Temperature dependence of field-responsive mechanisms in lead zirconate titanate

Chung, Ching-Chang; Fancher, Chris M.; Isaac, Catherine; Nikkel, Jason; Hennig, Eberhard; Jones, Jacob L.

doi:10.1111/jace.14979

Temperature dependence of field-responsive mechanisms in lead zirconate titanate

Journal Article · Wed May 17 00:00:00 EDT 2017 · Journal of the American Ceramic Society

DOI:https://doi.org/10.1111/jace.14979· OSTI ID:1376454

^[1]; ^[2]; Isaac, Catherine ^[3]; Nikkel, Jason ^[1]; Hennig, Eberhard ^[4]; Jones, Jacob L. ^[1]

North Carolina State Univ., Raleigh, NC (United States). Dept. of Materials Science and Engineering
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Neutron Scattering Science Directorate
Univ. of New South Wales, Sydney, NSW (Australia). Dept. of Materials Science and Engineering
PI Ceramic GmbH, Lederhose (Germany)

An electric field loading stage was designed for use in a laboratory diffractometer that enables in situ investigations of the temperature dependence in the field response mechanisms of ferroelectric materials. The stage was demonstrated in this paper by measuring PbZr_1-xTi_xO₃ (PZT) based materials—a commercially available PZT and a 1% Nb-doped PbZr_0.56Ti_0.44O₃ (PZT 56/44)—over a temperature range of 25°C to 250°C. The degree of non-180° domain alignment (η₀₀₂) of the PZT as a function of temperature was quantified. η₀₀₂ of the commercially available PZT increases exponentially with temperature, and was analyzed as a thermally activated process as described by the Arrhenius law. The activation energy for thermally activated domain wall depinning process in PZT was found to be 0.47 eV. Additionally, a field-induced rhombohedral to tetragonal phase transition was observed 5°C below the rhombohedral-tetragonal transition in PZT 56/44 ceramic. The field-induced tetragonal phase fraction was increased 41.8% after electrical cycling. Finally, a large amount of domain switching (η₀₀₂=0.45 at 1.75 kV/mm) was observed in the induced tetragonal phase.

View Accepted Manuscript (DOE)

Research Organization:: North Carolina State Univ., Raleigh, NC (United States); Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE Office of Science (SC); National Science Foundation (NSF) (United States); State of North Carolina (United States)

Contributing Organization:: Univ. of New South Wales, Sydney, NSW (Australia); PI Ceramic GmbH, Lederhose (Germany)

Grant/Contract Number:: AC05-00OR22725; AC02-06CH11357

OSTI ID:: 1376454

Alternate ID(s):: OSTI ID: 1608885
OSTI ID: 1378387

Journal Information:: Journal of the American Ceramic Society, Journal Name: Journal of the American Ceramic Society Journal Issue: 9 Vol. 100; ISSN 0002-7820

Publisher:: American Ceramic SocietyCopyright Statement

Country of Publication:: United States

Language:: English

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