Local probing of ferroelectric and ferroelastic switching through stress-mediated piezoelectric spectroscopy

Edwards, David; Bastani, Yaser; Cao, Ye; Chen, Long -Qing; Kalinin, Sergei V.; Kumar, Amit; Bassiri-Gharb, Nazanin; Brewer, Steven

doi:10.1002/admi.201500470

Local probing of ferroelectric and ferroelastic switching through stress-mediated piezoelectric spectroscopy

Journal Article · Mon Jan 18 23:00:00 EST 2016 · Advanced Materials Interfaces

DOI:https://doi.org/10.1002/admi.201500470· OSTI ID:1241469

Edwards, David ^[1]; Bastani, Yaser ^[2]; Cao, Ye ^[3]; Chen, Long -Qing ^[4]; Kalinin, Sergei V. ^[3]; Kumar, Amit ^[1]; Bassiri-Gharb, Nazanin ^[2]; Brewer, Steven ^[2]

Queenâs Univ. Belfast, Belfast (United Kingdom)
Georgia Institute of Technology, Atlanta, GA (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Pennsylvania State Univ., University Park, PA (United States)

The role of local strains is fundamental to the large effective piezoelectric and ferroelectric response of thin films. Therefore a method to investigate local strain-induced phenomena is imperative. Here, pressure induced domain reorganization is reported in lead zirconate titanate films with composition near the morphotropic phase boundary. An approach is thus demonstrated to simultaneously study the role of applied mechanical pressure on multiple local properties of the film. In particular, the modification of hysteresis loops collected at different tip pressures is consistent with first mostly ferroelastic and then ferroelectric dominated reorientation of domains under increasing applied pressure. The pressure induced domain writing is also investigated through phase field simulations where the applied pressure is generally found to increase the in-plane polarization of the domains with respect to the out-of-plane component, corroborating the experimental observations. The approach developed here has the potential to explore other hysteretic phenomena and phase transitions in a spatially resolved manner with varying local pressure.

View Accepted Manuscript (DOE)

Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE Office of Science (SC)

Grant/Contract Number:: AC05-00OR22725

OSTI ID:: 1241469

Journal Information:: Advanced Materials Interfaces, Journal Name: Advanced Materials Interfaces Journal Issue: 6 Vol. 2; ISSN 2196-7350

Publisher:: Wiley-VCHCopyright Statement

Country of Publication:: United States

Language:: English

References (43)

Influence of a Single Grain Boundary on Domain Wall Motion in Ferroelectrics Marincel, Daniel M.; Zhang, Huairuo; Kumar, Amit Advanced Functional Materials, Vol. 24, Issue 10 https://doi.org/10.1002/adfm.201302457	journal	October 2013
Nanoscale Mechanical Softening of Morphotropic BiFeO ₃ Heo, Yooun; Jang, Byong-Kweon; Kim, Seung Jin Advanced Materials, Vol. 26, Issue 45 https://doi.org/10.1002/adma.201401958	journal	October 2014
The Importance of Distributed Loading and Cantilever Angle in Piezo-Force Microscopy Huey, Bryan D.; Ramanujan, Chandra; Bobji, Musuvathi Journal of Electroceramics, Vol. 13, Issue 1-3 https://doi.org/10.1007/s10832-004-5114-y	journal	July 2004
Effect of substrate constraint on the stability and evolution of ferroelectric domain structures in thin films Li, Y. L.; Hu, S. Y.; Liu, Z. K. Acta Materialia, Vol. 50, Issue 2 https://doi.org/10.1016/S1359-6454(01)00360-3	journal	January 2002
In situ nanoindentation: Probing nanoscale multifunctionality Nili, Hussein; Kalantar-zadeh, Kourosh; Bhaskaran, Madhu Progress in Materials Science, Vol. 58, Issue 1 https://doi.org/10.1016/j.pmatsci.2012.08.001	journal	January 2013
Mechanical Control of Electroresistive Switching Kim, Yunseok; Kelly, Simon J.; Morozovska, Anna Nano Letters, Vol. 13, Issue 9 https://doi.org/10.1021/nl401411r	journal	August 2013
Enhancement of Local Piezoresponse in Polymer Ferroelectrics via Nanoscale Control of Microstructure Choi, Yoon-Young; Sharma, Pankaj; Phatak, Charudatta ACS Nano, Vol. 9, Issue 2 https://doi.org/10.1021/nn5067232	journal	January 2015
Ferroelectric PZT Thin Films by Sol-Gel Deposition Reaney, Ian M.; Taylor, David V.; Brooks, Keith G. Journal of Sol-Gel Science and Technology, Vol. 13, Issue 1/3, p. 813-820 https://doi.org/10.1023/A:1008690316261	journal	January 1998
Room-temperature ferroelectricity in strained SrTiO₃ Haeni, J. H.; Irvin, P.; Chang, W. Nature, Vol. 430, Issue 7001, p. 758-761 https://doi.org/10.1038/nature02773	journal	August 2004
Domain switching in polycrystalline ferroelectric ceramics Li, J. Y.; Rogan, R. C.; Üstündag, E. Nature Materials, Vol. 4, Issue 10 https://doi.org/10.1038/nmat1485	journal	September 2005
Direct imaging of the spatial and energy distribution of nucleation centres in ferroelectric materials Jesse, Stephen; Rodriguez, Brian J.; Choudhury, Samrat Nature Materials, Vol. 7, Issue 3 https://doi.org/10.1038/nmat2114	journal	February 2008
Ferroelectric polarization reversal via successive ferroelastic transitions Xu, Ruijuan; Liu, Shi; Grinberg, Ilya Nature Materials, Vol. 14, Issue 1 https://doi.org/10.1038/nmat4119	journal	October 2014
Thermodynamic theory of stress distribution in epitaxial Pb(Zr, Ti)O3 thin films Kim, H. Joon; Oh, S. Hoon; Jang, Hyun M. Applied Physics Letters, Vol. 75, Issue 20 https://doi.org/10.1063/1.125275	journal	November 1999
Domain wall motion and its contribution to the dielectric and piezoelectric properties of lead zirconate titanate films Xu, F.; Trolier-McKinstry, S.; Ren, W. Journal of Applied Physics, Vol. 89, Issue 2 https://doi.org/10.1063/1.1325005	journal	January 2001
Principle of ferroelectric domain imaging using atomic force microscope Hong, Seungbum; Woo, Jungwon; Shin, Hyunjung Journal of Applied Physics, Vol. 89, Issue 2, p. 1377-1386 https://doi.org/10.1063/1.1331654	journal	January 2001
Effect of domain structure on thermal stability of nanoscale ferroelectric domains Woo, Jungwon; Hong, Seungbum; Min, Dong Ki Applied Physics Letters, Vol. 80, Issue 21 https://doi.org/10.1063/1.1481537	journal	May 2002
Are strain-induced effects truly strain induced? A comprehensive study of strained LCMO thin films Dvorak, Joseph; Idzerda, Y. U.; Ogale, S. B. Journal of Applied Physics, Vol. 97, Issue 10 https://doi.org/10.1063/1.1845974	journal	May 2005
Ferroelectric/ferroelastic behavior and piezoelectric response of lead zirconate titanate thin films under nanoindentation Koval, V.; Reece, M. J.; Bushby, A. J. Journal of Applied Physics, Vol. 97, Issue 7 https://doi.org/10.1063/1.1870092	journal	April 2005
Domain rearrangement during nanoindentation in single-crystalline barium titanate measured by atomic force microscopy and piezoresponse force microscopy Schneider, G. A.; Scholz, T.; Muñoz-Saldaña, J. Applied Physics Letters, Vol. 86, Issue 19 https://doi.org/10.1063/1.1920410	journal	May 2005
Piezoelectric nonlinearity in ferroelectric thin films Bassiri Gharb, Nazanin; Trolier-McKinstry, Susan; Damjanovic, Dragan Journal of Applied Physics, Vol. 100, Issue 4 https://doi.org/10.1063/1.2266235	journal	August 2006
Injection charge assisted polarization reversal in ferroelectric thin films Kim, Yunseok; Bühlmann, Simon; Hong, Seungbum Applied Physics Letters, Vol. 90, Issue 7 https://doi.org/10.1063/1.2679902	journal	February 2007
Spatially resolved probing of Preisach density in polycrystalline ferroelectric thin films Guo, S.; Ovchinnikov, O. S.; Curtis, M. E. Journal of Applied Physics, Vol. 108, Issue 8 https://doi.org/10.1063/1.3493738	journal	October 2010
Critical thickness for extrinsic contributions to the dielectric and piezoelectric response in lead zirconate titanate ultrathin films Bastani, Yaser; Schmitz-Kempen, Thorsten; Roelofs, Andreas Journal of Applied Physics, Vol. 109, Issue 1 https://doi.org/10.1063/1.3527970	journal	January 2011
Domain configurations due to multiple misfit relaxation mechanisms in epitaxial ferroelectric thin films. I. Theory Speck, J. S.; Pompe, W. Journal of Applied Physics, Vol. 76, Issue 1 https://doi.org/10.1063/1.357097	journal	July 1994
Measurement of piezoelectric coefficients of ferroelectric thin films Lefki, K.; Dormans, G. J. M. Journal of Applied Physics, Vol. 76, Issue 3 https://doi.org/10.1063/1.357693	journal	August 1994
Nanoscale ferroelectric switching behavior at charged domain boundaries studied by angle-resolved piezoresponse force microscopy Park, Moonkyu; Hong, Seungbum; Kim, Jiyoon Applied Physics Letters, Vol. 99, Issue 14 https://doi.org/10.1063/1.3646761	journal	October 2011
Characterization of ferroelectric lead zirconate titanate films by scanning force microscopy Zavala, Genaro; Fendler, Janos H.; Trolier-McKinstry, Susan Journal of Applied Physics, Vol. 81, Issue 11 https://doi.org/10.1063/1.365350	journal	June 1997
Strain-modulated piezoelectric and electrostrictive nonlinearity in ferroelectric thin films without active ferroelastic domain walls Bassiri-Gharb, Nazanin; Trolier-McKinstry, Susan; Damjanovic, Dragan Journal of Applied Physics, Vol. 110, Issue 12 https://doi.org/10.1063/1.3665410	journal	December 2011
Collective dynamics underpins Rayleigh behavior in disordered polycrystalline ferroelectrics Bintachitt, P.; Jesse, S.; Damjanovic, D. Proceedings of the National Academy of Sciences, Vol. 107, Issue 16 https://doi.org/10.1073/pnas.0913172107	journal	April 2010
Domains, Domain Walls and Defects in Perovskite Ferroelectric Oxides: A Review of Present Understanding and Recent Contributions Pramanick, Abhijit; Prewitt, Anderson D.; Forrester, Jennifer S. Critical Reviews in Solid State and Materials Sciences, Vol. 37, Issue 4 https://doi.org/10.1080/10408436.2012.686891	journal	December 2012
Strain dependence of polarization and piezoelectric response in epitaxial BiFeO ₃ thin films Daumont, C.; Ren, W.; Infante, I. C. Journal of Physics: Condensed Matter, Vol. 24, Issue 16 https://doi.org/10.1088/0953-8984/24/16/162202	journal	March 2012
Domain populations in lead zirconate titanate thin films of different compositions via piezoresponse force microscopy Wu, A.; Vilarinho, P. M.; Shvartsman, V. V. Nanotechnology, Vol. 16, Issue 11 https://doi.org/10.1088/0957-4484/16/11/020	journal	September 2005
The band excitation method in scanning probe microscopy for rapid mapping of energy dissipation on the nanoscale Jesse, Stephen; Kalinin, Sergei V.; Proksch, Roger Nanotechnology, Vol. 18, Issue 43 https://doi.org/10.1088/0957-4484/18/43/435503	journal	September 2007
Resolution theory, and static and frequency-dependent cross-talk in piezoresponse force microscopy Jesse, S.; Guo, S.; Kumar, A. Nanotechnology, Vol. 21, Issue 40 https://doi.org/10.1088/0957-4484/21/40/405703	journal	September 2010
Effect of external stress on ferroelectricity in epitaxial thin films Emelyanov, A. Yu.; Pertsev, N. A.; Kholkin, A. L. Physical Review B, Vol. 66, Issue 21 https://doi.org/10.1103/PhysRevB.66.214108	journal	December 2002
Domain pinning near a single-grain boundary in tetragonal and rhombohedral lead zirconate titanate films Marincel, D. M.; Zhang, H. R.; Britson, J. Physical Review B, Vol. 91, Issue 13 https://doi.org/10.1103/PhysRevB.91.134113	journal	April 2015
Substrate Clamping Effects on Irreversible Domain Wall Dynamics in Lead Zirconate Titanate Thin Films Griggio, F.; Jesse, S.; Kumar, A. Physical Review Letters, Vol. 108, Issue 15 https://doi.org/10.1103/PhysRevLett.108.157604	journal	April 2012
Paraelectric thin films by nanoscale engineering of epitaxy and planar anisotropy for microwave phase shifter applications Akdogan, E.; Simon, William; Safari, Ahmad IEEE Transactions on Ultrasonics, Ferroelectrics and Frequency Control, Vol. 53, Issue 12 https://doi.org/10.1109/TUFFC.2006.180	journal	December 2006
Phase-Field Method of Phase Transitions/Domain Structures in Ferroelectric Thin Films: A Review Chen, Long-Qing Journal of the American Ceramic Society, Vol. 91, Issue 6 https://doi.org/10.1111/j.1551-2916.2008.02413.x	journal	June 2008
Stress Sensitivity of Piezoelectric Ceramics: Part 1. Sensitivity to Compressive Stress Parallel to the Polar Axis Krueger, Helmut H. A. The Journal of the Acoustical Society of America, Vol. 42, Issue 3 https://doi.org/10.1121/1.1910635	journal	September 1967
Enhancement of Ferroelectricity in Strained BaTiO₃ Thin Films Choi, K. J.; Biegalski, M.; Li, Y. L. Science, Vol. 306, Issue 5698, p. 1005-1009 https://doi.org/10.1126/science.1103218	journal	November 2004
Mechanical Writing of Ferroelectric Polarization Lu, H.; Bark, C. -W.; Esque de los Ojos, D. Science, Vol. 336, Issue 6077 https://doi.org/10.1126/science.1218693	journal	April 2012
Spectroscopic imaging in piezoresponse force microscopy: New opportunities for studying polarization dynamics in ferroelectrics and multiferroics Vasudevan, R. K.; Jesse, S.; Kim, Y. MRS Communications, Vol. 2, Issue 3 https://doi.org/10.1557/mrc.2012.15	journal	July 2012

Cited By (4)

Revealing the Interplay of Structural Phase Transitions and Ferroelectric Switching in Mixed Phase BiFeO ₃ Naden, Aaron B.; Edwards, David; Neumayer, Sabine M. Advanced Materials Interfaces, Vol. 5, Issue 21 https://doi.org/10.1002/admi.201801019	journal	October 2018
Stress-induced reversible and irreversible ferroelectric domain switching Chen, Zibin; Huang, Qianwei; Wang, Feifei Applied Physics Letters, Vol. 112, Issue 15 https://doi.org/10.1063/1.5020534	journal	April 2018
Investigation of AFM-based machining of ferroelectric thin films at the nanoscale Zhang, Fengyuan; Edwards, David; Deng, Xiong Journal of Applied Physics, Vol. 127, Issue 3 https://doi.org/10.1063/1.5133018	journal	January 2020
Local piezo-response for lead-free Ba0.9Ca0.1Ti0.9Zr0.1O3 electro-ceramic by switching spectroscopy Herrera-Pérez, Guillermo; Castillo-Sandoval, Isaí; Solís-Canto, Oscar Materials Research, Vol. 21, Issue 2 https://doi.org/10.1590/1980-5373-mr-2017-0605	journal	January 2018

Figures / Tables (6)

Similar Records

Ferroelectric/ferroelastic behavior and piezoelectric response of lead zirconate titanate thin films under nanoindentation

Journal Article · Thu Mar 31 23:00:00 EST 2005 · Journal of Applied Physics · OSTI ID:20668288

A finite element model of ferroelectric/ferroelastic polycrystals

Conference · Wed Feb 16 23:00:00 EST 2000 · OSTI ID:751349

Nanoscale Origins of Ferroelastic Domain Wall Mobility in Ferroelectric Multilayers

Journal Article · Mon Oct 31 00:00:00 EDT 2016 · ACS Nano · OSTI ID:1336210

Related Subjects

36 MATERIALS SCIENCE
ferroelastics
ferroelectrics
lead zirconate titanate
piezoelectric spectroscopy
piezoresponse force microscopy

Local probing of ferroelectric and ferroelastic switching through stress-mediated piezoelectric spectroscopy

Citation Formats

References (43)

Cited By (4)

Figures / Tables (6)

Similar Records

Related Subjects