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Title: Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging

Abstract

Here, we present and demonstrate a formalism by which three-dimensional (3D) Bragg x-ray coherent diffraction imaging (BCDI) can be implemented without moving the sample by scanning the energy of the incident x-ray beam. This capability is made possible by introducing a 3D Fourier transform that accounts for x-ray wavelength variability. We also demonstrate the approach by inverting coherent Bragg diffraction patterns from a gold nanocrystal measured with an x-ray energy scan. Furthermore, variable-wavelength BCDI will expand the breadth of feasible in situ 3D strain imaging experiments towards more diverse materials environments, especially where sample manipulation is difficult.

Authors:
 [1];  [1];  [2];  [2];  [3];  [4];  [3];  [1];  [1]
  1. Argonne National Lab. (ANL), Argonne, IL (United States). Materials Science Division
  2. Aix-Marseille Univ., and CNRS/IN2P3, Marseille (France)
  3. Argonne National Lab. (ANL), Argonne, IL (United States). X-ray Science Division
  4. European Synchrotron Radiation Facility (ESRF), Grenoble (France)
Publication Date:
Research Org.:
Argonne National Lab. (ANL), Argonne, IL (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
OSTI Identifier:
1352631
Alternate Identifier(s):
OSTI ID: 1333338
Grant/Contract Number:  
AC02-06CH11357
Resource Type:
Journal Article: Accepted Manuscript
Journal Name:
Physical Review Letters
Additional Journal Information:
Journal Volume: 117; Journal Issue: 22; Journal ID: ISSN 0031-9007
Publisher:
American Physical Society (APS)
Country of Publication:
United States
Language:
English
Subject:
73 NUCLEAR PHYSICS AND RADIATION PHYSICS

Citation Formats

Cha, W., Ulvestad, A., Allain, M., Chamard, V., Harder, R., Leake, S. J., Maser, J., Fuoss, P. H., and Hruszkewycz, S. O. Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging. United States: N. p., 2016. Web. doi:10.1103/PhysRevLett.117.225501.
Cha, W., Ulvestad, A., Allain, M., Chamard, V., Harder, R., Leake, S. J., Maser, J., Fuoss, P. H., & Hruszkewycz, S. O. Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging. United States. https://doi.org/10.1103/PhysRevLett.117.225501
Cha, W., Ulvestad, A., Allain, M., Chamard, V., Harder, R., Leake, S. J., Maser, J., Fuoss, P. H., and Hruszkewycz, S. O. Wed . "Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging". United States. https://doi.org/10.1103/PhysRevLett.117.225501. https://www.osti.gov/servlets/purl/1352631.
@article{osti_1352631,
title = {Three Dimensional Variable-Wavelength X-Ray Bragg Coherent Diffraction Imaging},
author = {Cha, W. and Ulvestad, A. and Allain, M. and Chamard, V. and Harder, R. and Leake, S. J. and Maser, J. and Fuoss, P. H. and Hruszkewycz, S. O.},
abstractNote = {Here, we present and demonstrate a formalism by which three-dimensional (3D) Bragg x-ray coherent diffraction imaging (BCDI) can be implemented without moving the sample by scanning the energy of the incident x-ray beam. This capability is made possible by introducing a 3D Fourier transform that accounts for x-ray wavelength variability. We also demonstrate the approach by inverting coherent Bragg diffraction patterns from a gold nanocrystal measured with an x-ray energy scan. Furthermore, variable-wavelength BCDI will expand the breadth of feasible in situ 3D strain imaging experiments towards more diverse materials environments, especially where sample manipulation is difficult.},
doi = {10.1103/PhysRevLett.117.225501},
url = {https://www.osti.gov/biblio/1352631}, journal = {Physical Review Letters},
issn = {0031-9007},
number = 22,
volume = 117,
place = {United States},
year = {2016},
month = {11}
}

Journal Article:

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Cited by: 1 work
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Works referenced in this record:

Imaging transient melting of a nanocrystal using an X-ray laser
journal, June 2015


Partial coherence effects on the imaging of small crystals using coherent x-ray diffraction
journal, November 2001


Noise models for low counting rate coherent diffraction imaging
journal, January 2012


Three-dimensional mapping of a deformation field inside a nanocrystal
journal, July 2006


Differential stress induced by thiol adsorption on facetted nanocrystals
journal, September 2011


Signature of dislocations and stacking faults of face-centred cubic nanocrystals in coherent X-ray diffraction patterns: a numerical study
journal, April 2015


Maximum-likelihood refinement for coherent diffractive imaging
journal, June 2012


Coherent X-ray diffraction imaging of strain at the nanoscale
journal, April 2009


Core–shell strain structure of zeolite microcrystals
journal, July 2013


Topological defect dynamics in operando battery nanoparticles
journal, June 2015


Elastic strain engineering for unprecedented materials properties
journal, February 2014


Utilizing broadband X-rays in a Bragg coherent X-ray diffraction imaging experiment
journal, July 2016


Invited Article: A unified evaluation of iterative projection algorithms for phase retrieval
journal, January 2007


Reconstruction of the Shapes of Gold Nanocrystals Using Coherent X-Ray Diffraction
journal, October 2001


Orientation variation of surface strain
journal, September 2007


Efficient modeling of Bragg coherent x-ray nanobeam diffraction
journal, January 2015


In situ three-dimensional reciprocal-space mapping during mechanical deformation
journal, July 2012


Three-dimensional diffraction mapping by tuning the X-ray energy
journal, March 2011


Lensless imaging using broadband X-ray sources
journal, June 2011


Phase retrieval algorithms: a comparison
journal, January 1982


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    Multi-wavelength Bragg coherent X-ray diffraction imaging of Au particles
    journal, February 2020