Increasing flame ionization detector (FID) sensitivity using post-column oxidation–methanation

Spanjers, Charles S.; Beach, Connor A.; Jones, Andrew J.; Dauenhauer, Paul J.

doi:10.1039/c6ay03363f

Increasing flame ionization detector (FID) sensitivity using post-column oxidation–methanation

Journal Article · Sun Jan 01 04:00:00 EST 2017 · Analytical Methods

DOI:https://doi.org/10.1039/c6ay03363f· OSTI ID:1388889

Spanjers, Charles S. ^[1]; Beach, Connor A. ^[1]; Jones, Andrew J. ^[2]; ^[3]

University of Minnesota; Department of Chemical Engineering and Materials Science; Minneapolis; USA
Activated Research Company; Eden Prairie; USA
University of Minnesota; Department of Chemical Engineering and Materials Science; Minneapolis; USA; Catalysis Center for Energy Innovation (CCEI)

Combining a microreactor with the flame ionization detector (FID) greatly increases its response to highly oxidized organic molecules.

Research Organization:: Energy Frontier Research Centers (EFRC) (United States). Catalysis Center for Energy Innovation (CCEI)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)

DOE Contract Number:: SC0001004

OSTI ID:: 1388889

Journal Information:: Analytical Methods, Journal Name: Analytical Methods Journal Issue: 12 Vol. 9; ISSN AMNECT; ISSN 1759-9660

Publisher:: Royal Society of Chemistry

Country of Publication:: United States

Language:: English

References (20)

Quantification in Gas Chromatography: Prediction of Flame Ionization Detector Response Factors from Combustion Enthalpies and Molecular Structures de Saint Laumer, Jean-Yves; Cicchetti, Esmeralda; Merle, Philippe Analytical Chemistry, Vol. 82, Issue 15 https://doi.org/10.1021/ac1006574	journal	August 2010
Quantification of biogenic volatile organic compounds with a flame ionization detector using the effective carbon number concept Faiola, C. L.; Erickson, M. H.; Fricaud, V. L. Atmospheric Measurement Techniques, Vol. 5, Issue 8 https://doi.org/10.5194/amt-5-1911-2012	journal	January 2012
Simultaneous determination of endocrine disrupting phenolic compounds and steroids in water by solid-phase extraction–gas chromatography–mass spectrometry Liu, R.; Zhou, J. L.; Wilding, A. Journal of Chromatography A, Vol. 1022, Issue 1-2 https://doi.org/10.1016/j.chroma.2003.09.035	journal	January 2004
The enigmatic mechanism of the flame ionization detector: Its overlooked implications for fossil fuel combustion modeling Schofield, Keith Progress in Energy and Combustion Science, Vol. 34, Issue 3 https://doi.org/10.1016/j.pecs.2007.08.001	journal	June 2008
Monitoring with carbon analyzers Arin, M. Louis Environmental Science & Technology, Vol. 8, Issue 10 https://doi.org/10.1021/es60095a009	journal	October 1974
Flame Ionization Detection of Carbon Monoxide for Gas Chromatographic Analysis. Porter, Kenneth; Volman, D. H. Analytical Chemistry, Vol. 34, Issue 7 https://doi.org/10.1021/ac60187a009	journal	June 1962
Flame Ionization Detector for Gas Chromatography McWILLIAM, I. G.; Dewar, R. A. Nature, Vol. 181, Issue 4611 https://doi.org/10.1038/181760a0	journal	March 1958
Qualitative and quantitative analysis of pyrolysis oil by gas chromatography with flame ionization detection and comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometry Sfetsas, Themistoklis; Michailof, Chrysa; Lappas, Angelos Journal of Chromatography A, Vol. 1218, Issue 21 https://doi.org/10.1016/j.chroma.2010.10.034	journal	May 2011
Response Factors for Gas Chromatographic Analyses Dietz, W. A. Journal of Chromatographic Science, Vol. 5, Issue 2 https://doi.org/10.1093/chromsci/5.2.68	journal	February 1967
Quantitative carbon detector (QCD) for calibration-free, high-resolution characterization of complex mixtures Maduskar, Saurabh; Teixeira, Andrew R.; Paulsen, Alex D. Lab on a Chip, Vol. 15, Issue 2 https://doi.org/10.1039/C4LC01180E	journal	January 2015
Ionization Methods for the Analysis of Gases and Vapors Lovelock, J. E. Analytical Chemistry, Vol. 33, Issue 2 https://doi.org/10.1021/ac60170a003	journal	February 1961
Synthesis of Methane from Water Gas ^1,2 Hightower, Frank W.; White, Alfred H. Industrial & Engineering Chemistry, Vol. 20, Issue 1 https://doi.org/10.1021/ie50217a009	journal	January 1928
Quantitative carbon detector for enhanced detection of molecules in foods, pharmaceuticals, cosmetics, flavors, and fuels Beach, Connor A.; Krumm, Christoph; Spanjers, Charles S. The Analyst, Vol. 141, Issue 5 https://doi.org/10.1039/C5AN02552D	journal	January 2016
Prediction of gas chromatography flame ionization detector response factors from molecular structures Jorgensen, Andrew D.; Picel, Kurt C.; Stamoudis, Vassilis C. Analytical Chemistry, Vol. 62, Issue 7 https://doi.org/10.1021/ac00206a007	journal	April 1990
Estimation of Flame-Ionization Detector Relative Response Factors for Oligomers of Alkyl and Aryl Ether Polyethoxylates using the Effective Carbon Number Concept Jones, F. W. Journal of Chromatographic Science, Vol. 36, Issue 5 https://doi.org/10.1093/chromsci/36.5.223	journal	May 1998
Calculation of Flame Ionization Detector Relative Response Factors Using the Effective Carbon Number Concept Scanlon, J. T.; Willis, D. E. Journal of Chromatographic Science, Vol. 23, Issue 8 https://doi.org/10.1093/chromsci/23.8.333	journal	August 1985
Determination of Carbon Dioxide in the Parts-Per-Million Range With Gas Chromatography Williams, F. W.; Woods, F. J.; Umstead, M. E. Journal of Chromatographic Science, Vol. 10, Issue 9 https://doi.org/10.1093/chromsci/10.9.570	journal	September 1972
Revealing pyrolysis chemistry for biofuels production: Conversion of cellulose to furans and small oxygenates Mettler, Matthew S.; Mushrif, Samir H.; Paulsen, Alex D. Energy Environ. Sci., Vol. 5, Issue 1 https://doi.org/10.1039/C1EE02743C	journal	January 2012
Aspects of the mechanism of the flame ionization detector Holm, Torkil Journal of Chromatography A, Vol. 842, Issue 1-2 https://doi.org/10.1016/S0021-9673(98)00706-7	journal	May 1999
Flame Ionization Detector for Gas Chromatography Harley, J.; Nel, W.; Pretorius, V. Nature, Vol. 181, Issue 4603 https://doi.org/10.1038/181177a0	journal	January 1958

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Complex mixture quantification without calibration using gas chromatography and a comprehensive carbon reactor in conjunction with flame ionization detection Bai, Ling; Carlton, Doug D.; Schug, Kevin A. Journal of Separation Science, Vol. 41, Issue 21 https://doi.org/10.1002/jssc.201800383	journal	October 2018

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