Synthesis of substituted pyrazines

Pagoria, Philip F.; Zhang, Mao Xi

Synthesis of substituted pyrazines

Patent · Tue Oct 04 00:00:00 EDT 2016

OSTI ID:1327969

Pagoria, Philip F.; Zhang, Mao Xi

A method for synthesizing a pyrazine-containing material according to one embodiment includes contacting an iminodiacetonitrile derivative with a base and a reagent selected from a group consisting of hydroxylamine, a hydroxylamine salt, an aliphatic primary amine, a secondary amine, an aryl-substituted alkylamine a heteroaryl-substituted alkyl amine, an alcohol, an alkanolamine and an aryl alcoholamine. Additional methods and several reaction products are presented. ##STR00001##

Research Organization:: Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: AC52-07NA27344

Assignee:: Lawrence Livermore National Security, LLC (Livermore, CA)

Patent Number(s):: 9,458,115

Application Number:: 12/426,774

OSTI ID:: 1327969

Country of Publication:: United States

Language:: English

References (8)

New synthesis of 2-amino-6-alkoxypyrazines from N-nitrosobis (cyanomethyl) amine and alkoxides Vohra, Saroj K.; Harrington, George W.; Zacharias, David E. The Journal of Organic Chemistry, Vol. 44, Issue 7 https://doi.org/10.1021/jo01321a021	journal	March 1979
The unusually mild and facile basic hydrolysis of N-nitroso-2-(methylamino)acetonitrile Chang, Shaw Kong.; Harrington, George W.; Veale, Harry S. The Journal of Organic Chemistry, Vol. 41, Issue 23 https://doi.org/10.1021/jo00885a022	journal	November 1976
Theoretical Calculation and Molecular Design for High Explosives: Theoretical Study on Polynitropyrazines and TheirN-oxides Li, Jinshan; Huang, Yigang; Dong, Haishan Propellants, Explosives, Pyrotechnics, Vol. 29, Issue 4 https://doi.org/10.1002/prep.200400052	journal	August 2004
MATERIALS SCIENCE: Muscles Made from Metal Baughman, R. H. Science, Vol. 300, Issue 5617 https://doi.org/10.1126/science.1082270	journal	April 2003
Charge-Induced Reversible Strain in a Metal Weissmuller, J. Science, Vol. 300, Issue 5617 https://doi.org/10.1126/science.1081024	journal	April 2003
Surface-Stress Induced Macroscopic Bending of Nanoporous Gold Cantilevers Kramer, Dominik; Viswanath, Raghavan Nadar; Weissmüller, Jörg Nano Letters, Vol. 4, Issue 5 https://doi.org/10.1021/nl049927d	journal	May 2004
Molecular design of analogues of 2,6-diamino-3,5-dinitropyrazine-1-oxide He, Wendi; Zhou, Ge; Li, Jingshan Journal of Molecular Structure: THEOCHEM, Vol. 668, Issue 2-3, p. 201-208 https://doi.org/10.1016/j.theochem.2003.10.058	journal	January 2004
Heterocyclic imines and amines. Part XVI. 2,6-Diaminopyrazine and its 1-oxide from iminodiacetonitrile Barot, Nandkishor R.; Elvidge, John A. Journal of the Chemical Society, Perkin Transactions 1 https://doi.org/10.1039/P19730000606	journal	January 1973

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Synthesis of substituted pyrazines

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