Multiscale Characterization of Structural Compositional and Textural Heterogeneity of Nano-porous Geomaterials

Technical Report · Fri Sep 01 04:00:00 EDT 2017

DOI:https://doi.org/10.2172/1395648· OSTI ID:1395648

Yoon, Hongkyu ^[1]

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1. Sandia National Lab. (SNL-NM), Albuquerque, NM (United States). Geomechanics Dept.

The purpose of the project was to perform multiscale characterization of low permeability rocks to determine the effect of physical and chemical heterogeneity on the poromechanical and flow responses of shales and carbonate rocks with a broad range of physical and chemical heterogeneity . An integrated multiscale imaging of shale and carbonate rocks from nanometer to centimeter scales include s dual focused ion beam - scanning electron microscopy (FIB - SEM) , micro computed tomography (micro - CT) , optical and confocal microscopy, and 2D and 3D energy dispersive spectroscopy (EDS). In addition, mineralogical mapping and backscattered imaging with nanoindentation testing advanced the quantitative evaluat ion of the relationship between material heterogeneity and mechanical behavior. T he spatial distribution of compositional heterogeneity, anisotropic bedding patterns, and mechanical anisotropy were employed as inputs for brittle fracture simulations using a phase field model . Comparison of experimental and numerical simulations reveal ed that proper incorporation of additional material information, such as bedding layer thickness and other geometrical attributes of the microstructures, can yield improvements on the numerical prediction of the mesoscale fracture patterns and hence the macroscopic effective toughness. Overall, a comprehensive framework to evaluate the relationship between mechanical response and micro-lithofacial features can allow us to make more accurate prediction of reservoir performance by developing a multi - scale understanding of poromechanical response to coupled chemical and mechanical interactions for subsurface energy related activities.

• Research Organization: Sandia National Laboratories (SNL-NM), Albuquerque, NM (United States)
• Sponsoring Organization: USDOE National Nuclear Security Administration (NNSA)
• DOE Contract Number: AC04-94AL85000; NA0003525
• OSTI ID: 1395648
• Report Number(s): SAND--2017-10273; 657213
• Country of Publication: United States
• Language: English

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36 MATERIALS SCIENCE