High cycle fatigue in the transmission electron microscope

Bufford, Daniel C.; Stauffer, Douglas; Mook, William M.; Syed Asif, S. A.; Boyce, Brad L.; Hattar, Khalid

doi:10.1021/acs.nanolett.6b01560

Title: High cycle fatigue in the transmission electron microscope

Journal Article · Tue Jun 28 00:00:00 EDT 2016 · Nano Letters

DOI:https://doi.org/10.1021/acs.nanolett.6b01560· OSTI ID:1271014

Bufford, Daniel C. ^[1]; Stauffer, Douglas ^[2]; Mook, William M. ^[1]; Syed Asif, S. A. ^[2]; Boyce, Brad L. ^[1]; Hattar, Khalid ^[1]

Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)
Hysitron, Inc., Eden Prairie, MN (United States)

One of the most common causes of structural failure in metals is fatigue induced by cyclic loading. Historically, microstructure-level analysis of fatigue cracks has primarily been performed post mortem. However, such investigations do not directly reveal the internal structural processes at work near micro- and nanoscale fatigue cracks and thus do not provide direct evidence of active microstructural mechanisms. In this paper, the tension–tension fatigue behavior of nanocrystalline Cu was monitored in real time at the nanoscale by utilizing a new capability for quantitative cyclic mechanical loading performed in situ in a transmission electron microscope (TEM). Controllable loads were applied at frequencies from one to several hundred hertz, enabling accumulations of 10⁶ cycles within 1 h. The nanometer-scale spatial resolution of the TEM allows quantitative fatigue crack growth studies at very slow crack growth rates, measured here at ~10^–12 m·cycle^–1. This represents an incipient threshold regime that is well below the tensile yield stress and near the minimum conditions for fatigue crack growth. Evidence of localized deformation and grain growth within 150 nm of the crack tip was observed by both standard imaging and precession electron diffraction orientation mapping. Finally, these observations begin to reveal with unprecedented detail the local microstructural processes that govern damage accumulation, crack nucleation, and crack propagation during fatigue loading in nanocrystalline Cu.

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Research Organization:: Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Contributing Organization:: Hysitron, Inc., Eden Prairie, MN (United States)

Grant/Contract Number:: AC04-94AL85000; FG02-04ER83979; FG02-07ER84813

OSTI ID:: 1271014

Report Number(s):: SAND2016-6822J; 645284

Journal Information:: Nano Letters, Journal Name: Nano Letters; ISSN 1530-6984

Publisher:: American Chemical SocietyCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 32 works

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