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Making a Hybrid Microfluidic Platform Compatible for In Situ Imaging by Vacuum-Based Techniques

Journal Article · · Journal of Vacuum Science and Technology A--Vacuum, Surfaces and Films
DOI:https://doi.org/10.1116/1.3654147· OSTI ID:1029080
A self-contained microfluidic-based device was designed and fabricated for in situ imaging of aqueous surfaces using vacuum techniques. The device is a hybrid between a microfluidic PDMS block and external accessories, all portable on a small platform (10 cm-8 cm). The key feature is that a small aperture with a diameter of 2-3 micrometers is opened to the vacuum, which serves as a detection window for in situ imaging of aqueous surfaces. Vacuum compatibility and temperature drop due to water vaporization are the two most important challenges in this invention. Theoretical calculations and fabrication strategies are presented from multiple design aspects. In addition, results from the time-of-flight secondary ion mass spectrometry (ToF-SIMS) of aqueous surfaces are presented.
Research Organization:
Pacific Northwest National Laboratory (PNNL), Richland, WA (US), Environmental Molecular Sciences Laboratory (EMSL)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC05-76RL01830
OSTI ID:
1029080
Report Number(s):
PNNL-SA-81346; 30203; 42330; 36603; 36601; KC0301020
Journal Information:
Journal of Vacuum Science and Technology A--Vacuum, Surfaces and Films, Journal Name: Journal of Vacuum Science and Technology A--Vacuum, Surfaces and Films Journal Issue: 6 Vol. 29
Country of Publication:
United States
Language:
English

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