Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging

Cha, W.; Ulvestad, A.; Allain, M.; Chamard, V.; Harder, R.; Leake, S. J.; Maser, J.; Fuoss, P. H.; Hruszkewycz, S. O.

doi:10.1103/PhysRevLett.117.225501

Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging

Journal Article · Wed Nov 23 00:00:00 EST 2016 · Physical Review Letters

DOI:https://doi.org/10.1103/PhysRevLett.117.225501· OSTI ID:1352631

Cha, W. ^[1]; Ulvestad, A. ^[1]; Allain, M. ^[2]; Chamard, V. ^[2]; Harder, R. ^[3]; Leake, S. J. ^[4]; Maser, J. ^[3]; Fuoss, P. H. ^[1]; Hruszkewycz, S. O. ^[1]

Argonne National Lab. (ANL), Argonne, IL (United States). Materials Science Division
Aix-Marseille Univ., and CNRS/IN2P3, Marseille (France)
Argonne National Lab. (ANL), Argonne, IL (United States). X-ray Science Division
European Synchrotron Radiation Facility (ESRF), Grenoble (France)

Here, we present and demonstrate a formalism by which three-dimensional (3D) Bragg x-ray coherent diffraction imaging (BCDI) can be implemented without moving the sample by scanning the energy of the incident x-ray beam. This capability is made possible by introducing a 3D Fourier transform that accounts for x-ray wavelength variability. We also demonstrate the approach by inverting coherent Bragg diffraction patterns from a gold nanocrystal measured with an x-ray energy scan. Furthermore, variable-wavelength BCDI will expand the breadth of feasible in situ 3D strain imaging experiments towards more diverse materials environments, especially where sample manipulation is difficult.

View Accepted Manuscript (DOE)

Research Organization:: Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1352631

Alternate ID(s):: OSTI ID: 1333338

Journal Information:: Physical Review Letters, Journal Name: Physical Review Letters Journal Issue: 22 Vol. 117; ISSN 0031-9007; ISSN PRLTAO

Publisher:: American Physical Society (APS)Copyright Statement

Country of Publication:: United States

Language:: English

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Cited By (7)

Variable‐Wavelength Quick Scanning Nanofocused X‐Ray Microscopy for In Situ Strain and Tilt Mapping Richard, Marie‐Ingrid; Cornelius, Thomas W.; Lauraux, Florian Small, Vol. 16, Issue 6 https://doi.org/10.1002/smll.201905990	journal	January 2020
X-ray Microscopy Jacobsen, Chris Cambridge University Press https://doi.org/10.1017/9781139924542	book	January 2019
Sparse recovery of undersampled intensity patterns for coherent diffraction imaging at high X-ray energies Maddali, S.; Calvo-Almazan, I.; Almer, J. Scientific Reports, Vol. 8, Issue 1 https://doi.org/10.1038/s41598-018-23040-y	journal	March 2018
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Multi-wavelength Bragg coherent X-ray diffraction imaging of Au particles Lauraux, F.; Cornelius, T. W.; Labat, S. Journal of Applied Crystallography, Vol. 53, Issue 1 https://doi.org/10.1107/s1600576719017163	journal	February 2020
X-ray microscopy Lider, V. V. Physics-Uspekhi, Vol. 60, Issue 2 https://doi.org/10.3367/ufne.2016.06.037830	journal	February 2017
Sparse recovery of undersampled intensity patterns for coherent diffraction imaging at high X-ray energies Maddali, Siddharth; Calvo-Almazan, Irene; Almer, Jonathan arXiv https://doi.org/10.48550/arxiv.1712.01108	text	January 2017

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