High temperature microstructural stability and recrystallization mechanisms in 14YWT alloys

Aydogan, E.; El-Atwani, O.; Takajo, S.; Vogel, S. C.; Maloy, S. A.

doi:10.1016/j.actamat.2018.02.006

Title: High temperature microstructural stability and recrystallization mechanisms in 14YWT alloys

Journal Article · Fri Feb 09 00:00:00 EST 2018 · Acta Materialia

DOI:https://doi.org/10.1016/j.actamat.2018.02.006· OSTI ID:1422892

Aydogan, E. ^[1];

^[1]; Takajo, S. ^[2];

^[1];

^[1]

Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
Los Alamos National Lab. (LANL), Los Alamos, NM (United States); JFE Steel Corp., Kurashiki (Japan)

In-situ neutron diffraction experiments were performed on room temperature compressed 14YWT nanostructured ferritic alloys at 1100°C and 1150°C to understand their thermally activated static recrystallization mechanisms. The existence of high density of Y-Ti-O rich nano-oxides (<5 nm) shift the recrystallization temperature up due to Zener pinning of the grain boundaries, making these materials attractive for high temperature applications. This study serves to quantify the texture evolution in-situ and understand the effect of particles on the recrystallization mechanisms in 14YWT alloys. We have shown, both experimentally and theoretically, that there is considerable recovery in the 20% compressed sample after 6.5 h annealing at 1100°C while recrystallization occurs within an hour of annealing at 1100°C and 1150°C in the 60% compressed samples. Moreover, the 60% compressed samples show {112}<110> and {112}<111> texture components during annealing, in contrast to the conventional recrystallization textures in body centered cubic alloys. Furthermore, nano-oxide size, shape, density and distribution are considerably different in unrecrystallized and abnormally grown grains. Transmission electron microscopy analysis shows that oxide particles having a size between 5 and 30 nm play a critical role for recrystallization mechanisms in 14YWT nanostructured ferritic alloys.

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Research Organization:: Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

Sponsoring Organization:: USDOE Office of Nuclear Energy (NE)

Grant/Contract Number:: AC52-06NA25396

OSTI ID:: 1422892

Report Number(s):: LA-UR-18-20894; TRN: US1801666

Journal Information:: Acta Materialia, Vol. 148; ISSN 1359-6454

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 27 works

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