Microstructural stability and mechanical behavior of FeNiMnCr high entropy alloy under ion irradiation

Leonard, Keith J.; Bei, Hongbin; Zinkle, Steven J.; Kiran Kumar, N. A. P.; Li, C.

doi:10.1016/j.actamat.2016.05.007

Title: Microstructural stability and mechanical behavior of FeNiMnCr high entropy alloy under ion irradiation

Journal Article · Fri May 13 00:00:00 EDT 2016 · Acta Materialia

DOI:https://doi.org/10.1016/j.actamat.2016.05.007· OSTI ID:1256811

Leonard, Keith J. ^[1]; Bei, Hongbin ^[1]; Zinkle, Steven J. ^[2]; Kiran Kumar, N. A. P. ^[1]; Li, C. ^[3]

Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Univ. of Tennessee, Knoxville, TN (United States)
Univ. of Tennessee, Knoxville, TN (United States)

In recent years, high entropy alloys (HEAs) have attracted significant attention due to their excellent mechanical properties and good corrosion resistance, making them potential candidates for high temperature fission and fusion structural applications. However there is very little known about their radiation resistance, particularly at elevated temperatures relevant for energy applications. In the present study, a single phase (face centered cubic) concentrated solid solution alloy of composition 27%Fe-28%Ni-27%Mn-18%Cr was irradiated with 3 or 5.8 MeV Ni ions at temperatures ranging from room temperature to 700 °C and midrange doses from 0.03 to 10 displacements per atom (dpa). Transmission electron microscopy (TEM), scanning transmission electron microscopy with energy dispersive x-ray spectrometry (STEM/EDS) and X-ray diffraction (XRD) were used to characterize the radiation defects and microstructural changes. Irradiation at higher temperatures showed evidence of relatively sluggish solute diffusion with limited solute depletion or enrichment at grain boundaries. The main microstructural feature at all temperatures was high-density small dislocation loops. Voids were not observed at any irradiation condition. Nano-indentation tests on specimens irradiated at room temperature showed a rapid increase in hardness ~35% and ~80% higher than the unirradiated value at 0.03 and 0.3 dpa midrange doses, respectively. The irradiation-induced hardening was less pronounced for 500 °C irradiations (<20% increase after 3 dpa). Overall, the examined HEA material exhibits superior radiation resistance compared to conventional single phase Fe-Cr-Ni austenitic alloys such as stainless steels. Furthermore, the present study provides insight on the fundamental irradiation behavior of a single phase HEA material over a broad range of irradiation temperatures.

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Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Fusion Energy Sciences (FES)

Grant/Contract Number:: AC05-00OR22725

OSTI ID:: 1256811

Alternate ID(s):: OSTI ID: 1326425

Journal Information:: Acta Materialia, Vol. 113, Issue C; ISSN 1359-6454

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 331 works

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A Novel Low-Activation VCrFeTaxWx (x = 0.1, 0.2, 0.3, 0.4, and 1) High-Entropy Alloys with Excellent Heat-Softening Resistance Zhang, Weiran; Liaw, Peter; Zhang, Yong Entropy, Vol. 20, Issue 12 https://doi.org/10.3390/e20120951	journal	December 2018
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Proton Irradiation Effects on Hardness and the Volta Potential of Welding 308L Duplex Stainless Steel Jiang, Baolong; Peng, Qunjia; Jiao, Zhijie Micromachines, Vol. 10, Issue 1 https://doi.org/10.3390/mi10010011	journal	December 2018

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