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Structure–kinetic relationship study of organozinc reagents

Journal Article · · ChemComm
DOI:https://doi.org/10.1039/c4cc01135j· OSTI ID:1241304
Phenylzinc reagents prepared from various zinc halides show distinct kinetic features in the palladium-catalyzed Negishi-type oxidative coupling reaction, in which the phenylzinc reagent prepared from ZnI2 gives the highest rate. In situ infrared and X-ray absorption spectroscopy studies show that the higher reaction rate was observed for longer Zn–C bond distances.
Research Organization:
Argonne National Laboratory (ANL)
Sponsoring Organization:
Wuhan University; Argonne National Laboratory - Chemical Sciences and Engineering Division; Chinese Academy of Sciences (CAS); National Natural Science Foundation of China (NSFC); Materials Research Collaborative Access Team (MRCAT); USDOE Office of Science - Office of Basic Energy Sciences
DOE Contract Number:
AC02-06CH11357
OSTI ID:
1241304
Journal Information:
ChemComm, Journal Name: ChemComm Vol. 50; ISSN 1359-7345
Publisher:
Royal Society of Chemistry
Country of Publication:
United States
Language:
English

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