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U.S. Department of Energy
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Controlled molecular weight poly(arylene ether benzimidazole)s endcapped with benzimidazole and acetylene groups

Conference ·
OSTI ID:141676
; ;  [1]
  1. NASA Langley Research Center, Hampton, VA (United States)

As a continuation of work on poly(arylene ether benzimidazole)s (PAEBIs), a series of controlled molecular weight polymers endcapped with benzimidazole, ethynyl, and phenylethynyl groups were prepared at stoichiometric imbalances of 7 and 10 mole percent and characterized. Earlier work with benzimidazole endcapped PAEBIs prepared at stoichiometric imbalances as high as 7 mole percent has shown very good retention of thin film properties up to 232{degrees}C. Ethynyl and phenylethynyl endcapped PAEBIs, air cured to 330{degrees}C, exhibited increases in Tgs of {approximately}20-30{degrees}C with respect to benzimidazole endcapped PAEBIs. Thin film properties for the ethynyl and phenylethynyl endcapped PAEBIs were similar to benzimidazole endcapped PAEBIs up to 232{degrees}C. Ethynyl and phenylethynyl endcapped PAEBI films tested at 250{degrees}C exhibited good retention of tensile properties.

OSTI ID:
141676
Report Number(s):
CONF-930304--
Country of Publication:
United States
Language:
English