistry A, Vol. 7, Issue 24 https://doi.org/10.1039/c9ta01911a	journal	January 2019
High Li ⁺ transference gel interface between solid-oxide electrolyte and cathode for quasi-solid lithium-ion batteries Subramani, Ramesh; Tseng, Yu-Hsien; Lee, Yuh-Lang Journal of Materials Chemistry A, Vol. 7, Issue 19 https://doi.org/10.1039/c9ta02515d	journal	January 2019
In situ observation of lithium metal plating in a sulfur-based solid electrolyte for all-solid-state batteries Kim, Seong Heon; Kim, KiHong; Choi, Hyungkook Journal of Materials Chemistry A, Vol. 7, Issue 22 https://doi.org/10.1039/c9ta02614b	journal	January 2019
Building better all-solid-state batteries with Li-garnet solid electrolytes and metalloid anodes Afyon, Semih; Kravchyk, Kostiantyn V.; Wang, Shutao Journal of Materials Chemistry A, Vol. 7, Issue 37 https://doi.org/10.1039/c9ta04999a	journal	January 2019
Rationalizing the interphase stability of Li\|doped-Li ₇ La ₃ Zr ₂ O ₁₂ via automated reaction screening and machine learning Liu, Bo; Yang, Jiong; Yang, Hongliang Journal of Materials Chemistry A, Vol. 7, Issue 34 https://doi.org/10.1039/c9ta06748e	journal	January 2019
Understanding the effects of chemical reactions at the cathode–electrolyte interface in sulfide based all-solid-state batteries Jung, Sung-Kyun; Gwon, Hyeokjo; Lee, Seok-Soo Journal of Materials Chemistry A, Vol. 7, Issue 40 https://doi.org/10.1039/c9ta08517c	journal	January 2019
Alkaliphilic Cu ₂ O nanowires on copper foam for hosting Li/Na as ultrastable alkali-metal anodes Ma, Yong; Gu, Yuting; Yao, Yuanzhou Journal of Materials Chemistry A, Vol. 7, Issue 36 https://doi.org/10.1039/c9ta08687k	journal	January 2019
In situ thermally polymerized solid composite electrolytes with a broad electrochemical window for all-solid-state lithium metal batteries Li, Zhuo; Xie, Hui-Xin; Zhang, Xing-Yan Journal of Materials Chemistry A, Vol. 8, Issue 7 https://doi.org/10.1039/c9ta09969g	journal	January 2020
Probing into the origin of an electronic conductivity surge in a garnet solid-state electrolyte Song, Yongli; Yang, Luyi; Tao, Lei Journal of Materials Chemistry A, Vol. 7, Issue 40 https://doi.org/10.1039/c9ta10269h	journal	January 2019
Stable artificial solid electrolyte interphase films for lithium metal anode via metal–organic frameworks cemented by polyvinyl alcohol Fan, Lishuang; Guo, Zhikun; Zhang, Yu Journal of Materials Chemistry A, Vol. 8, Issue 1 https://doi.org/10.1039/c9ta10405d	journal	January 2020
Single-ion conducting gel polymer electrolytes: design, preparation and application Deng, Kuirong; Zeng, Qingguang; Wang, Da Journal of Materials Chemistry A, Vol. 8, Issue 4 https://doi.org/10.1039/c9ta11178f	journal	January 2020
The activation entropy for ionic conduction and critical current density for Li charge transfer in novel garnet-type Li _6.5 La _2.9 A _0.1 Zr _1.4 Ta _0.6 O ₁₂ (A = Ca, Sr, Ba) solid electrolytes Palakkathodi Kammampata, Sanoop; Yamada, Hirotoshi; Ito, Tomoko Journal of Materials Chemistry A, Vol. 8, Issue 5 https://doi.org/10.1039/c9ta12193e	journal	January 2020
A porous framework infiltrating Li–O ₂ battery: a low-resistance and high-safety system Zhang, Yi-Peng; Li, Yi-Qiu; Cui, Zhong-Hui Sustainable Energy & Fuels, Vol. 4, Issue 4 https://doi.org/10.1039/d0se00024h	journal	January 2020
Continuous plating/stripping behavior of solid-state lithium metal anode in a 3D ion-conductive framework Yang, Chunpeng; Zhang, Lei; Liu, Boyang Proceedings of the National Academy of Sciences, Vol. 115, Issue 15 https://doi.org/10.1073/pnas.1719758115	journal	March 2018
Recent progress for all solid state battery using sulfide and oxide solid electrolytes Shoji, Mao; Cheng, Eric Jianfeng; Kimura, Takeshi Journal of Physics D: Applied Physics, Vol. 52, Issue 10 https://doi.org/10.1088/1361-6463/aaf7e2	journal	January 2019
Dual regulation of Li ⁺ migration of Li _6.4 La ₃ Zr _1.4 M _0.6 O ₁₂ (M = Sb, Ta, Nb) by bottleneck size and bond length of M−O Xiang, Xing; Chen, Fei; Yang, Wenyun Journal of the American Ceramic Society, Vol. 103, Issue 4 https://doi.org/10.1111/jace.16920	journal	December 2019
How Metallic Protection Layers Extend the Lifetime of NASICON-Based Solid-State Lithium Batteries Cortes, Francisco Javier Quintero; Lewis, John A.; Tippens, Jared Journal of The Electrochemical Society, Vol. 167, Issue 5 https://doi.org/10.1149/2.0032005jes	journal	October 2019
Review—Solid Electrolytes for Safe and High Energy Density Lithium-Sulfur Batteries: Promises and Challenges Judez, Xabier; Zhang, Heng; Li, Chunmei Journal of The Electrochemical Society, Vol. 165, Issue 1 https://doi.org/10.1149/2.0041801jes	journal	June 2017
Review—Li Metal Anode in Working Lithium-Sulfur Batteries Cheng, Xin-Bing; Huang, Jia-Qi; Zhang, Qiang Journal of The Electrochemical Society, Vol. 165, Issue 1 https://doi.org/10.1149/2.0111801jes	journal	June 2017
Electrochemical Stability of Garnet-Type Li ₇ La _2.75 Ca _0.25 Zr _1.75 Nb _0.25 O ₁₂ with and without Atomic Layer Deposited-Al ₂ O ₃ under CO ₂ and Humidity Hofstetter, Kyle; Samson, Alfred Junio; Dai, Jiaqi Journal of The Electrochemical Society, Vol. 166, Issue 10 https://doi.org/10.1149/2.0201910jes	journal	January 2019
Self-Supporting Dendritic Copper Porous Film Inducing the Lateral Growth of Metallic Lithium for Highly Stable Li Metal Battery Chen, Lijuan; Wang, Mingyong; Lv, Aijing Journal of The Electrochemical Society, Vol. 166, Issue 16 https://doi.org/10.1149/2.0371916jes	journal	January 2019
Lithium Dissolution/Deposition Behavior of Al-Doped Li ₇ La ₃ Zr ₂ O ₁₂ Ceramics with Different Grain Sizes Matsuki, Yuma; Noi, Kousuke; Deguchi, Minako Journal of The Electrochemical Society, Vol. 166, Issue 3 https://doi.org/10.1149/2.0661903jes	journal	January 2019
Design of Porous Solid Electrolytes for Rechargeable Metal Batteries Thomas-Alyea, Karen E. Journal of The Electrochemical Society, Vol. 165, Issue 7 https://doi.org/10.1149/2.1151807jes	journal	January 2018
Review—Practical Challenges Hindering the Development of Solid State Li Ion Batteries Kerman, Kian; Luntz, Alan; Viswanathan, Venkatasubramanian Journal of The Electrochemical Society, Vol. 164, Issue 7 https://doi.org/10.1149/2.1571707jes	journal	January 2017
Synergistic Effect of 3D Current Collectors and ALD Surface Modification for High Coulombic Efficiency Lithium Metal Anodes Chen, Kuan-Hung; Sanchez, Adrian J.; Kazyak, Eric ECS Meeting Abstracts, Vol. MA2019-02, Issue 6 https://doi.org/10.1149/ma2019-02/6/527	journal	September 2019
Interface effects on self-forming rechargeable Li/I2-based solid state batteries Abraham, Alyson; Dunkin, Mikaela R.; Huang, Jianping MRS Communications, Vol. 9, Issue 02 https://doi.org/10.1557/mrc.2019.42	journal	April 2019
Insights into a layered hybrid solid electrolyte and its application in long lifespan high-voltage all-solid-state lithium batteries Yu, Shicheng; Schmohl, Sebastian; Liu, Zigeng RWTH Aachen University https://doi.org/10.18154/rwth-2019-03232	text	January 2019
SYNTHESIS OF Li-CONDUCTIVE NANOPARTICLES WITH NASICON-TYPE STRUCTURE Lisovskyi, Ivan; Solopan, Serhii; Khomenko, Volodymyr Ukrainian Chemistry Journal, Vol. 85, Issue 11 https://doi.org/10.33609/0041-6045.85.11.2019.28-40	journal	December 2019
All-Solid-State Lithium Battery Working without an Additional Separator in a Polymeric Electrolyte Cho, Seonggyu; Kim, Shinho; Kim, Wonho Polymers, Vol. 10, Issue 12 https://doi.org/10.3390/polym10121364	journal	December 2018
Building better all-solid-state batteries with Li-garnet solid electrolytes and metalloid anodes Afyon, Semih; Kravchyk, Kostiantyn V.; Wang, Shutao ETH Zurich https://doi.org/10.3929/ethz-b-000372251	text	January 2019
Lattice-Geometry Effects in Garnet Solid Electrolytes: A Lattice-Gas Monte Carlo Simulation Study Morgan, Benjamin J. arXiv https://doi.org/10.48550/arxiv.1707.00491	preprint	January 2017

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