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Title: New developments in laser-heated diamond anvil cell with in situ synchrotron x-ray diffraction at High Pressure Collaborative Access Team

Journal Article · · Review of Scientific Instruments
DOI:https://doi.org/10.1063/1.4926895· OSTI ID:1335884
 [1];  [1];  [1];  [2];  [1]
  1. Carnegie Institution of Washington, Argonne, IL (United States)
  2. Carnegie Institution of Washington, Washington, D.C. (United States)

An overview of the in situ laser heating system at the High Pressure Collaborative Access Team, with emphasis on newly developed capabilities, is presented. Since its establishment at the beamline 16-ID-B a decade ago, laser-heated diamond anvil cell coupled with in situ synchrotron x-ray diffraction has been widely used for studying the structural properties of materials under simultaneous high pressure and high temperature conditions. Recent developments in both continuous-wave and modulated heating techniques have been focusing on resolving technical issues of the most challenging research areas. Furthermore, the new capabilities have demonstrated clear benefits and provide new opportunities in research areas including high-pressure melting, pressure-temperature-volume equations of state, chemical reaction, and time resolved studies.

Research Organization:
Carnegie Institution of Washington, Washington, D.C. (United States); Carnegie Inst. of Science, Argonne, IL (United States)
Sponsoring Organization:
USDOE National Nuclear Security Administration (NNSA)
Grant/Contract Number:
NA0002006; AC02-06CH11357; FG02-99ER45775; NA0001974
OSTI ID:
1335884
Alternate ID(s):
OSTI ID: 1228679
Journal Information:
Review of Scientific Instruments, Vol. 86, Issue 7; ISSN 0034-6748
Publisher:
American Institute of Physics (AIP)Copyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 83 works
Citation information provided by
Web of Science

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Microstructures define melting of molybdenum at high pressures journal March 2017
Synthesis of quenchable amorphous diamond journal August 2017
Altered chemistry of oxygen and iron under deep Earth conditions journal January 2019
Thermal equation of state of Molybdenum determined from in situ synchrotron X-ray diffraction with laser-heated diamond anvil cells journal February 2016
High-pressure discovery of β-NiBi journal January 2017
The influence of wavelength-dependent absorption and temperature gradients on temperature determination in laser-heated diamond-anvil cells journal January 2017
A CO 2 laser heating system for in situ high pressure-temperature experiments at HPCAT journal August 2018
Advanced Spectral Analysis Program journal February 2019
Multimode scanning X-ray diffraction microscopy for diamond anvil cell experiments journal February 2019
Laser heating setup for diamond anvil cells for in situ synchrotron and in house high and ultra-high pressure studies journal October 2019
New developments in high-pressure X-ray diffraction beamline for diamond anvil cell at SPring-8 journal January 2020
Origins of ultralow velocity zones through slab-derived metallic melt journal May 2016
High-pressure/high-temperature phase diagram of zinc journal June 2018
High-pressure studies with x-rays using diamond anvil cells journal November 2016
High pressure x-ray diffraction techniques with synchrotron radiation journal July 2016
High-pressure melting curve of sulfur up to 65 GPa journal August 2019
Experimental observations of large changes in electron density distributions in β Ge journal December 2019
Synthesis of a polar ordered oxynitride perovskite journal June 2017
Laser-heating system for high-pressure X-ray diffraction at the Extreme Conditions beamline I15 at Diamond Light Source journal October 2018
Carbon-boron clathrates as a new class of sp 3 -bonded framework materials journal January 2020
Portable double-sided pulsed laser heating system for time-resolved geoscience and materials science applications text January 2017
Synthesis of Manganese Mononitride with Tetragonal Structure under Pressure journal September 2019
Discovery of Cu 3 Pb journal September 2018
Postaragonite phases of CaCO3 at lower mantle pressures text January 2018
Synthesis of a polar ordered oxynitride perovskite text January 2017
Laser-heating system for high-pressure X-ray diffraction at the Extreme Conditions beamline I15 at Diamond Light Source text January 2018
Portable double-sided pulsed laser heating system for time-resolved geoscience and materials science applications journal August 2017
High-pressure high-temperature phase diagram of zinc text January 2018