Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging

doi:https://doi.org/10.1103/PhysRevLett.117.225501

Title: Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging

Abstract

Here, we present and demonstrate a formalism by which three-dimensional (3D) Bragg x-ray coherent diffraction imaging (BCDI) can be implemented without moving the sample by scanning the energy of the incident x-ray beam. This capability is made possible by introducing a 3D Fourier transform that accounts for x-ray wavelength variability. We also demonstrate the approach by inverting coherent Bragg diffraction patterns from a gold nanocrystal measured with an x-ray energy scan. Furthermore, variable-wavelength BCDI will expand the breadth of feasible in situ 3D strain imaging experiments towards more diverse materials environments, especially where sample manipulation is difficult.

Authors:

Cha, W. ^[1]; Ulvestad, A. ^[1]; Allain, M. ^[2]; Chamard, V. ^[2]; Harder, R. ^[3]; Leake, S. J. ^[4]; Maser, J. ^[3]; Fuoss, P. H. ^[1]; Hruszkewycz, S. O. ^[1]

Argonne National Lab. (ANL), Argonne, IL (United States). Materials Science Division
Aix-Marseille Univ., and CNRS/IN2P3, Marseille (France)
Argonne National Lab. (ANL), Argonne, IL (United States). X-ray Science Division
European Synchrotron Radiation Facility (ESRF), Grenoble (France)

Publication Date:: 2016-11-23

Research Org.:: Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

OSTI Identifier:: 1352631

Alternate Identifier(s):: OSTI ID: 1333338

Grant/Contract Number:: AC02-06CH11357

Resource Type:: Journal Article: Accepted Manuscript

Journal Name:: Physical Review Letters

Additional Journal Information:: Journal Volume: 117; Journal Issue: 22; Journal ID: ISSN 0031-9007

Publisher:: American Physical Society (APS)

Country of Publication:: United States

Language:: English

Subject:: 73 NUCLEAR PHYSICS AND RADIATION PHYSICS

Citation Formats


                    Cha, W., Ulvestad, A., Allain, M., Chamard, V., Harder, R., Leake, S. J., Maser, J., Fuoss, P. H., and Hruszkewycz, S. O. Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging.  United States: N. p., 2016. 
        Web.  doi:10.1103/PhysRevLett.117.225501.

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                    Cha, W., Ulvestad, A., Allain, M., Chamard, V., Harder, R., Leake, S. J., Maser, J., Fuoss, P. H., & Hruszkewycz, S. O. Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging.  United States.  https://doi.org/10.1103/PhysRevLett.117.225501

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                    Cha, W., Ulvestad, A., Allain, M., Chamard, V., Harder, R., Leake, S. J., Maser, J., Fuoss, P. H., and Hruszkewycz, S. O. Wed .  
        "Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging".  United States.  https://doi.org/10.1103/PhysRevLett.117.225501.  https://www.osti.gov/servlets/purl/1352631.

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@article{osti_1352631,

  title        = {Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging},

  author       = {Cha, W. and Ulvestad, A. and Allain, M. and Chamard, V. and Harder, R. and Leake, S. J. and Maser, J. and Fuoss, P. H. and Hruszkewycz, S. O.},

  abstractNote = {Here, we present and demonstrate a formalism by which three-dimensional (3D) Bragg x-ray coherent diffraction imaging (BCDI) can be implemented without moving the sample by scanning the energy of the incident x-ray beam. This capability is made possible by introducing a 3D Fourier transform that accounts for x-ray wavelength variability. We also demonstrate the approach by inverting coherent Bragg diffraction patterns from a gold nanocrystal measured with an x-ray energy scan. Furthermore, variable-wavelength BCDI will expand the breadth of feasible in situ 3D strain imaging experiments towards more diverse materials environments, especially where sample manipulation is difficult.},

  doi          = {10.1103/PhysRevLett.117.225501},

  url          = {https://www.osti.gov/biblio/1352631},
  journal      = {Physical Review Letters},

  issn         = {0031-9007},

  number       = 22,

  volume       = 117,

  place        = {United States},

  year         = {2016},

  month        = {11}

}

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Elastic strain engineering for unprecedented materials properties
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Works referencing / citing this record:

Variable‐Wavelength Quick Scanning Nanofocused X‐Ray Microscopy for In Situ Strain and Tilt Mapping
journal, January 2020

Richard, Marie‐Ingrid; Cornelius, Thomas W.; Lauraux, Florian
Small, Vol. 16, Issue 6
https://doi.org/10.1002/smll.201905990

Sparse recovery of undersampled intensity patterns for coherent diffraction imaging at high X-ray energies
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Maddali, S.; Calvo-Almazan, I.; Almer, J.
Scientific Reports, Vol. 8, Issue 1
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Multi-wavelength Bragg coherent X-ray diffraction imaging of Au particles
journal, February 2020

Lauraux, F.; Cornelius, T. W.; Labat, S.
Journal of Applied Crystallography, Vol. 53, Issue 1
https://doi.org/10.1107/s1600576719017163

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Similar Records

Title: Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging

Abstract

Citation Formats

Imaging transient melting of a nanocrystal using an X-ray laser journal, June 2015

Partial coherence effects on the imaging of small crystals using coherent x-ray diffraction journal, November 2001

Noise models for low counting rate coherent diffraction imaging journal, January 2012

Three-dimensional mapping of a deformation field inside a nanocrystal journal, July 2006

Differential stress induced by thiol adsorption on facetted nanocrystals journal, September 2011

Signature of dislocations and stacking faults of face-centred cubic nanocrystals in coherent X-ray diffraction patterns: a numerical study journal, April 2015

Maximum-likelihood refinement for coherent diffractive imaging journal, June 2012

Coherent X-ray diffraction imaging of strain at the nanoscale journal, April 2009

Core–shell strain structure of zeolite microcrystals journal, July 2013

Topological defect dynamics in operando battery nanoparticles journal, June 2015

Anomalous coherent diffraction of core-shell nano-objects: A methodology for determination of composition and strain fields journal, January 2013

Elastic strain engineering for unprecedented materials properties journal, February 2014

Utilizing broadband X-rays in a Bragg coherent X-ray diffraction imaging experiment journal, July 2016

Invited Article: A unified evaluation of iterative projection algorithms for phase retrieval journal, January 2007

Reconstruction of the Shapes of Gold Nanocrystals Using Coherent X-Ray Diffraction journal, October 2001

Orientation variation of surface strain journal, September 2007

Efficient modeling of Bragg coherent x-ray nanobeam diffraction journal, January 2015

In situ three-dimensional reciprocal-space mapping during mechanical deformation journal, July 2012

Three-dimensional diffraction mapping by tuning the X-ray energy journal, March 2011

Lensless imaging using broadband X-ray sources journal, June 2011

Phase retrieval algorithms: a comparison journal, January 1982

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Sparse recovery of undersampled intensity patterns for coherent diffraction imaging at high X-ray energies journal, March 2018

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Imaging transient melting of a nanocrystal using an X-ray laser
journal, June 2015

Partial coherence effects on the imaging of small crystals using coherent x-ray diffraction
journal, November 2001

Noise models for low counting rate coherent diffraction imaging
journal, January 2012

Three-dimensional mapping of a deformation field inside a nanocrystal
journal, July 2006

Differential stress induced by thiol adsorption on facetted nanocrystals
journal, September 2011

Signature of dislocations and stacking faults of face-centred cubic nanocrystals in coherent X-ray diffraction patterns: a numerical study
journal, April 2015

Maximum-likelihood refinement for coherent diffractive imaging
journal, June 2012

Coherent X-ray diffraction imaging of strain at the nanoscale
journal, April 2009

Core–shell strain structure of zeolite microcrystals
journal, July 2013

Topological defect dynamics in operando battery nanoparticles
journal, June 2015

Anomalous coherent diffraction of core-shell nano-objects: A methodology for determination of composition and strain fields
journal, January 2013

Elastic strain engineering for unprecedented materials properties
journal, February 2014

Utilizing broadband X-rays in a Bragg coherent X-ray diffraction imaging experiment
journal, July 2016

Invited Article: A unified evaluation of iterative projection algorithms for phase retrieval
journal, January 2007

Reconstruction of the Shapes of Gold Nanocrystals Using Coherent X-Ray Diffraction
journal, October 2001

Orientation variation of surface strain
journal, September 2007

Efficient modeling of Bragg coherent x-ray nanobeam diffraction
journal, January 2015

In situ three-dimensional reciprocal-space mapping during mechanical deformation
journal, July 2012

Three-dimensional diffraction mapping by tuning the X-ray energy
journal, March 2011

Lensless imaging using broadband X-ray sources
journal, June 2011

Phase retrieval algorithms: a comparison
journal, January 1982

Variable‐Wavelength Quick Scanning Nanofocused X‐Ray Microscopy for In Situ Strain and Tilt Mapping
journal, January 2020

Sparse recovery of undersampled intensity patterns for coherent diffraction imaging at high X-ray energies
journal, March 2018

Multi-wavelength Bragg coherent X-ray diffraction imaging of Au particles
journal, February 2020