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U.S. Department of Energy
Office of Scientific and Technical Information

Thermal/chemical degradation of inorganic membrane materials

Technical Report ·
DOI:https://doi.org/10.2172/10185708· OSTI ID:10185708

The overall objective of this program is to evaluate the long-term thermal and chemical degradation of inorganic membranes that are being developed to separate gaseous products produced by the gasification or combustion of coal in fixed-, fluidized-, and entrained-bed gasifiers, direct coal-fired turbines, and pressurized-fluidized-bed combustors. Specific objectives of this program are to (1) quantify the extent of the degradation process for the three most detrimental mechanisms by performing laboratory-scale experiments, and (2) develop a predictive model for membrane degradation under operating conditions. At present, no inorganic membranes are commercially available for application in the high-temperature, high-pressure (HTHP) gas environments encountered in integrated gasification combined cycle (IGCC), pressurized fluidized bed combustion (PFBC), and direct coal fired turbine (DCFT) applications. Most of the inorganic membrane development efforts have focused on hydrogen separation membranes which may be used in an IGCC system for maximizing hydrogen production from coal gas or to remove H{sub 2}S and NH{sub 3} contaminants via thermal or catalytic decomposition of these contaminants. The candidate inorganic membranes may be grouped as follows: dense metallic membranes; silica based membranes; alumina based membranes; and carbon based membranes. Results are reported for membrane characterization done so far.

Research Organization:
SRI International, Menlo Park, CA (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
AC21-92MC28053
OSTI ID:
10185708
Report Number(s):
DOE/MC/28053--94/C0367; CONF-9406131--24; ON: DE95000547; BR: AA1505000
Country of Publication:
United States
Language:
English