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Spectroscopic and computational analysis of the molecular interactions in the ionic liquid ion pair [BMP]+[TFSI]-

Journal Article · · Journal of Molecular Liquids

1-Butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide ([BMP]{sup +}[TFSI]{sup -}) ion pairs were studied using DFT at the B3LYP/6-31 + G(d) level. Nine locally stable conformations of the ion pair were located. In the most stable conformation, [TFSI]{sup -} takes a cis conformation and lies below the pyrrolidinium ring. Atoms-in-molecules (AIM) and electron density analysis indicated the existence of nine hydrogen bonds. Interaction energies were recalculated at the Second-order Møller–Plesset (MP2) level to show the importance of dispersion interaction. Further investigation through natural bond orbital (NBO) analysis provided insight into the importance of charge transfer interactions in the ion pair. Harmonic vibrations of the ion pair were calculated and compared with vibrations of the free ions as well as the experimental infrared spectrum. Assignments and frequency shifts are discussed in light of the inter-ionic interactions.

Research Organization:
National Energy Technology Laboratory - In-house Research
Sponsoring Organization:
USDOE Office of Fossil Energy (FE)
DOE Contract Number:
FE0004000
OSTI ID:
1129545
Report Number(s):
A-UNIV-PUB-031
Journal Information:
Journal of Molecular Liquids, Journal Name: Journal of Molecular Liquids Journal Issue: C Vol. 175; ISSN 0167-7322
Publisher:
Elsevier
Country of Publication:
United States
Language:
English

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