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Techniques for optimizing nanotips derived from frozen taylor cones

Patent ·
OSTI ID:1411394

Optimization techniques are disclosed for producing sharp and stable tips/nanotips relying on liquid Taylor cones created from electrically conductive materials with high melting points. A wire substrate of such a material with a preform end in the shape of a regular or concave cone, is first melted with a focused laser beam. Under the influence of a high positive potential, a Taylor cone in a liquid/molten state is formed at that end. The cone is then quenched upon cessation of the laser power, thus freezing the Taylor cone. The tip of the frozen Taylor cone is reheated by the laser to allow its precise localized melting and shaping. Tips thus obtained yield desirable end-forms suitable as electron field emission sources for a variety of applications. In-situ regeneration of the tip is readily accomplished. These tips can also be employed as regenerable bright ion sources using field ionization/desorption of introduced chemical species.

Research Organization:
Hirsch Scientific, Pacifica, CA (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
SC0011345
Assignee:
Hirsch, Gregory
Patent Number(s):
9,837,239
Application Number:
15/361,911
OSTI ID:
1411394
Country of Publication:
United States
Language:
English

References (9)

Vacuum electrospray of volatile liquids assisted by infrared laser irradiation journal February 2012
Stable field-induced electron emission from a solidified liquid metal ion source journal January 1998
Large optical field enhancement for nanotips with large opening angles journal June 2015
Electron emission characteristics of solidified gold alloy liquid metal ion sources journal May 1999
New materials and processes for field emission ion and electron emitters journal March 2013
Formation of a nano-emitter for electron field emission on a liquid metal ion source tip after solidification of the alloy journal December 2002
A single-atom sharp iridium tip as an emitter of gas field ion sources journal July 2009
Liquid-metal-jet anode electron-impact x-ray source journal August 2003
Preparation and Characterization of Single-Atom Tips journal December 2004

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