Synthesis of macroporous structures

Stein, Andreas; Holland, Brian T.; Blanford, Christopher F.; Yan, Hongwei

Title: Synthesis of macroporous structures

Patent · Tue Jan 20 00:00:00 EST 2004

OSTI ID:1174692

Stein, Andreas; Holland, Brian T.; Blanford, Christopher F.; Yan, Hongwei

The present application discloses a method of forming an inorganic macroporous material. In some embodiments, the method includes: providing a sample of organic polymer particles having a particle size distribution of no greater than about 10%; forming a colloidal crystal template of the sample of organic polymer particles, the colloidal crystal template including a plurality of organic polymer particles and interstitial spaces therebetween; adding an inorganic precursor composition including a noncolloidal inorganic precursor to the colloidal crystal template such that the precursor composition permeates the interstitial spaces between the organic polymer particles; converting the noncolloidal inorganic precursor to a hardened inorganic framework; and removing the colloidal crystal template from the hardened inorganic framework to form a macroporous material. Inorganic macroporous materials are also disclosed.

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Research Organization:: Univ. of Minnesota, Minneapolis, MN (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: FG02-93-ER14384

Assignee:: Regents of the University of Minnesota (Minneapolis, MN)

Patent Number(s):: 6,680,013

Application Number:: 09/549,078

OSTI ID:: 1174692

Country of Publication:: United States

Language:: English

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