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Cu 2 ZnSnSe 4 Photovoltaic Absorber Layers Evaluated by Transmission X‐Ray Microscopy Tomography: Composition Fluctuations on the Length Scale of Grains

Journal Article · · Solar RRL
 [1];  [2];  [3];  [4];  [5];  [5];  [3];  [6]
  1. Department of Materials Science and Engineering University of Utah 50 Central Campus Drive Salt Lake City UT 84112 USA
  2. Department of Electrical and Computer Engineering University of Utah 50 Central Campus Drive Salt Lake City UT 84112 USA
  3. Stanford Synchrotron Radiation Lightsource SLAC National Accelerator Laboratory 2575 Sand Hill Road Menlo Park CA 94025 USA
  4. Stanford Institute for Materials and Energy Sciences SLAC National Accelerator Laboratory 2575 Sand Hill Road Menlo Park CA 94025 USA
  5. National Renewable Energy Laboratory 15013 Denver West Parkway Golden CO 80401 USA
  6. Department of Materials Science and Engineering University of Utah 50 Central Campus Drive Salt Lake City UT 84112 USA, Department of Electrical and Computer Engineering University of Utah 50 Central Campus Drive Salt Lake City UT 84112 USA

The origins of open‐circuit voltage deficits in Cu 2 ZnSnS(e) 4 ‐based solar cells have been an intense topic of research over the past few years as device efficiencies have never approached those of CuInGaSe 2 based cells despite the materials sharing similar crystal and electronic structures. In this work, we use transmission X‐ray microscopy tomography to investigate the length scales over which elemental fluctuations occur. We find and show evidence of micron‐scale Cu to Zn anti‐correlations over a previously inaccessible combination of resolution and sample size that is consistent with the length scale of grains in this material. This result yields further insight into the causes of the large open‐circuit voltage deficits regularly seen in these devices as well as the challenges of achieving compositional homogeneity in this material.

Sponsoring Organization:
USDOE
Grant/Contract Number:
NONE; AC02-76SF00515
OSTI ID:
1401037
Alternate ID(s):
OSTI ID: 1659998
Journal Information:
Solar RRL, Journal Name: Solar RRL Journal Issue: 1 Vol. 1; ISSN 2367-198X
Publisher:
Wiley Blackwell (John Wiley & Sons)Copyright Statement
Country of Publication:
Germany
Language:
English

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  • Vora, Nirav; Blackburn, Jeffrey; Repins, Ingrid
  • Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films, Vol. 30, Issue 5 https://doi.org/10.1116/1.4732529
journal September 2012
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