Procedures for the synthesis of ethylenediamine bisborane and ammonia borane

Ramachandran, Padi Veeraraghavan; Gagare, Pravin D.; Mistry, Hitesh; Biswas, Bidyut

Title: Procedures for the synthesis of ethylenediamine bisborane and ammonia borane

Patent · Tue Jan 03 00:00:00 EST 2017

OSTI ID:1338064

Ramachandran, Padi Veeraraghavan; Gagare, Pravin D.; Mistry, Hitesh; Biswas, Bidyut

A method for synthesizing ammonia borane includes (a) preparing a reaction mixture in one or more solvents, the reaction mixture containing sodium borohydride, at least one ammonium salt, and ammonia; and (b) incubating the reaction mixture at temperatures between about 0.degree. C. to about room temperature in an ambient air environment under conditions sufficient to form ammonia borane. Methods for synthesizing ethylenediamine bisborane, and methods for dehydrogenation of ethylenediamine bisborane are also described.

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Research Organization:: Purdue Univ., West Lafayette, IN (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: FG36-06GO86050

Assignee:: PURDUE RESEARCH FOUNDATION (West Lafayette, IN)

Patent Number(s):: 9,534,002

Application Number:: 13/809,316

OSTI ID:: 1338064

Resource Relation:: Patent File Date: 2011 Jul 06

Country of Publication:: United States

Language:: English

References (13)

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