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Title: High-resolution dielectric characterization of minerals: A step towards understanding the basic interactions between microwaves and rocks

Abstract

Microwave energy was demonstrated to be potentially beneficial for reducing the cost of several steps of the mining process. Significant literature was developed about this topic but few studies are focused on understanding the interaction between microwaves and minerals at a fundamental level in order to elucidate the underlying physical processes that control the observed phenomena. This is ascribed to the complexity of such phenomena, related to chemical and physical transformations, where electrical, thermal and mechanical forces play concurrent roles. In this work a new characterization method for the dielectric properties of mineral samples at microwave frequencies is presented. The method is based upon the scanning microwave microscopy technique that enables measurement of the dielectric constant, loss factor and conductivity with extremely high spatial resolution and accuracy. As opposed to conventional dielectric techniques, the scanning microwave microscope can then access and measure the dielectric properties of micrometric-sized mineral inclusions within a complex structure of natural rock. In this work two micrometric hematite inclusions were characterized at a microwave frequency of 3 GHz. Scanning electron microscopy/energy-dispersive x-ray spectroscopy and confocal micro-Raman spectroscopy were used to determine the structural details and chemical and elemental composition of mineral sample on similar scale.

Authors:
 [1];  [2];  [1];  [2];  [1];  [1]
  1. Univ. of Nottingham (United Kingdom)
  2. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Publication Date:
Research Org.:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1408654
DOE Contract Number:  
AC05-00OR22725
Resource Type:
Journal Article
Journal Name:
International Journal of Mineral Processing
Additional Journal Information:
Journal Volume: 151; Journal Issue: C; Journal ID: ISSN 0301-7516
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE

Citation Formats

Monti, T., Tselev, A., Udoudo, O., Ivanov, I. N., Dodds, C., and Kingman, S. W. High-resolution dielectric characterization of minerals: A step towards understanding the basic interactions between microwaves and rocks. United States: N. p., 2016. Web. doi:10.1016/j.minpro.2016.04.003.
Monti, T., Tselev, A., Udoudo, O., Ivanov, I. N., Dodds, C., & Kingman, S. W. High-resolution dielectric characterization of minerals: A step towards understanding the basic interactions between microwaves and rocks. United States. doi:10.1016/j.minpro.2016.04.003.
Monti, T., Tselev, A., Udoudo, O., Ivanov, I. N., Dodds, C., and Kingman, S. W. Wed . "High-resolution dielectric characterization of minerals: A step towards understanding the basic interactions between microwaves and rocks". United States. doi:10.1016/j.minpro.2016.04.003.
@article{osti_1408654,
title = {High-resolution dielectric characterization of minerals: A step towards understanding the basic interactions between microwaves and rocks},
author = {Monti, T. and Tselev, A. and Udoudo, O. and Ivanov, I. N. and Dodds, C. and Kingman, S. W.},
abstractNote = {Microwave energy was demonstrated to be potentially beneficial for reducing the cost of several steps of the mining process. Significant literature was developed about this topic but few studies are focused on understanding the interaction between microwaves and minerals at a fundamental level in order to elucidate the underlying physical processes that control the observed phenomena. This is ascribed to the complexity of such phenomena, related to chemical and physical transformations, where electrical, thermal and mechanical forces play concurrent roles. In this work a new characterization method for the dielectric properties of mineral samples at microwave frequencies is presented. The method is based upon the scanning microwave microscopy technique that enables measurement of the dielectric constant, loss factor and conductivity with extremely high spatial resolution and accuracy. As opposed to conventional dielectric techniques, the scanning microwave microscope can then access and measure the dielectric properties of micrometric-sized mineral inclusions within a complex structure of natural rock. In this work two micrometric hematite inclusions were characterized at a microwave frequency of 3 GHz. Scanning electron microscopy/energy-dispersive x-ray spectroscopy and confocal micro-Raman spectroscopy were used to determine the structural details and chemical and elemental composition of mineral sample on similar scale.},
doi = {10.1016/j.minpro.2016.04.003},
journal = {International Journal of Mineral Processing},
issn = {0301-7516},
number = C,
volume = 151,
place = {United States},
year = {2016},
month = {4}
}