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Deformation of Diopside Single Crystal at Mantle Pressure, 1, Mechanical Data

Journal Article · · Physics of the Earth and Planetary Interiors
Steady-state deformation experiments were carried out in a deformation-DIA (D-DIA) high-pressure apparatus on oriented diopside single crystals, at pressure (P) ranging from 3.8 to 8.8 GPa, temperature (T) from 1100 to 1400 C, and differential stress ({sigma}) between 0.2 and 1.7 GPa. Three compression directions were chosen in order to test the activity of diopside dislocation slip systems, i.e., 1/2<1 1 0>{l_brace}1 {bar 1} 0{r_brace} systems activated together, both [1 0 0](0 1 0) and [0 1 0](1 0 0) systems together, or [0 0 1] dislocation slip activated in (1 0 0), (0 1 0) and {l_brace}1 1 0{r_brace} planes. Constant applied stress and specimen strain rates ({var_epsilon}) were monitored in situ using time-resolved synchrotron X-ray diffraction and radiography, respectively. Transmission electron microscopy (TEM) investigation of the run products revealed that dislocation creep was responsible for sample deformation. Comparison of the present high-P data with those obtained at room-P by Raterron and Jaoul (1991) - on similar crystals deformed at comparable T-{sigma} conditions - allows quantifying the effect of P on 1/2<1 1 0>{l_brace} 1 {bar 1} 0{r_brace} activity. This translates into the activation volume V* = 17 {+-} 6 cm{sup 3}/mol in the corresponding creep power law. Our data also show that both 1/2<1 1 0> dislocation slips and [0 0 1] have comparable slip activities at mantle P and T, while [1 0 0](0 1 0) and [0 1 0](1 0 0) slip systems remain marginal. These results show that P has a significant effect on high-T dislocation creep in diopside, the higher the pressure the harder the crystal, and that this effect is stronger on 1/2<1 1 0> slip than on [0 0 1] slip.
Research Organization:
Brookhaven National Laboratory (BNL) National Synchrotron Light Source
Sponsoring Organization:
DOE - OFFICE OF SCIENCE
DOE Contract Number:
AC02-98CH10886
OSTI ID:
1019981
Report Number(s):
BNL--95827-2011-JA
Journal Information:
Physics of the Earth and Planetary Interiors, Journal Name: Physics of the Earth and Planetary Interiors Journal Issue: 3-4 Vol. 177; ISSN 0031-9201; ISSN PEPIAM
Country of Publication:
United States
Language:
English

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