Investigation of High-Energy Ion-Irradiated MA957 Using Synchrotron Radiation under In-Situ Tension

Mo, Kun; Yun, Di; Miao, Yinbin; Liu, Xiang; Pellin, Michael; Almer, Jonathan; Park, Jun-Sang; Stubbins, James; Zhu, Shaofei; Yacout, Abdellatif

doi:10.3390/ma9010015

Title: Investigation of High-Energy Ion-Irradiated MA957 Using Synchrotron Radiation under In-Situ Tension

Journal Article · Sat Jan 02 00:00:00 EST 2016 · Materials

DOI:https://doi.org/10.3390/ma9010015· OSTI ID:1419362

Mo, Kun; Yun, Di; Miao, Yinbin; Liu, Xiang; Pellin, Michael; Almer, Jonathan; Park, Jun-Sang; Stubbins, James; Zhu, Shaofei; Yacout, Abdellatif

In this paper, an MA957 oxide dispersion-strengthened (ODS) alloy was irradiated with high-energy ions in the Argonne Tandem Linac Accelerator System. Fe ions at an energy of 84 MeV bombarded MA957 tensile specimens, creating a damage region similar to 7.5 μm in depth; the peak damage (similar to 40 dpa) was estimated to be at similar to 7 μm from the surface. Following the irradiation, in-situ high-energy X-ray diffraction measurements were performed at the Advanced Photon Source in order to study the dynamic deformation behavior of the specimens after ion irradiation damage. In-situ X-ray measurements taken during tensile testing of the ion-irradiated MA957 revealed a difference in loading behavior between the irradiated and un-irradiated regions of the specimen. At equivalent applied stresses, lower lattice strains were found in the radiation-damaged region than those in the un-irradiated region. This might be associated with a higher level of Type II stresses as a result of radiation hardening. The study has demonstrated the feasibility of combining high-energy ion radiation and high-energy synchrotron X-ray diffraction to study materials' radiation damage in a dynamic manner.

View Journal Article

Cite

Export

Save

Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC-02-06CH11357; AC02-06CH11357

OSTI ID:: 1419362

Alternate ID(s):: OSTI ID: 1357253

Journal Information:: Materials, Journal Name: Materials Vol. 9 Journal Issue: 12; ISSN 1996-1944

Publisher:: MDPI AGCopyright Statement

Country of Publication:: Switzerland

Language:: English

Citation Metrics:

Cited by: 10 works

Citation information provided by
Web of Science

References (46)

Correlation between chemical composition and size of very small oxide particles in the MA957 ODS ferritic alloy Sakasegawa, H.; Chaffron, L.; Legendre, F. Journal of Nuclear Materials, Vol. 384, Issue 2 https://doi.org/10.1016/j.jnucmat.2008.11.001	journal	February 2009
The transport and fate of helium in nanostructured ferritic alloys at fusion relevant He/dpa ratios and dpa rates Yamamoto, T.; Odette, G. R.; Miao, P. Journal of Nuclear Materials, Vol. 367-370 https://doi.org/10.1016/j.jnucmat.2007.03.047	journal	August 2007
A critical stress–critical area statistical model of the curve for MA957 in the cleavage transition Yang, W. J.; Odette, G. R.; Yamamoto, T. Journal of Nuclear Materials, Vol. 367-370 https://doi.org/10.1016/j.jnucmat.2007.03.203	journal	August 2007
Emulation of reactor irradiation damage using ion beams Was, G. S.; Jiao, Z.; Getto, E. Scripta Materialia, Vol. 88 https://doi.org/10.1016/j.scriptamat.2014.06.003	journal	October 2014
A review of refractory metal alloys and mechanically alloyed-oxide dispersion strengthened steels for space nuclear power systems El-Genk, Mohamed S.; Tournier, Jean-Michel Journal of Nuclear Materials, Vol. 340, Issue 1 https://doi.org/10.1016/j.jnucmat.2004.10.118	journal	April 2005
Ion-induced swelling of ODS ferritic alloy MA957 tubing to 500 dpa Toloczko, M. B.; Garner, F. A.; Voyevodin, V. N. Journal of Nuclear Materials, Vol. 453, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2014.06.011	journal	October 2014
Recent Developments in Irradiation-Resistant Steels Odette, G. R.; Alinger, M. J.; Wirth, B. D. Annual Review of Materials Research, Vol. 38, Issue 1, p. 471-503 https://doi.org/10.1146/annurev.matsci.38.060407.130315	journal	August 2008
Load partitioning between ferrite and cementite during elasto-plastic deformation of an ultrahigh-carbon steel Young, M. L.; Almer, J. D.; Daymond, M. R. Acta Materialia, Vol. 55, Issue 6 https://doi.org/10.1016/j.actamat.2006.11.004	journal	April 2007
Core/shell structures of oxygen-rich nanofeatures in oxide-dispersion strengthened Fe–Cr alloys Marquis, Emmanuelle A. Applied Physics Letters, Vol. 93, Issue 18, Article No. 181904 https://doi.org/10.1063/1.3000965	journal	November 2008
Nano-cluster stability following neutron irradiation in MA957 oxide dispersion strengthened material Ribis, J.; Lozano-Perez, S. Journal of Nuclear Materials, Vol. 444, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2013.10.010	journal	January 2014
Effect of neutron irradiation on nanoclusters in MA957 ferritic alloys Miller, M. K.; Hoelzer, D. T. Journal of Nuclear Materials, Vol. 418, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2011.07.031	journal	November 2011
Structural and chemical matrix evolution following neutron irradiation in a MA957 oxide dispersion strengthened material Ribis, J. Journal of Nuclear Materials, Vol. 434, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2012.11.038	journal	March 2013
A Monte Carlo computer program for the transport of energetic ions in amorphous targets Biersack, J. P.; Haggmark, L. G. Nuclear Instruments and Methods, Vol. 174, Issue 1-2, p. 257-269 https://doi.org/10.1016/0029-554X(80)90440-1	journal	August 1980
In situ characterization of Grade 92 steel during tensile deformation using concurrent high energy X-ray diffraction and small angle X-ray scattering Wang, Leyun; Li, Meimei; Almer, Jonathan Journal of Nuclear Materials, Vol. 440, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2013.04.063	journal	September 2013
Stability of ferritic MA/ODS alloys at high temperatures Miller, M. K.; Hoelzer, D. T.; Kenik, E. A. Intermetallics, Vol. 13, Issue 3-4 https://doi.org/10.1016/j.intermet.2004.07.036	journal	March 2005
High-energy X-ray optics with silicon saw-tooth refractive lenses Shastri, S. D.; Almer, J.; Ribbing, C. Journal of Synchrotron Radiation, Vol. 14, Issue 2 https://doi.org/10.1107/S0909049507003962	journal	February 2007
An assessment of the contributing factors to the superior properties of a nanostructured steel using in situ high-energy X-ray diffraction Cheng, S.; Wang, Y. D.; Choo, H. Acta Materialia, Vol. 58, Issue 7 https://doi.org/10.1016/j.actamat.2009.12.028	journal	April 2010
Irradiation creep and density changes observed in MA957 pressurized tubes irradiated to doses of 40–110dpa at 400–750°C in FFTF Toloczko, M. B.; Garner, F. A.; Maloy, S. A. Journal of Nuclear Materials, Vol. 428, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2012.04.005	journal	September 2012
Introduction to two-dimensional X-ray diffraction He, Bob Baoping Powder Diffraction, Vol. 18, Issue 2 https://doi.org/10.1154/1.1577355	journal	June 2003
Lattice swelling and modulus change in a helium-implanted tungsten alloy: X-ray micro-diffraction, surface acoustic wave measurements, and multiscale modelling Hofmann, F.; Nguyen-Manh, D.; Gilbert, M. R. Acta Materialia, Vol. 89 https://doi.org/10.1016/j.actamat.2015.01.055	journal	May 2015
The determination of a continuum mechanics equivalent elastic strain from the analysis of multiple diffraction peaks Daymond, Mark R. Journal of Applied Physics, Vol. 96, Issue 8 https://doi.org/10.1063/1.1794896	journal	October 2004
Load partitioning between ferrite/martensite and dispersed nanoparticles of a 9Cr ferritic/martensitic (F/M) ODS steel at high temperatures Zhang, Guangming; Mo, Kun; Miao, Yinbin Materials Science and Engineering: A, Vol. 637 https://doi.org/10.1016/j.msea.2015.04.037	journal	June 2015
Atom probe tomography analysis of high dose MA957 at selected irradiation temperatures Bailey, Nathan A.; Stergar, Erich; Toloczko, Mychailo Journal of Nuclear Materials, Vol. 459 https://doi.org/10.1016/j.jnucmat.2015.01.006	journal	April 2015
Load sharing in tungsten fiber reinforced Kanthal composites Clausen, B.; Bourke, Mark A. M.; Brown, Donald W. Materials Science and Engineering: A, Vol. 421, Issue 1-2 https://doi.org/10.1016/j.msea.2005.10.004	journal	April 2006
Microstructure and impact properties of ferritic ODS ODM401 (14%Cr-ODS of MA957 type) Hadraba, Hynek; Kazimierzak, Bohumil; Stratil, Ludek Journal of Nuclear Materials, Vol. 417, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2011.01.066	journal	October 2011
On the role of alloy composition and processing parameters in nanocluster formation and dispersion strengthening in nanostuctured ferritic alloys Alinger, M. J.; Odette, G. R.; Hoelzer, D. T. Acta Materialia, Vol. 57, Issue 2 https://doi.org/10.1016/j.actamat.2008.09.025	journal	January 2009
Lattice strain and damage evolution of 9–12%Cr ferritic/martensitic steel during in situ tensile test by X-ray diffraction and small angle scattering Pan, Xiao; Wu, Xianglin; Mo, Kun Journal of Nuclear Materials, Vol. 407, Issue 1 https://doi.org/10.1016/j.jnucmat.2010.07.003	journal	December 2010
Lattice strain evolution during uniaxial tensile loading of stainless steel Clausen, Bjørn; Lorentzen, Torben; Bourke, Mark A. M. Materials Science and Engineering: A, Vol. 259, Issue 1 https://doi.org/10.1016/S0921-5093(98)00878-8	journal	January 1999
In situ synchrotron tensile investigations on the phase responses within an oxide dispersion-strengthened (ODS) 304 steel Miao, Yinbin; Mo, Kun; Zhou, Zhangjian Materials Science and Engineering: A, Vol. 625 https://doi.org/10.1016/j.msea.2014.12.017	journal	February 2015
Irradiation creep and swelling from 400 to 600 °C of the oxide dispersion strengthened ferritic alloy MA957 Toloczko, M. B.; Gelles, D. S.; Garner, F. A. Journal of Nuclear Materials, Vol. 329-333 https://doi.org/10.1016/j.jnucmat.2004.04.296	journal	August 2004
On the use of SRIM for computing radiation damage exposure Stoller, R. E.; Toloczko, M. B.; Was, G. S. Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 310 https://doi.org/10.1016/j.nimb.2013.05.008	journal	September 2013
Synchrotron study on load partitioning between ferrite/martensite and nanoparticles of a 9Cr ODS steel Mo, Kun; Zhou, Zhangjian; Miao, Yinbin Journal of Nuclear Materials, Vol. 455, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2014.06.060	journal	December 2014
Stability of non-stoichiometric clusters in the MA957 ODS ferrtic alloy Sakasegawa, H.; Legendre, F.; Boulanger, L. Journal of Nuclear Materials, Vol. 417, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2010.12.056	journal	October 2011
On the microstructure and strengthening mechanism in oxide dispersion-strengthened 316 steel: A coordinated electron microscopy, atom probe tomography and in situ synchrotron tensile investigation Miao, Yinbin; Mo, Kun; Zhou, Zhangjian Materials Science and Engineering: A, Vol. 639 https://doi.org/10.1016/j.msea.2015.05.064	journal	July 2015
Deformation and damage processes during creep of Incoloy MA957 Wilshire, B.; Lieu, T. Materials Science and Engineering A, Vol. 386, Issue 1-2 https://doi.org/10.1016/S0921-5093(04)00969-4	journal	November 2004
In situ synchrotron tensile investigations on 14YWT, MA957, and 9-Cr ODS alloys Lin, Jun-Li; Mo, Kun; Yun, Di Journal of Nuclear Materials, Vol. 471 https://doi.org/10.1016/j.jnucmat.2015.10.049	journal	April 2016
Microstructural changes and void swelling of a 12Cr ODS ferritic-martensitic alloy after high-dpa self-ion irradiation Chen, Tianyi; Aydogan, Eda; Gigax, Jonathan G. Journal of Nuclear Materials, Vol. 467 https://doi.org/10.1016/j.jnucmat.2015.09.016	journal	December 2015
The evolution of internal stress and dislocation during tensile deformation in a 9Cr ferritic/martensitic (F/M) ODS steel investigated by high-energy X-rays Zhang, Guangming; Zhou, Zhangjian; Mo, Kun Journal of Nuclear Materials, Vol. 467 https://doi.org/10.1016/j.jnucmat.2015.09.014	journal	December 2015
Use of Rietveld refinement for elastic macrostrain determination and for evaluation of plastic strain history from diffraction spectra Daymond, M. R.; Bourke, M. A. M.; Von Dreele, R. B. Journal of Applied Physics, Vol. 82, Issue 4 https://doi.org/10.1063/1.365956	journal	August 1997
Investigation of deformation and microstructural evolution in Grade 91 ferritic–martensitic steel by in situ high-energy X-rays Wang, Leyun; Li, Meimei; Almer, Jonathan Acta Materialia, Vol. 62 https://doi.org/10.1016/j.actamat.2013.10.003	journal	January 2014
Transmission electron microscopy characterization of the nanofeatures in nanostructured ferritic alloy MA957 Wu, Y.; Haney, E. M.; Cunningham, N. J. Acta Materialia, Vol. 60, Issue 8 https://doi.org/10.1016/j.actamat.2012.03.012	journal	May 2012
Load Partitioning and Strain-Induced Martensite Formation during Tensile Loading of a Metastable Austenitic Stainless Steel Hedström, P.; Lindgren, L. E.; Almer, J. Metallurgical and Materials Transactions A, Vol. 40, Issue 5 https://doi.org/10.1007/s11661-009-9807-3	journal	March 2009
Tensile and fracture toughness properties of MA957: implications to the development of nanocomposited ferritic alloys Alinger, M. J.; Odette, G. R.; Lucas, G. E. Journal of Nuclear Materials, Vol. 307-311 https://doi.org/10.1016/S0022-3115(02)01220-5	journal	December 2002
Synchrotron Radiation Study on Alloy 617 and Alloy 230 for VHTR Application Mo, Kun; Tung, Hsiao-Ming; Almer, Jonathon Journal of Pressure Vessel Technology, Vol. 135, Issue 2 https://doi.org/10.1115/1.4007041	journal	March 2013
Temperature-dependent elastic anisotropy and mesoscale deformation in a nanostructured ferritic alloy Stoica, G. M.; Stoica, A. D.; Miller, M. K. Nature Communications, Vol. 5, Issue 1 https://doi.org/10.1038/ncomms6178	journal	October 2014
Dislocation evolution during tensile deformation in ferritic–martensitic steels revealed by high-energy X-rays Li, Meimei; Wang, Leyun; Almer, Jonathan D. Acta Materialia, Vol. 76 https://doi.org/10.1016/j.actamat.2014.05.026	journal	September 2014

Cited By (1)

Effects of Zr Addition on Strengthening Mechanisms of Al-Alloyed High-Cr ODS Steels Ren, Jian; Yu, Liming; Liu, Yongchang Materials, Vol. 11, Issue 1 https://doi.org/10.3390/ma11010118	journal	January 2018

Similar Records

Fabrication technological development of the oxide dispersion strengthened alloy MA957 for fast reactor applications

Technical Report · Mon Mar 27 00:00:00 EST 2000 · OSTI ID:1419362

Hamilton, ML; Gelles, DS; Lobsinger, RJ; +7 more

In-situ high-energy X-ray characterization of neutron irradiated HT-UPS stainless steel under tensile deformation

Journal Article · Fri Jul 06 00:00:00 EDT 2018 · Acta Materialia · OSTI ID:1419362

Xu, Chi; Zhang, Xuan; Chen, Yiren; +5 more

In situ high-energy X-ray diffraction study of tensile deformation of neutron-irradiated polycrystalline Fe-9%Cr alloy

Journal Article · Fri Dec 30 00:00:00 EST 2016 · Acta Materialia · OSTI ID:1419362

Zhang, Xuan; Li, Meimei; Park, Jun -Sang; +4 more

Related Subjects

36 MATERIALS SCIENCE
43 PARTICLE ACCELERATORS
in situ tensile test
oxide dispersion-strengthened (ODS)
ion irradiation
synchrotron radiation

Title: Investigation of High-Energy Ion-Irradiated MA957 Using Synchrotron Radiation under In-Situ Tension

Citation Formats

References (46)

Cited By (1)

Similar Records

Related Subjects