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Title: A priori checking of the light-response and data quality before extended data collection in pump–probe photocrystallography experiments

Abstract

In picosecond and slower pump–probe diffraction experiments, collection of response–ratio correlation sets prior to full data collection provides an invaluable confirmation of the existence of a light-induced signal prior to full data collection. If a response to light exposure is observed, the quality of the data being collected can be assessed. We present a number of such correlation plots both for synchrotron and in-house pump–probe data collection.

Authors:
 [1];  [1];  [1]; ORCiD logo [1]; ORCiD logo [1];  [1];  [1]
  1. Univ. at Buffalo, NY (United States). Dept. of Chemistry
Publication Date:
Research Org.:
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22); National Science Foundation (NSF)
OSTI Identifier:
1345412
DOE Contract Number:  
W-31-109-ENG-38; NSF/CHE-1346572
Resource Type:
Journal Article
Resource Relation:
Journal Name: Acta Crystallographica. Section B, Structural Science, Crystal Engineering and Materials (Online); Journal Volume: 73; Journal Issue: 1
Country of Publication:
United States
Language:
ENGLISH

Citation Formats

Coppens, Philip, Makal, Anna, Fournier, Bertrand, Jarzembska, Katarzyna N., Kamiński, Radosław, Basuroy, Krishnayan, and Trzop, Elzbieta. A priori checking of the light-response and data quality before extended data collection in pump–probe photocrystallography experiments. United States: N. p., 2017. Web. doi:10.1107/S2052520616017558.
Coppens, Philip, Makal, Anna, Fournier, Bertrand, Jarzembska, Katarzyna N., Kamiński, Radosław, Basuroy, Krishnayan, & Trzop, Elzbieta. A priori checking of the light-response and data quality before extended data collection in pump–probe photocrystallography experiments. United States. doi:10.1107/S2052520616017558.
Coppens, Philip, Makal, Anna, Fournier, Bertrand, Jarzembska, Katarzyna N., Kamiński, Radosław, Basuroy, Krishnayan, and Trzop, Elzbieta. Mon . "A priori checking of the light-response and data quality before extended data collection in pump–probe photocrystallography experiments". United States. doi:10.1107/S2052520616017558.
@article{osti_1345412,
title = {A priori checking of the light-response and data quality before extended data collection in pump–probe photocrystallography experiments},
author = {Coppens, Philip and Makal, Anna and Fournier, Bertrand and Jarzembska, Katarzyna N. and Kamiński, Radosław and Basuroy, Krishnayan and Trzop, Elzbieta},
abstractNote = {In picosecond and slower pump–probe diffraction experiments, collection of response–ratio correlation sets prior to full data collection provides an invaluable confirmation of the existence of a light-induced signal prior to full data collection. If a response to light exposure is observed, the quality of the data being collected can be assessed. We present a number of such correlation plots both for synchrotron and in-house pump–probe data collection.},
doi = {10.1107/S2052520616017558},
journal = {Acta Crystallographica. Section B, Structural Science, Crystal Engineering and Materials (Online)},
number = 1,
volume = 73,
place = {United States},
year = {Mon Jan 23 00:00:00 EST 2017},
month = {Mon Jan 23 00:00:00 EST 2017}
}