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Polymeric molecular sieve membranes for gas separation

Patent ·
OSTI ID:1375236

A porous polymer membrane useful in gas separation, the porous polymer membrane comprising a polymeric structure having crosslinked aromatic groups and a hierarchical porosity in which micropores having a pore size less than 2 nm are present at least in an outer layer of the porous polymer membrane, and macropores having a pore size of over 50 nm are present at least in an inner layer of the porous polymer membrane. Also described are methods for producing the porous polymer membrane in which a non-porous polymer membrane containing aromatic rings is subjected to a Friedel-Crafts crosslinking reaction in which a crosslinking molecule crosslinks the aromatic rings in the presence of a Friedel-Crafts catalyst and organic solvent under sufficiently elevated temperature, as well as methods for using the porous polymer membranes for gas or liquid separation, filtration, or purification.

Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC05-00OR22725
Assignee:
UT-BATTELLE, LLC
Patent Number(s):
9,731,249
Application Number:
14/667,968
OSTI ID:
1375236
Country of Publication:
United States
Language:
English

References (9)

Polymers of intrinsic microporosity (PIMs): organic materials for membrane separations, heterogeneous catalysis and hydrogen storage journal January 2006
Solution-Processed, Organophilic Membrane Derived from a Polymer of Intrinsic Microporosity journal March 2004
Nanoporous organic polymer networks journal April 2012
A Superacid-Catalyzed Synthesis of Porous Membranes Based on Triazine Frameworks for CO2 Separation journal June 2012
Preparation of free-standing high quality mesoporous carbon membranes journal February 2010
Polymers of Intrinsic Microporosity (PIMs): Bridging the Void between Microporous and Polymeric Materials journal April 2005
An Efficient Polymer Molecular Sieve for Membrane Gas Separations journal January 2013
Porous, Crystalline, Covalent Organic Frameworks journal November 2005
Conjugated Microporous Polymers journal March 2009

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